HTC-13 / HTSP

1
HTC-13 / HTSP-3 (2014)
13th International Symposium on Hyphenated Techniques in
Chromatography and Separation Technology
29 – 31 January 2014
3rd International Symposium on Hyphenated Techniques for
Sample Preparation
28 – 29 January 2014
Symposia organised by the Royal Flemish Chemical Society (KVCV), Belgium and
the Royal Society of Chemistry (RSC), UK
Venue: Site Oud Sint-Jan, Mariastraat 38, B-8000 Bruges (Belgium)
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1. CONFERENCE COMMITTEES
INTERNATIONAL ORGANIZING COMMITTEE
Frédéric Lynen, Belgium (Conference chair)
Hernan Cortes, USA (Chairman scientific committee)
Rudy Senten, Belgium (Secretary)
Freddy Van Damme
Tom Lynch, United Kingdom (RSC)
LOCAL ORGANIZING COMMITTEE
Frédéric Lynen, Belgium (Conference Chair, sponsoring)
Rudy Senten, Belgium (Secretary, Treasurer)
Rob Edam, The Netherlands (Workforce coordinator)
Etienne Jooken, Belgium (Site coordinator, Logistics)
Deirdre Cabooter, Belgium (Registrations, Chairman Poster Prize)
Joeri Vercammen, Belgium (Short Courses, tutorials)
Sebastiaan Eeltink, The Netherlands (Coordinator Scientific Program, Book of Abstract)
Chris Smits, Belgium (Social program)
SCIENTIFIC COMMITTEE
Hernan Cortes, USA (Chairman)
Hian Kee Lee, Singapore
Gert Desmet, Belgium
Tuulia Hyötyläinen, Finland
Luigi Mondello, Italy
Philip Marriott, Australia
Janusz Pawliszyn, Canada
Valérie Pichon, France
Robert Shellie, Australia
Yvan Vander Heyden, Belgium
Ian Wilson, UK
Ralf Zimmermann, Germany
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2. DELEGATES
•
•
•
•
•
•
•
RSC: (19) 21
Company delegate: (48) 46
Scholarship: (3) 4
Invited guests: (4) 6
Delegates: (200) 159
Committee members (organizing, scientific, executive): (44) 46
Invited speakers: (20) 22
(total = 306)
DELEGATES/DAY
date
Tuesday 28 January 2014
Wednesday 29 January 2014
Thursday 30 January 2014
Friday 31 January 2014
delegates
(161) 122
(330) 302
(313) 293
(304) 286
activity
HTSP-3
HTC-13 + HTSP-3 + RSC
HTC-13 + RSC
HTC-13 + RSC
DELEGATES/COUNTRY
Australia
Austria
Belgium
Brazil
Canada
Columbia
Botswana
Czech Republic
Croatia
Finland
France
Germany
Greece
Israel
Italy
Japan
5
4
112
2
3
2
1
3
1
1
19
19
3
1
6
6
Luxemburg
Norway
Oman
Poland
Russia
S. Korea
Saudi Arabia
Servia
Singapore
South Africa
Spain
Switzerland
Taiwan
The Netherlands
UK
USA
1
1
1
3
1
1
2
1
1
2
6
7
2
25
52
10
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3. SCIENTIFIC PROGRAMME
• LECTURES AND COMPANY SEMINARS
activity
HTSP-3
subtotal
HTC-13
RSC
total
Award session
0
1
1
2
plenary
2
2
0
4
keynote
5
23
1
29
oral
15
39
11
65
tutorial
0
8
2
10
product
seminars
subtotal
0
7
0
7
22
80
15
117
• POSTERS
(Hyphenated) sample preparation
Gas chromatography / mass
spectrometry
GC X GC
26
27
12
Column technology
9
LC-MS
24
LC X LC
7
New Instrumentation, methods, and
detection techniques
9
Sub- and supercritical fluid
chromatography
6
(Bio-)pharmaceutical
6
Life sciences (including proteomics and
metabolomics)
total
11
137
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4. AWARDS
• LIFETIME-ACHIEVEMENT AWARD
The Lifetime Achievement Award in Chromatography, sponsored by LC-GC Europe, was established in
2006 to recognize outstanding achievements in hyphenated techniques in chromatography and for
distinguished service to the International chromatographic community.
