Overview of the Compound Semiconductor Materials Committee Activities Compound Semiconductor Materials Standards Committee Charter • To develop standards required for the transfer of compound semiconductor and related materials from supplier to user and for equipment design. These standards exist in support of integrated circuits, microwave devices, and opto-electronic applications. Participating Companies* Global Compound Semiconductor Materials Technical Committee 3M Air Liquide AIST AIXTRON Brewer Science Bridgestone ChemTrace Chunghwa Picture Tubes Climax Molybdenum Cree Dow Corning DuPont Entegris FM Approvals Fraunhofer Freiberger Global Power Device GLOBALFOUNDRIES Green Solar Tech Harbin Institute HCL America Hitachi Infineon Technologies IQE Istituto CNR-IMEM JolyWood Sunwatt Lehighton Electronics LPE spa Nanometrics Norstel Northrop Grumman NOVASiC Novati Technologies Pall Corporation Panasonic Rasa Industries Samsung SemiMap Scientific Shin-Etsu Handotai Showa Denko SiCrystal SOL Corporation SUMCO Corporation Sumika Chemical Sumitomo Suss MicroTec TBEA SunOasis Toshiba Yingli Green Energy Zygo Corporation * Partial List Published Standards [1/2] Doc # Details SEMI M9 Specifications for Polished Monocrystalline Gallium Arsenide Wafers SEMI M15 Polished Wafer Defect Limits Table for Semi-Insulating Gallium Arsenide Wafers SEMI M23 Specification for Polished Monocrystalline Indium Phosphide Wafers SEMI M36 SEMI M37 SEMI M39 SEMI M42 SEMI M46 SEMI M54 Test Method for Measuring Etch Pit Density (EPD) in Low Dislocation Density Gallium Arsenide Wafers Test Method for Measuring Etch Pit Density (EPD) in Low Dislocation Density Indium Phosphide Wafers Test Method for Measuring Resistivity and Hall Coefficient and Determining Hall Mobility in Semi-Insulating GaAs Single Crystals Specification for Compound Semiconductor Epitaxial Wafers Test Method for Measuring Carrier Concentrations in Epitaxial Layer Structures by ECV Profiling Guide for Semi-Insulating (SI) GaAs Material Parameters Published Standards [2/2] Doc # SEMI M55 SEMI M63 SEMI M64 SEMI M65 SEMI M75 SEMI M79 SEMI M81 SEMI M82 SEMI M83 Details Specification for Polished Monocrystalline Silicon Carbide Wafers Guideline: Test Method for Measuring the Al Fraction in AlGaAs on GaAs Substrates by High Resolution X-Ray Diffraction Test Method for the EL2 Deep Donor Concentration in Semi-Insulating (SI) Gallium Arsenide Single Crystals by Infrared Absorption Spectroscopy Specifications for Sapphire Substrates to use for Compound Semiconductor Epitaxial Wafers Specifications for Polished Monocrystalline Gallium Antimonide Wafers Specification for Round 100 mm Polished Monocrystalline Germanium Wafers for Solar Cell Applications Guide to Defects Found in Monocrystalline Silicon Carbide Substrates Test Method for the Carbon Acceptor Concentration in Semi-Insulating Gallium Arsenide Single Crystals by Infrared Absorption Spectroscopy Test Method for Determination of Dislocation Etch Pit Density in Monocrystals of III-V Compound Semiconductors North America Compound Semiconductor Materials Committee Leadership • Committee Co-chairs – Jim Oliver (Northrop Grumman) – Russ Kremer (Freiberger CM USA) Current Committee Structure NA Compound Semiconductor Materials Committee C: Jim Oliver (Northrop Grumman) C: Russ Kremer (Freiberger CM USA) Electrical Properties TF Silicon Carbide TF L: Austin Blew / (Lehighton Electronics) L: Open Gallium Nitride (GaN) TF L: Judy Kronwasser (NOVASiC) M55 5-Year Review TF L: Judy Kronwasser (NOVASiC) Meeting Information • Last meeting – May 21 in conjunction with CS MANTECH 2014 Denver, Colorado, USA • Next meeting – Virtual Meeting via Web meeting and Teleconference • November 2014 Recent Ballot Results Document # Document Title 4979 New Standard: Specification for Round, Polished GaN Wafers 5593 Line Item Revision to SEMI M9.7-0708, Specification for Round 150 mm Diameter Polished Monocrystalline Gallium Arsenide Wafers (Notched) Line Item 1 – Addition of Thickness, center point of 550 um to §4, Physical Requirements Committee Action