ﻫﻴﺌﺔ ﺍﻝﺘﻘﻴﻴﺱ ﻝﺩﻭل ﻤﺠﻠﺱ ﺍﻝﺘﻌﺎﻭﻥ ﻝﺩﻭل ﺍﻝﺨﻠﻴﺞ ﺍﻝﻌﺭﺒﻴﺔ GCC STANDARDIZATION ORGANIZATION (GSO) GSO ISO 7837:2009 (E) ISO 7837:1992 ﺘﻘﺩﻴﺭ ﺤﺠﻡ ﺍﻝﻜﺜﺎﻓﺔ )ﺍﻝﺤﺭﺓ( ﻝﺤﺒﻴﺒﺎﺕ ﺍﻷﺴﻤﺩﺓ-ﺍﻷﺴﻤﺩﺓ Fertilizers - Determination of bulk density (loose) of fine-grained fertilizers ICS : 65.080 Fertilizers - Determination of bulk density (loose) of fine-grained fertilizers Date of GSO Technical Council : 28-29/10/1430 h(17-18/10/2009) : Standard Issuing Status GSO STANDARD GSO ISO 7837:2009 ﺘﻘـﺩﻴـﻡ ﻫﻴﺌﺔ ﺍﻝﺘﻘﻴﻴﺱ ﻝﺩﻭل ﻤﺠﻠﺱ ﺍﻝﺘﻌﺎﻭﻥ ﻝﺩﻭل ﺍﻝﺨﻠﻴﺞ ﺍﻝﻌﺭﺒﻴﺔ ﻫﻴﺌﺔ ﺇﻗﻠﻴﻤﻴﺔ ﺘﻀﻡ ﻓـﻲ ﻋـﻀﻭﻴﺘﻬﺎ ﺍﻷﺠﻬـﺯﺓ ﻭﻤﻥ ﻤﻬﺎﻡ ﺍﻝﻬﻴﺌﺔ ﺇﻋﺩﺍﺩ ﺍﻝﻤﻭﺍﺼﻔﺎﺕ ﺍﻝﻘﻴﺎﺴـﻴﺔ، ﺍﻝﻭﻁﻨﻴﺔ ﻝﻠﻤﻭﺍﺼﻔﺎﺕ ﻭﺍﻝﻤﻘﺎﻴﻴﺱ ﻓﻲ ﺩﻭل ﺍﻝﺨﻠﻴﺞ ﺍﻝﻌﺭﺒﻴﺔ . ﻭﺍﻝﻠﻭﺍﺌﺢ ﺍﻝﻔﻨﻴﺔ ﺍﻝﺨﻠﻴﺠﻴﺔ ﺒﻭﺍﺴﻁﺔ ﻝﺠﺎﻥ ﻓﻨﻴﺔ ﻤﺘﺨﺼﺼﺔ ﻭﻗﺩ ﻗﺎﻤﺕ ﻫﻴﺌﺔ ﺍﻝﺘﻘﻴﻴﺱ ﻝﺩﻭل ﻤﺠﻠﺱ ﺍﻝﺘﻌﺎﻭﻥ ﻝﺩﻭل ﺍﻝﺨﻠﻴﺞ ﺍﻝﻌﺭﺒﻴﺔ ﻀﻤﻥ ﺒﺭﻨﺎﻤﺞ ﻋﻤل ﺍﻝﻠﺠﻨـﺔ ﺍﻝﻔﻨﻴـﺔ ( " ﻗﻁﺎﻉ ﻤﻭﺍﺼﻔﺎﺕ ﺍﻝﻤﻨﺘﺠﺎﺕ ﺍﻝﻜﻴﻤﺎﺌﻴﺔ ﻭﺍﻝﻐﺯل ﻭﺍﻝﻨﺴﻴﺞ " ﺒﺘﺒﻨﻲ ﺍﻝﻤﻭﺍﺼﻔﺔ ﺍﻝﻘﻴﺎﺴﻴﺔ ﺍﻝﺩﻭﻝﻴـﺔ1 ) ﺭﻗـﻡ ﺘﻘﺩﻴﺭ ﺤﺠﻡ ﺍﻝﻜﺜﺎﻓﺔ )ﺍﻝﺤﺭﺓ( ﻝﺤﺒﻴﺒﺎﺕ ﺍﻷﺴﻤﺩﺓ" ﻭﺍﻝﺘﻲ ﺃﺼـﺩﺭﺘﻬﺎ- "ﺍﻷﺴﻤﺩﺓISO 7837:1992 ﺭﻗـﻡ ﻭﻗﺎﻤﺕ ﺍﻹﻤﺎﺭﺍﺕ ﺍﻝﻌﺭﺒﻴﺔ ﺍﻝﻤﺘﺤﺩﺓ ﺒﺈﻋﺩﺍﺩ ﻤﺸﺭﻭﻉ ﻫﺫﻩ، "ﺍﻝﻤﻨﻅﻤﺔ ﺍﻝﺩﻭﻝﻴﺔ ﻝﻠﺘﻘﻴﻴﺱ" ﻭﺫﻝﻙ ﺒﻠﻐﺘﻬﺎ ﺍﻷﺼﻠﻴﺔ . ﺍﻝﻤﻭﺍﺼﻔﺔ ﻭﻗﺩ ﺍﻋﺘﻤﺩﺕ ﻫﺫﻩ ﺍﻝﻤﻭﺍﺼﻔﺔ ﻜﻤﻭﺍﺼﻔﺔ ﻗﻴﺎﺴﻴﺔ ﺨﻠﻴﺠﻴﺔ ﺩﻭﻥ ﺇﺩﺨﺎل ﺃﻴﺔ ﺘﻌﺩﻴﻼﺕ ﻓﻨﻴﺔ ﻋﻠﻴﻬﺎ ﻭﺫﻝـﻙ ﻓـﻲ . (2009/10/18-17) هـ1430/10/29-28 ﺍﻝﺫﻱ ﻋﻘﺩ ﺒﺘﺎﺭﻴﺦ، (18) ﺍﺠﺘﻤﺎﻉ ﺍﻝﻤﺠﻠﺱ ﺍﻝﻔﻨﻲ ﺭﻗﻡ Foreword GCC Standardization Organization (GSO) is a regional Organization which consists of the National Standards Bodies of GCC member States. One of GSO main functions is to issue Gulf Standards /Technical regulations through specialized technical committees (TCs). GSO through the technical program of committee TC No.(1) "Chemical and Textiles Products Sector TC" has adopted the International Standard No. ISO 7837:1992 "Fertilizers - Determination of bulk density (loose) of fine-grained fertilizers" issued by (International Organization for Standardization) in its original language. The Draft Standard has been prepared by United Arab Emirates . This standard has been approved as a Gulf Standard without any technical modifications by GSO Technical Council in its meeting No. (18) , held on 28-29/10/1430h (17-18/10/2009) . 1 INTERNATIONAL STANDARD Second edition 1992-07-0 1 FerMizers - Determination of bulk density (loose) of fine-grained fertilizers Engrais engrais - D6termination fins de la masse vohiique tassement Reference number ISO 7837: 1992(E) ISO 7837:1992(E) Fareward ISO (the International Organization for Standardization) is a worldwide federation of national Standards bodies (ISO member bodies). The work of preparing International Standards is normally carried out through ISO technical committees. Esch member body interested in a subject for which a technical committee has been established has the right to be represented on that committee. International organizations, governmental and non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization. Draft International Standards adopted by the technical committees are circulated to the member bodies for voting. Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote. International Standard ISO/TC 134, Fertilizers Physical ISO 7837 was prepared and seil conditioners, by Technical Committee Sub-Committee SC 3, properties. This second edition cancels and replaces the (ISO 7837:1983), which has been technically revised. 