Previous recipients of the Lifetime Achievement Award are Professor James Jorgenson, University of
North Carolina, Chapel Hill, USA, (2006) Dr. Robert Smits, Oostduinkerke, Belgium, (2008), Professor
Pat Sandra, Ghent University, Ghent, Belgium (2010) and Professor Milos V. Novotny, Indiana
University, Bloomington, USA
The 2014 Lifetime Achievement Award recipient, presented at the HTC-13 Conference on 29 January
2014 is Professor Milton L. LEE, H. Tracy Hall Professor of Chemistry (1985-present) at the
Department of Chemistry and Biochemistry, Brigham Young University, Provo, Utah (USA).
Professor LEE is specialized in micro separation techniques, monolithic stationary phases and in
hand-portable GC-MS.
•
HTC-AWARD
The most innovative paper or poster receives the HTC-Award, sponsored by Elsevier Science. This
Award was established in 1996.
Previous HTC-Award winners are Janusz Pawliszyn, University of Ontario, Canada (1996), Semjon
Semenov, University of Moscow, Russia (1998), Heidi Goenaga-Infante, University of Antwerp,
Belgium (2000), Aviv Amirav, Tel Aviv university, Israel (2002), Gert Desmet, Free University of
Brussels, Belgium (2004), Luigi Mondello, University of Messina, Italy (2006), Robert Shellie,
University of Tasmania, Australia (2008), Oliver Trapp, University of Heidelberg, Germany (2010) and
Tuulia Hyötyläinen, VTT Research Institute, Finland (2012)
The 2014 Award recipient is Dr. Frank DAVID, Research Institute for Chromatography, Kortrijk and
University of Gent (Belgium)
• POSTER AWARD
The most innovative poster contributions of HTC-13 received the HTC-13 Poster Award.
Jelle DE VOS, Vrije Universiteit Brussel, Brussels (Belgium) received the first Poster Award
Poster P_INST_3.
A fundamental study of post-column focusing in liquid chromatography
Authors: Jelle De Vos, Gert Desmet and Sebastiaan Eeltink
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Piotr ALVAREZ, Ghent University, Ghent (belgium) received the second Poster Award
Poster P_LIFE_5.
Combining multiplexed gel capillary electrophoresis with liquid chromatography for offline
comprehensive analysis of complex oligonucleotide samples
Authors: Piotr Alvarez and Frederic Lynen
Thorsten TEUTENBERG, Institut für Energie- und Umwelttechnik e.V., Duisburg (Germany) received
the third Poster Award
Poster P_LCMS_12.
Evaluation of a concept hyphenating flame ionization detection with nano- and capillary liquid
chromatography
Authors: Thorsten Teutenberg, Christian Becker, Maik Jochmann, Oliver Gassner and Steffen Wiese
• KNOX MEDAL WINNER
Peter Schoenmakers, University of Amsterdam, The Netherlands received the Knox Medal during the
opening session of the RSC-session on Thursday 30 January 2014.
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5. STATE-OF-THE-ART AND KEYNOTE LECTURES
PLENARY LECTURES
Monoliths and size exclusion chromatography for separation of large biomolecular assemblies
Alois Jungbauer, Petra Steppert
University of Natural Resources and Life Sciences Vienna, Vienna, Austria.
