Linearity of Coriolis Mass Flowmeters Dean Standiford Director Global Calibration Quality Overview !! Purpose: –! To answer the customer’s question, “How do I know the output from my Coriolis flow meter is valid beyond the calibrated mass flow range?” !! Scope: –! High Capacity Coriolis flow meters •! 6”, 8”, 10” •! >25% of maximum flow range •! Based on water calibration March 26, 2014 2 1! Summary Coriolis flowmeters are inherently linear devices. Each Coriolis flowmeter has a unique mass flow calibration constant (flow calibration factor, FCF), that when determined correctly, is valid for the entire operating mass flow range. March 26, 2014 3 Agenda !! Coriolis mass flow equation !! Calibration processes !! Mass Flow Linearity Results !! Validating the Calibration !! Conclusion March 26, 2014 4 2! Mass Flow w/Coriolis Flowmeters !! Basic Measurement Measuring tubes are forced to oscillate producing a sine wave. At zero flow, the two tubes vibrate in phase with each other. When flow is introduced, the Coriolis forces cause the tubes to twist resulting in a phase shift. The time difference between the sine waves is measured and is directly proportional to mass flow rate. !"#$%&'()% !"#$%"&# &'()$(%*"+,-..% /"01)2+$#$3(% 43)$(%*"+,-..% /"01)2+$#$3(% +,-.$-%/"*01''% &"23.4*$#$)-% 5).$-%/"*01''% &"23.4*$#$)-% !"#$% !"#$% !"#$%&"''$($)*$% March 26, 2014 5 Coriolis Mass Flow Equation !! Mathematical Derivation Force: "!#$%& "#! ""#'() "#$%&'( "#+! ! ""#)* (1) Coriolis Force, named for Gustav Coriolis (2) Because the direction of the flow changes between the inlet and outlet tube, the direction of the force changes. As the tube vibrates about axis “o”, an oscillation moment develops: %%%&$ '$ ( %%%%& !"# #) ') ! (3) ####$& '(')" % )& ! !" % ! Since: ###$ *%,! ! " #$% & " #&'#() *%+ , combine equations (2) & (3) '(! '() or ! " #$%& (4) March 26, 2014 6 3! Coriolis Mass Flow Equation !! Mathematical Derivation cont’d. '(! '() Making the substitution into: ! " #$%& %& !$ ! ' !" # (5) Equation (4) becomes: (6) ! " #$ %&'()*! The moment “M” is being resisted by the mechanical properties of the sensor tube. The torque on the tube is given by: (7) ! " #$ %! Where: !" ! is the stiffness of the tube & !! is the amount of twist (in degrees). By definition: ! " #! so: !" # $ %& '()*+,! (8) $% & !" # ! '( )*+, (9) March 26, 2014 7 Coriolis Mass Flow Equation !! Mathematical Derivation cont’d. By definition: !" # $ ! % &' (10) $ & % ! Substituting (10) into (9): !" # '( )*+, $% ) *+! &'( Coriolis Mass Flowmeter (11) All of the values (except !"!) are constants that when lumped together MMI calls the flow calibration factor: (12) !" # $%$ & '(! !" # $%$ & '() * ()+ ,! !" # $%$ & '( ) *$%$ & '(+ ,! 30000 25000 Reference Mass Flow, kg/min !" # 20000 15000 10000 5000 equation of a line: ! " # $ % & '! ! " #$%&' ( )*)! 0 ! " #$%&'(&)% * +,-.- / 0%1 2! 