Mechanical Properties of Bedded Rock Salt Zhao Yan-Lin School of Energy and Safety, Hunan University of Science and Technology, Xiangtan 411201, China; Hunan Provincial Key Laboratory of Safe Mining Techniques of Coal Mines, Hunan University of Science and Technology, Xiangtan 411201, China e-mail: [email protected] Wan Wen School of Energy and Safety, Hunan University of Science and Technology, Xiangtan 411201, China; Hunan Provincial Key Laboratory of Safe Mining Techniques of Coal Mines,Hunan University of Science and Technology, Xiangtan 411201, China ABSTRACT Taking the Sodium Chloride rock salt specimens containing mudstone interbed which located at 600-700 m level of Yun Ying salt-mine in Hubei as the research objects, the conventional mechanical tests on the specimens and uniaxial compression creep tests on the specimens under multi batch stress levels were performed. The conventional mechanical tests obtained the result that the bedded rock salt is a kind of special combined soft rock,its elastic modulus is comparative little, but lateral deformation of the rock salt is great under uniaxial compression stress state. Through creep experiments , the results were obtained as follows: (1) If the duration of creep is enough long , the attenuation creep stage, the steady creep stage and the accelerative creep stage are appeared during the bedded rock salt creep, with the accelerative creep stage last longer compared with other rocks. (2) The phenomenon of invagination of interlayer and bulge of rock salt is found at the teady creep stage. Uncoordinated creep deformation may lead to shear dislocation in the interbed KEYWORDS: bedded rock salt, creep characteristics, creep test, failure mechanism INTRODUCTION Energy resources are very important to nation's economy, petroleum and natural gas are strategic resources, which has been related to economic development and society stabilization of a country. Underground storage project of oil is used to regulate the demand of the market, which is also related to national energy security. At present, underground gas storage projects are almost constructed in sedimentary rocks of rock salt, because rock salt has good physical properties including compact structure, relatively low porosity (0.01%-5%) and good - 9347 - Vol. 19 [2014], Bund. Z 9348 creep behavior [1-3]. Salt cavern construction is a pioneered attempt for strategic reserve in China. As the first salt cavern gas storage in China, Jintan salt cavern underground gas storage is a complicated systemic project [4,5]. Salt cavern underground gas storage need to be built in rock salt purity better, but the scarcity of salt dome type ore deposit in China, the salt layer often contain many interlayer, gas storage is built in bedded rock salt deposit rather than thick salt dome , which will meet more complicated mechanical and technical issues[6]. The issues include the creep convergence stability of dissolved cavity and creep properties heterogeneity of bedded rock salt. At present, scholars have done a large number of test and theoretical analysis for the mechanical properties of rock salt at home and abroad, especially the creep characteristics. U.Hunsche et al. [7] made a more detailed study on the creep constitutive model of rock salt. Jianchun ma etc. [8] made a systemic study on the rheological properties of rock salt. Chunhe Yang et al. [8] has established the Cosserat medium extension constitutive model of salt rock mass. Wei zhong Chen et al. [9] has established nonlinear creep damage constitutive model of rock salt. Bedded salt rock is a kind of special combined soft rock, creep properties of bedded rock salt and the creep damage failure process between bedded rock salt and interlayer are worth further research. The short and long term experiments of bedded salt rock specimen cored from 600-700 m level of Yun Ying salt-mine in Hubei were studied in this paper. SHORT-TERM MECHANICAL CHARACTERISTICS OF BEDDED ROCK SALT Taking the Sodium Chloride rock salt specimens containing mudstone interbed which located at 600-700 m level of Yun Ying salt-mine in Hubei as the research objects. Using geological drilling rig to obtain core. Because of layered salt rocks containing weak surface layer, standard specimen can not be obtained. Based on the rock mechanics test standards, cylindrical specimen of 2:1 ratio of height to diameter can be used, its size is φ 90mm × 180mm . Short-term mechanical characteristics Various conventional experiment have been made for bedded rock salt, pure rock salt and mudstone, the following conclusions can be obtained. (1) Bedded salt rock is a kind of special combined soft rock, compared with the common rock, its uniaxial compressive strength and deformation modulus are relatively small, while lateral deformation capacity is very large. When axial stress σ = 0.5σ c (where σ c =compressive strength of rock salt specimen), transverse deformation coefficient of bedded rock salt can reach 0.48. Table 1 is the experimental results of bedded rock salt samples under uniaxial compression. Vol. 19 [2014], Bund. Z 9349 (2) Poisson's ratio of mudstone interbed is