SPME for on-site and lab quantification in complex systems – advantages and limitations
Janusz Pawliszyn
Department of Chemistry, University of Waterloo, Waterloo, ON, CA
Biological and biomimetic approach for selective sample pretreatment: development and application
to trace analysis in real samples and hyphenation with miniaturized analytical devices
Valérie Pichon, Audrey Combes, Fabien Brothier
ESPCI ParisTech/UPMC, Paris, FR
Instrument influences on observed column performance
Gert Desmet, Kim Vanderlinden, Yoachim Vanderheyden, Ken Broeckhoven
Vrije Universiteit Brussel, Brussels, BE
From good multi-dimensional data to great multi-dimensional information
Hans-Gerd Janssen, Ngoc A Dang , Sonja Kaal-Peters , Arend Kolk, Gabriel Vivo Truyols
Unilever Research and Development Vlaardingen, NL
One-dimensional and comprehensive two-dimensional gas chromatography coupled to a multireflection, ultra-high resolution time-of-flight-mass spectrometer for characterization of complex
mixtures
Ralf Zimmermann a, Thomas Gröger a, Marie Schäffer a, Benedikt Weggler a, Jürgen Wendt b,
Martin Sklorz a, Theo Schwemer a
A Joint Mass Spectrometry Centre of University of Rostock, Chair of Analytical Chemistry,
Rostock/Germany and Helmholtz Zentrum München, DE
B LECO Instrumente GmbH, DE
RSC: KNOX MEDAL WINNER
Selective two-dimensional separations in a hyphenation context
Peter Schoenmakers
University of Amsterdam, NL
LIFE-TIME-ACHIEVEMENT AWARD HTC-13
Thermal Gradient Gas Chromatography – A New Paradigm for Hyphenation
Milton L. Lee, Anzi Wang, Jesse A. Contreras, Samuel E. Tolley, Matthew C. Asplund, Department of
Chemistry and Biochemistry
Aaron R. Hawkins, Department of Electrical and Computer Engineering
H. Dennis Tolley, Department of Statistics
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Brigham Young University, Provo, USA
KEYNOTE LECTURES
GC-MS and mass fingerprinting for understanding and measuring aroma characteristics in food
products
P. Dirinck, I. Dirinck
Odour & Flavour Consultancy bvba and SENSNET vzw, BE
Use of liquid chromatography-high resolution mass spectrometry (LC-HRMS) in bioanalytical assays
applying micro-sampling of biological fluids blood for the determination of drug pharmacokinetics in
clinical studies
Juan Pablo Rincon, Roland J.W.Meesters
Universidad de los Andes, Bogota, CO
Multi-stir bar sorptive extraction (mSBSE): A new approach for SBSE using both non-polar and polar
coatings
Nobuo Ochiai, Kikuo Sasamoto, Teruyo Ieda, Frank David, Pat Sandra
Gerstel, Tokyo, JP
Use of laboratory chromatographs as online-instruments for wastewater monitoring
Monika Wortberg, Winfried Ziemer, Christian Eichberger
BASF, Ludwigshafen, DE
Systematic optimisation and evaluation of LC×LC separation of phenolics: Fundamental aspects and
selected applications
A. de Villiers 1, K.M. Kalili 1, C.M. Willemse 1, M.A. Stander 2,3
1 Stellenbosch University, Department of Chemistry and Polymer Science, SA
2 Stellenbosch University, Central Analytical Facility, SA
3 Stellenbosch University, Department of Biochemistry, SA
Rapid collection of high solute amounts by using an on-line four-dimensional LC-GC-GC-GC