0 5000 10000 15000 20000 Coriolis Mass Flow, kg/min 25000 30000 March 26, 2014 8 4! Calibration Processes !! Calibration operation that, under specified conditions, in a first step, establishes a relation between the quantity values with measurement uncertainties provided by measurement standards and corresponding indications with associated measurement uncertainties and, in a second step, uses this information to establish a relation for obtaining a measurement result from an indication. NOTE 1 A calibration may be expressed by a statement, calibration function, calibration diagram, calibration curve, or calibration table. In some cases, it may consist of an additive or multiplicative correction of the indication with associated measurement uncertainty. NOTE 2 Calibration should not be confused with adjustment of a measuring system, often mistakenly called “self-calibration”, nor with verification of calibration VIM – International vocabulary of metrology, Basic and general concepts and terms (JCGM 200:2008) March 26, 2014 9 Calibration Processes !! calibration - The comparison of measuring equipment of unknown measurement uncertainty to a reference standard of known measurement uncertainty to determine an estimate of the error. –! Such as: comparing the reading of a flow meter to a calibrated reference to determine the estimate of error (step 1), which can then be used to adjust the flow meter output if required (step 2). !! verification - Evidence by calibration that specified requirements have been met. –! A decision made by analyzing the calibration data. March 26, 2014 10 5! Calibration Processes !! Micro Motion mass flow calibration process for a Coriolis Mass Flowmeter –! Ensure stable process conditions –! Determine Coriolis zero offset •! Intercept !" # $%$ & '( ) *$%$ & '(+ ,! –! Determine mass flow error at the best flowrate for adjusting FCF –! Make an adjustment to the FCF •! Slope !" # $%$ & '( ) *$%$ & '(+ ,! –! Verify the adjustment is valid March 26, 2014 11 Calibration Processes !! What is the “best flowrate” for adjusting the FCF? –! Because Coriolis flowmeters are linear devices: •! Any flowrate where errors are minimized –! Zero stability –! Process repeatability –! System Limitations March 26, 2014 12 6! Calibration Processes 254cm (10”)+ line sizes 186kw (250hp) + pumps 30t (66,139lb) weigh systems Multiple reference meters March 26, 2014 13 Calibration Process – FCF Adjustment Coriolis Mass Flowmeter 0.50 50% of Maximum Flow Rate = Nominal Flow Rate (~1 bar dp) 0.40 <#%'5':". =>= ?.@/-%5"0%* !$0A" 0.30 Typical Error, % 0.20 0.10 0.00 -0.10 -0.20 !"#"$%$&'('%)*"++,+-*./"*%,*'01+"$-".*2(,3* 0,'-" $0.*-4,+%"+*&$%14* %'5"- -0.30 -0.40 -0.50 6++,+- ./"*%,* 789*,2*:"+,*-%$&'('%)*-#"1'2'1$%',0*;$(/" 0 10 20 30 40 50 60 70 Flow Rate, % Maximum 80 90 100 110 March 26, 2014 14 7! Mass Flow Linearity Results CMF300 S/N: 11005156 0.50 3.5 0.40 3.0 !"#$%&'()*)(&+,-./012/(3'456&/1( 0.30 Mass Error, % of Reading 0.10 2.0 0.00 1.5 -0.10 -0.20 1.0 -0.30 761..-61(864# -0.40 -0.50 Pressure Drop, bar 2.5 0.20 0.5 50% of Maximum Flow Rate = Nominal Flow Rate (~1bar dp) 20 30 40 50 60 70 Flow Rate, % Maximum Test #1 Test #2 80 90 100 0.0 Test #3 March 26, 2014 15 Mass Flow Linearity Results CMFHC2 S/N: 13053120 0.50 0.40 !"#$%&'()*)(&+,-./012/(3'456&/1(7899(:;<0$2 0.30 Mass Error, % of Reading 0.20 0.10 0.00 -0.10 -0.20 -0.30 -0.40 -0.50 0 2,000 4,000 6,000 8,000 Flow Rate, kg/min Test #1 10,000 12,000 14,000 16,000 Test #2 March 26, 2014 16 8! Mass Flow Linearity Results CMFHC3 S/N: 12074130 0.50 0.40 0.30 Typical FCF adjustment flowrate = 12,000 kg/min Mass Error, % of Reading 0.20 0.10 0.00 -0.10 -0.20 -0.30 -0.40 -0.50 0 2000 4000 6000 8000 10000 12000 Mass Flow Rate, kg/min USA 14000 Netherlands 16000 18000 20000 China March 26, 2014 17 Mass Flow Linearity Results CMFHC4 S/N: 12074922 0.50 0.40 0.30 Typical FCF adjustment flowrate = 12,000 kg/min Mass Error, % of Reading 0.20 0.10 0.00 -0.10 -0.20 -0.30 -0.40 -0.50 0 5000 10000 USA 15000 Flow Rate, kg/min China Test #1 20000 25000 30000 China Test #2 March 26, 2014 18 9! Validating the Calibration Coriolis mass flow meters are linear, but how does MMI provide confidence to its customers about the data? !! Gather Historical Data –! 