Failed and returned to the TF for rework Passed committee review. (Superclean) Documents under Development Doc # 4979A Details New Standard: Specification for Polished Monocrystalline C-Plane Gallium Nitride Wafers 5220 New Standard: Test Method for Measuring Vanadium Concentration in Silicon Carbide by Secondary Ion Mass Spectrometry 5593 Line Item Revision to SEMI M9.7-0708, Specification for Round 150 mm Diameter Polished Monocrystalline Gallium Arsenide Wafers (Notched) Task Force Updates [1/5] • Electrical Properties TF / ASTM F1.15 Subcommittee (1/3) – GaN HEMT Mobility Round Robin Update • II-VI Incorporated sent five samples of their 3” Silicon Carbide substrates • Dr. Xiang Ming Pan (IQE-RF) will assist with growing the Epi • Round Robin Work Group – The first round: non-contact / non-destructive measurement on wafers such as GaN on SiC – The second round: wafers will be cleaving into 10 x10 mm with ohmic for measure by Destructive Hall measurements » The round robin needs help in developing procedures for cleaving the wafers and making contacts » Volunteers are welcomed to confirm, test schedules and condition for non-destructive / destructive testing » Please contact the round robin leader, Danh Nguyen at [email protected] or 610-377-5990 Task Force Updates [2/5] • Electrical Properties TF / ASTM F1.15 Subcommittee (2/3) – F1.15 GaN Epitaxial Wafer Reference Material TF • Goal: Develop test methods for evaluating transport properties of GaN epi-layers • The TF was able to obtain wafer samples from Ostendo (formerly TDI, Inc.) and Kyma – Samples from Ostendo are GaN on Sapphire, 2 inch and includes one unintentionally doped n-type and one Si doped – Sample from Kyma is GaN on Sapphire, 3 inch and is unintentionally doped n-type Task Force Updates [3/5] • Electrical Properties TF / ASTM F1.15 Subcommittee (3/3) – F1.15 GaN Epitaxial Wafer Reference Material TF (continued) • Electrical hall testing was performed on the wafer samples obtained – Results of the electrical hall testing on the sample from Kyma will be used in the follow-up GaN round robin measurements – The sample wafers will then be shipped to Danh Nguyen • The TF will carry on with its testing of non-destructive and destructive methods for electrical, optical and microstructural on the samples obtained – electrical: Eddy-current; Hall; C-V, CTLM; – optical: PL, CL, Raman; – microstructural: TEM, XRD Task Force Updates [4/5] • SEMI M55 (Polished Monocrystalline Silicon Carbide Wafers) Five-Year Review TF – The TF will await further word regarding the IP review of SEMI M55 from Arnd Weber (SiCrystal) • Silicon Carbide (SiC) TF – The TF is still looking for a TF leader – The TF deferred to the EU Silicon Carbide TF where most of the SiC activities have been occurring • The EU Silicon Carbide TF reviewed Intellectual Property (IP) for the SiC 100 mm and SiC 150 mm documents • Document 5370 (Revision to add a subordinate standard to SEMI M55, 150 mm SiC Wafer Specification) pending publication. • Document 3784E (100 mm SiC Wafer Specification) is currently being drafted and will be balloted in Cycle 4-2014. Task Force Updates [5/5] • Gallium Nitride (GaN) TF – Document 4979, (Polished Monocrystalline GaN Wafers) • The document was failed by the committee after receiving useful feedback and comments from voters. • The TF will continue to improve the document based on feedback received from the voters. – The TF will reballot the document as 4979A sometime in 2014 before the next meeting in November 2014. Thank You! For more information or to participate in any NA CSM activities, please contact Michael Tran ([email protected]) Europe Compound Semiconductor Materials Committee Leadership • Committee Co-chair – Arnd Weber; SiCrystal, Germany • 2nd Co-chair position vacant – Looking for a 2nd co-chair Meeting Information • Last meeting • • • Nuremburg, Germany April 10th, 2014 Next meeting • To be decided ECS Committee Structure & Leaders Compound Semiconductor Materials Committee Co-Chair: Arnd Weber - SiCrystal 5-year review TF L: Hans-Christian Alt / HM