preparative instrument
Luigi Mondello 1,2, Danilo Sciarrone 1, Sebastiano Pantò 1, Peter Q. Tranchida 1
1 Dipartimento di Scienze del Farmaco e dei Prodotti per la Salute - University of Messina, Messina,
IT
2 Centro Integrato di Ricerca (C.I.R.), University Campus Bio-Medico, Roma, IT
You are what you eat: Using GCxGC to unravel the diet of the whale shark
Robert Shellie, Laura Tedone
ACROSS, UTAS, Hobart, AU
Towards a simpler future in comprehensive two dimensional gas chromatography
Tadeusz Gorecki, Matthew Edwards, Ahmed Mostafa
University of Waterloo, Waterloo, ON, CA
New hyphenated techniques for aroma analysis
Frank David 1, Maria Rambla-Alegre 1, Nobuo Ochiai 2, Kikuo Sasamoto 2, Kazuhisa Mitsui 3, Eri Masugi
3
, Yuta Yoshimura 3, Hisanori Nagata 3, Pat Sandra 1
1 Research Institute for Chromatography, Kortrijk, Belgium
2 Japan Tobacco Inc., Tobacco Science Research Center, Yokohama, Japan
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3 GERSTEL K.K., Tokyo Japan
Pulsed flow modulation GCxGC-MS with cold EI – the emergence of GCxGCxMS
Aviv Amirav, Alexander B. Fialkov, Uri Keshet, Tal Alon
School of Chemistry, Tel Aviv University, IS
Design of the selectivity of stationary phases
Michael Lämmerhofer
University of Tuebingen, Tuebingen, DE
Detailed characterization of the kinetic performance of first and second generation silica monolithic
columns for reversed-phase chromatography separations.
Deirdre Cabooter, Alison Vanmessen, Ken Broeckhoven, Kazuki Nakanishi, Sander Deridder, Gert
Desmet
KU Leuven, Leuven, BE
Translational environmental analytical chemistry: laboratory-to-field possibilities
Hian Kee Lee
National University of Singapore, Singapore, SG
Polymeric monolithic materials for miniaturised bioanalysis
Emily Hilder, Boon Hon Wei, Chris Desire, Dario Arrua, Esme Candish, Robert Shellie, Andrew Gooley
University of Tasmania, Hobart, AU
Large Scale Metabolic Phenotyping of Populations and Patients
Jeremy K. Nicholson
Imperial College, UK
Next generation blood sampling in mass spectrometry based point of care diagnostics
Fred Regnier, JinHee Kim, Tim Woenker
Purdue University, West Lafayette, USA
Combination of LC/MS and multivariate data analysis in the search for lipid biomarkers of serious
human diseases
Michal Holčapek, Eva Cífková, Miroslav Lísa, Blanka Červená
University of Pardubice, Faculty of Chemical Technology, Department of Analytical Chemistry,
Pardubice, CZ
Planar microfluidic devices and selective detection in multi-dimensional gas chromatography
Hernan J. Cortes 1,3, Robert A. Shellie 1, Jim Luong 1,2
1 Australian Centre for Research on Separation Science (ACROSS), University of Tasmania, AU
2 Dow Chemical Canada ULC, CA
3 HJ Cortes Consulting LLC, USA
Interaction of volatile organic compounds with airborne particulate matter by means of selected ion
flow tube mass spectrometry (SIFT-MS)
Christophe Walgraeve, Herman Van Langenhove, Kristof Demeestere
Ghent University, Gent, BE
High throughput peptides characterization in crude venoms: online sequencing and disulfide bridges
annotation using multidimensional separation methods coupled to mass spectrometry.