30+ production meter calibration samples –! FCF calibrated at a flow rate less than maximum !! Analyze data to a 95% confidence level for conclusions March 26, 2014 19 Validating the Calibration CMFHC3 FCF Calibration at Boulder and then Verified at Higher Flowrate at Ede or AFTC 0.50 0.40 0.30 Batch Error, % 0.20 0.10 0.00 -0.10 -0.20 -0.30 -0.40 -0.50 0 5000 USA- FCF Calibration 10000 15000 Flow Rate, kg/min Netherlands- FCF Verify 20000 25000 China- FCF Verify March 26, 2014 20 10! Validating the Calibration Summary CMFHC3 FCF Verify Error % A nderson-Darling N ormality Test -0.04 0.00 0.04 0.08 A -S quared P -V alue 0.46 0.240 M ean S tDev V ariance S kew ness Kurtosis N 0.008767 0.031685 0.001004 -0.154286 0.245871 30 M inimum 1st Q uartile M edian 3rd Q uartile M aximum -0.061000 -0.007925 0.009600 0.024375 0.083300 95% C onfidence Interv al for M ean -0.003065 0.020598 95% C onfidence Interv al for M edian 0.003675 0.021654 95% C onfidence Interv al for S tDev 9 5 % C onfidence Inter vals 0.025234 Mean 0.042594 RSS of lab uncertainties = 0.042% Median 0.000 0.005 0.010 0.015 0.020 0.025 March 26, 2014 21 Validating the Calibration CMFHC4 FCF Calibration at Boulder and then Verified at Higher Flowrate at Ede or AFTC 0.50 0.40 0.30 Batch Error, % 0.20 0.10 0.00 -0.10 -0.20 -0.30 -0.40 -0.50 0 5000 10000 USA- FCF Calibration 15000 20000 Flow Rate, kg/min Netherlands- FCF Verify 25000 30000 35000 China- FCF Verify March 26, 2014 22 11! Validating the Calibration Summary CMFHC4 FCF Verify Error % A nderson-Darling N ormality Test -0.10 -0.05 0.00 0.05 A -S quared P -V alue 0.27 0.659 M ean S tDev V ariance S kew ness Kurtosis N -0.022345 0.040204 0.001616 0.404551 0.565730 33 M inimum 1st Q uartile M edian 3rd Q uartile M aximum -0.100360 -0.047830 -0.019780 -0.001220 0.076900 95% C onfidence Interv al for M ean -0.036600 -0.008089 95% C onfidence Interv al for M edian -0.037828 -0.009015 95% C onfidence Interv al for S tDev 9 5 % C onfidence Inter vals 0.032331 Mean 0.053177 RSS of lab uncertainties = 0.042% Median -0.040 -0.035 -0.030 -0.025 -0.020 -0.015 -0.010 March 26, 2014 23 Validating the Calibration - Conclusions !! Gather Historical Data –! 30+ production meter calibration samples –! FCF calibrated at a flow rate less than maximum !! Analyze data to a 95% confidence level for conclusions –! Sample data is normally distributed –! Mean Error for Both meters is less than 0.042% •! (RSS of flow stand uncertainty) March 26, 2014 24 12! Conclusion Coriolis flowmeters are inherently linear devices. Each Coriolis flowmeter has a unique mass flow calibration constant (flow calibration factor, FCF), that when determined correctly, is valid for the entire operating mass flow range. Mass Flow Error is within the meter specification when FCF is calibrated at less than maximum flow rate. March 26, 2014 25 13!
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