New Silicon Carbide TF L: Arnd Weber - SiCrystal Contactless Resistivity and Mobility Mapping TF L: Wolfgang Jantz - Semimap Global SiC Task Force • Leader: Arnd-Dietrich Weber, SiCrystal • Rationale: Create a basic standard for SiC wafer material and a specification for 2” ,3”, 100mm and 150mm SiC wafers • Status: 100mm wafers (document 3784E) Relaunch of technical work completed Approved for Ballot Cycle 4 in 2014 • SiC 150mm wafer standard (Document 5370): Committee approval of superclean ballot review. -> Publication in progress. Contactless Capacitive Resistivity Measurement of SI-Semiconductors TF • Leader: Wolfgang Jantz, Semimap • Rationale : Create a standard for Capacitive Measurements (separate from NA TF addressing resistivity measurements in general; transfer and upgrading of DIN50448 ) Members of TF : U. Kretzer/FCM, H.-Ch.. Alt/FH München Invitation to Hitachi Cable and J. Oliver/Northrop Grumman • Ballot 5075 (reapproval of M54 s.i. GaAs material parameters) passed • Reapproved SNARF/TFOF (procedural issue) • Work on a draft is ongoing, preparation of round robin New: 5-year Review TF • Leader: Hans-Christian Alt, FHM Rationale: perform 5-year review of GaAs related documents: SEMI M46, SEMI M63, SEMI M64 • New SNARFS: – SEMI M46: Guideline: test method for measuring the al fraction in AlGaAs on GaAs substrates by high resolution x-ray diffraction – SEMI M63: test method for measuring carrier concentrations in epitaxial layer structures by ecv profiling – SEMI M64: test method for the El2 deep donor concentration in semi-insulating (Si) gallium arsenide single crystals by infrared absorption spectroscopy Recently Issued Ballot Cycle 4-2014 Document # 3874E Document Title Committee Action Specification for 100 mm round polished mono SiC Material and Wafer crystalline 4H and 6H silicon carbide wafers to SEMI Specification M55-0308 Ballot Results • Ballot 5370: Specification for 150mm Silicon Carbide single-crystalline substrates – Ballot passed committee review • Return Percentage: 60.29% • Accept percentage: 100% – Ballot is awaiting further review by the Audits & Review Subcommittee. Thank You! For more information or to participate in any Europe CSM activities, please contact Andrea Busch ([email protected]) Japan Compound Semiconductor Materials Committee General Information • Leadership – Co-chairs • Masayoshi Obara/ Shin-Etsu Handotai Co., Ltd. – Compound Semiconductor Materials committee representative to the JRSC – GCS voting member • OPEN • Meeting – No TC meeting for long time Compound Semiconductor Materials Committee Organization Japan Compound Semiconductor Materials Committee Masayoshi Obara / SEH TBD International SiC TF Taizo Hoshino/ Nippon Steel 5 year Review TF Leader: Open Sapphire Substrate TF Toshiro Kotaki/ Namiki Precision Jewel Global 200mm GaAs Specification TF Leader: Open Current Status • No activity. However, the committee is interested in the activity related to the sapphire wafer specification under HB LED TC. • Need to discuss whether or not the following task forces disband or energize – Global 200mm GaAs Wafer Specification TF – Five-year Review TF Thank you! For more information, please contact: Junko Collins, SEMI Japan [email protected] Get Involved! • Get your company support • Register today: www.semi.org/standardsmembership • SEMI Standards Technical Committees Assembly & Packaging Automated Test Equipment Compound Semiconductor Mat’ls Environmental Health & Safety Facilities FPD Materials & Components FPD Metrology Gases High-Brightness LED Information & Control Liquid Chemicals MEMS / NEMS Metrics Micropatterning Photovoltaic Photovoltaic Automation Photovoltaic Materials Physical Interfaces & Carriers Silicon Wafer Traceability 3DS-IC (three-dimensional stacked integrated circuits) Staff Contacts Global Compound Semiconductor Materials Committee North America Michael Tran 408.943.7019 [email protected] Japan Junko Collins 81.3.3222.5819 [email protected] Europe Andrea Busch 33.4.3878.9652 [email protected]
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