smaller than bedded rock salt, however, the elastic modulus of mudstone is bigger. Fig.1 is the stress-strain curve of three kinds of rock specimens, when the loading stress reaches the peak stress, axial strain of rock salt is the largest, bedded rock salt takes second place, mudstone minimum. The elastic modulus of mudstone is 4.2 times higher than rock salt, Poisson’s ratio of mudstone is about 0.74 times of the rock salt. Under the same stress level, the deformation of salt rock is a lot bigger than mudstone, uniaxial compressive strength of mudstone is slightly bigger than rock salt. When the uniaxial compressive stress acts on the bedded rock salt, the deformation is mainly composed of rock salt layers in bedded salt rocks. Table 1: Experimental results of layered rock salt samples under uniaxial compression uniaxial compressive strength σ c /MPa 22.8MPa σ = 0.5σ c The appearance of macro cracks Poisson ratio μ tangent modulus E / GPa axial stress σ v /MPa axial strain ε/ % 0.48 8.1GPa 16.5 0.45 Figure 1: Stress-strain curve of three kinds of rock specimens LONG-TERM MECHANICAL CHARACTERISTICS OF BEDDED ROCK SALT To study the long-term strength of bedded rock salt, mid long term uniaxial static creep test of bedded salt rock specimens has been done, which was conducted by RYL - 600 microcomputer control rock shear rheometer and controlled by Japan panasonic whole digital ac servo high system. Experimental apparatus are shown in Fig.2. Vol. 19 [2014], Bund. Z 9350 Figure 2: Uniaxial static creep test of layered rock salt Uniaxial static creep test was conducted by single-stage loading way, single-stage loading had a total of four batches, four batches of axial stress were respectively σ 1 = 8MPa, σ 2 = 11MPa, σ 3 = 14MPa, σ 4 = 16MPa . Figure 3: Creep curve of bedded rock salt 2#( σ = 11MPa ) Figure 4: Creep curve of bedded rock salt 4#( σ = 16MPa ) Vol. 19 [2014], Bund. Z 9351 Fig.3 is the creep test curve of bedded salt rock specimen 2 # when loading stress is 11MPa. Under the stress level, creep in the period of attenuation, steady period and period of acceleration can be shown all in 130d. Attenuation creep stage lasts about 15d. The attenuation creep strain is 70%~80% of total creep strain, the steady-state creep stage last very long, steady-state creep rate is about 6.07×10-6/d, when t=130d , creep goes into the accelerated creep stage, and specimen was damaged 12 days later. Fig.4 is the creep test curve of bedded salt rock specimen 4 # when loading stress is 16 MPa. The total creep time is 160 d. Under the stress level, attenuation creep stage lasted about 30d, Steady creep rate is about 3.7×10-5/d. when t=127d , creep went into the accelerated creep stage, specimen was damaged 33 days later. Test found that bedded rock salt specimen creep has two notable features;(1)In the steady-state creep stage, creep rate of rock salt is greater than mudstone interbed, rock salt has stronger rheological properties, the steady state creep stage appeared the phenomenon of specimen dissection inward concave and rock salt layer bulge outward. Oil and gas reservoir is established in bedded rock salt, shear dislocation of rock salt layer provides channels for oil and gas leakage. Figure 5 is a schematic diagram of creep failure of each interlayer of bedded rock salt.(2)Compared with the other rocks, accelerating creep stage of bedded salt rock lasts longer, when loading stress is 11MPa~16MPa, accelerating creep stage is 10d~32d. Cleavage plane of easily splitting exists in the rock salt crystal, rock salt crystal is easy to be split along the plane that parallel to the cleavage plane into cubes under the action of external force. Generally, microfissure can be formed and develop gradually when the bedded salt rock is in the early stage of creep. Cracks basically achieve stability in steady-state creep stage, when creep enter the stage of accelerated creep, some damage phenomena are found in many bedded salt rock specimens, firstly, interlayer splitting failure, and then salt rock of interbedded pulling damage, at last, bedded salt rock failure as the axial tension crack splitting. Figure 5: Schematic diagram of creep failure of each interlayer of bedded rock salt Vol. 19 [2014], Bund. Z 9352 CONCLUSION (1) Bedded salt rock is a kind of special combined soft rock, deformation modulus is relatively small, while lateral deformation capacity is very large. When the uniaxial compressive stress acts on the bedded rock salt, the deformation is mainly composed of rock salt layers in bedded salt rocks. (2) Creep rate of rock salt is greater than mudstone interbed in steady-state creep stage, specimen dissection inward concave and salt rock layer bulge outward. The uncoordinated creep may lead to shear dislocation in the interbed. (3) In full long creep time, attenuation creep stage, steady-state creep stage and accelerating creep stage, three stages of bedded salt rock creep are all appeared, and the accelerated creep stage lasts long. REFERENCES [1] Thorms R L, Gehle R L. A brief history of salt cavern use[C]//USA: SMRI Fall Meeting, 2000. 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