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Loic Quinton 1, Michel Degueldre 1, Julien Echterbille 1, Philippe Massonet 1, Marion Verdenaud 1,
Nicolas Gilles 1, De Pauw Edwin 1
1 Mass Spectrometry Laboratory, GIGA-R, Université de Liège, BE
2 CEA/DSV/iBiTec-S/SIMOPRO Toxins, Receptors and Channels team, FR
Multiple reaction monitoring, a good old friend rediscovered in hypothesis-driven proteomics
Simon Devos, Bart Devreese
Ghent University, Gent, BE
Last developments in chromatography coupled to mass spectrometry to guarantee a high level of
chemical food safety
Bruno Le Bizec, Emmanuelle Bichon, Frabrice Monteau, Stephanie Prevost, Ludivine Seree, JeanPhilippe Antignac, Gaud Dervilly-Pinel
Laberca, Nantes, FR
Characterization of cheese using a foodomics approach
Erwin Kaal, Cock Tas, Joep van Rijn, Adriana Carvalho de Souza, Eduard Derks, Brenda Ammerlaan,
Marjon Kok, Lizette Maljaars, Marcel van Tilborg
DSM Biotechnology Center, Delft, NL
Pimp my GC
Philip Marriott, Sung-Chin Tong, Blagoj Mitrevski, Sun Kim Lee
Monash University, Clayton, AU
Quantitative offline and online characterization of petrochemical and petroleum samples by
Comprehensive Two-Dimensional Gas Chromatography coupled to FID/SCD/NCD/TOF-MS
Kevin van Geem
Ghent University, Ghent, BE
Modulation and signal enhancement in liquid chromatography
Jelle De Vos, Gert Desmet, Sebastiaan Eeltink
Vrije Universiteit Brussels, BE
Impact of extra-column band-broadening on the peak capacities of ultra-fast gradient separations in
2D-LC/UV or 2D-LC/MS
Monika Dittmann, Stephan Buckenmaier
Agilent Technologies, Waldbronn, DE
Reading the decomposition chemistry of human remains with a new pair of glasses
Jean - François Focant, PH. Stefanuto, S. Stadler, K. Perrault, R. Pesesse, S. Forbes
University of Liège, Liège, BE
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6. EXHIBITORS AND SPONSORS
The organizers wish to express their dearest appreciation to the following sponsors for their
generous support. Without their valuable financial and technical support, this major symposium
would not have been possible.
AB Sciex
Cheryl Goodall, Warrington, Cheshire, United Kingdom
Nina Dressel, Darmstadt, Germany
Exhibitor
Achrom
Nina Van Bockstal, Zulte, Belgium
Exhibitor
Advion
Kees Vlak, Harlow, United Kingdom
Exhibitor
American Elements
Lyon, France
Sponsor
Atas GL
Geert Alkema, Eindhoven, The Netherlands
Exhibitor
Campro Scientific and FMS
Chris van Wakeren, Veenendaal, The Netherlands
Yunyun Zou, Watertown, MA, USA
Exhibitor
Chromatography Today
St. Albans, United Kingdom
Chromedia
Frank Van Geel, The Netherlands
Elsevier
Betty Chang, Bejing, China
HTC-Award
Fonds Wetenschappelijk Onderzoek Vlaanderen
Brussel, Belgium
Conference subsidy
Gerstel Gmbh & Co. KG
Kaj Petersen, Mülheim an der Ruhr, Germany
Golden sponsor
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Ionbench
Pieter DeKocker, Joigny, France
JSB
Marko Koenen, Eindhoven, The Netherlands
LC-GC Europe (Advanstar)
Alasdair Matheson, Wrexham, Chester, United Kingdom
Life Time achievement Award
Markes International Ltd.
Gavin Davies, Llantrisant, United Kingdom
Platinum Sponsor
Peak Scientific
Ann McLaren, Renfrewshire, United Kingdom
Exhibitor
Pfizer
Roman Szucs, Sandwich, United Kingdom
Sponsor
Polyintell
Sami Bayoudh, Val-de-Reuil, France
Exhibitor
RIC
Pol Verschelde, Kortrijk, Belgium
Sponsor
Sample Q
Joeri Vercammen, Louvain-la-Neuve, Belgium
Exhibitor
SerCoLab bvba
Frans Thijs, Antwerpen, Belgium
Exhibitor
Shimadzu Europa GmbH
Uta Steeger, Duisburg, Germany
Golden sponsor
Sigma/Aldrich
Frank Michel, Taufkirchen, Germany
Golden sponsor
Waters S.A.S.
Diana Perrier, Saint-Quentin en Yvelines, France
Golden sponsor