0 ISO 1992 All rights reserved. NO part of this publication may be reproduced or by any means, electronie or mechanical, including photocopying permission in writing from the publisher. International Organization for Standardization Gase Postale 56 + CH-1211 Geneve 20 l Switzerland Printed in Switzerland ii first edition or utilized in any form and microfilm, without ISO 7837:1992(E) lntroductian A method for the determination of the bulk density (loose) of solid fertilizers having particle sizes within the frequently encountered range from about 0,5 mm to 5 mm is specified in ISO 3944:1992, Fertilizers - Determination of bulk density (Moose). This method is not, however, suitable for fine-grained fertilizers having a large proportion of particles of diameters less than 0,5 mm. Such fertilizers pass with difficulty, in most cases, from the specified funnel into the measuring cylinder, generally Cause considerable dust nuisance, and are inclined to form hollow spaces (air cavities) within their bulk volume. The bulk density values obtained are, thus, too low. In the case of fine-grained fertilizers, dust-tight, non-clogging apparatus, cylinder. therefore, it is necessary to use a with a relatively wide measuring ... Ill INTERNATIONAL Fertilizers fine-grained 1 STANDARD - ISO 7837:1992(E) Determination fertilizers, of bulk density Scope 3 This International Standard specifies a method for the determination of the bulk density ( oose) of solid fine-grained fertilizers. The method is applicable to fertilizers Nhich contain a large proportion of particles of diameters less than 0,5 117113. For fertilizers which contain a large proportion NOTE 1 of particles of diameters within the range from 0,5 mm to 5 mm, a method is specified in ISO 3944. The method is applicabie to dry fertilizers only. If the fertilizer has absorbed moisture during transport or storage, it is necessaty to dry it in an environmental chamber, with constant low humidity, Prior to the determination. Definition references Solid fertilizers - Reduction of sam- ples. ISO 8358:1991, Solid samples for chemical the The bulk density (IooseJ is expressed cubic centimetre (g/cm ). 4 in grams per Principle Pouring of the fertilizer from a specified filling device into a specified measuring cylinder of known volume and weighing of the contents of the cylinder. Apparatus capable of weighing to the nearest 5.2 Apparatus for determination of bulk density (loose), having the approximate dimensions given in figure 1 and consisting of the following. The following Standards contain provisions which, through reference in this text, constitute provisions of this International Standard. At the time of publication, the editions indicated were valid. All standards are subject to revision, and Parties to agreements based on this International Standard are encouraged to investigate the possibility of applying the most recent editions of the Standards indicated below. Members of IEC and ISO maintain registers of currently valid International Standards. ISO 7742:1988, Standard, 3.1 bulk density (loose) of a fertilizer: The mass per volume of a material after it has been tipped freely into a Container under specified conditions. 5.1 Balance, 1 Cl* Normative of For the purposes of this International following definition applies. 5 2 (loose) ferfilizers and physical - Reparation analysis. 5.2.1 Filling device (4) with spring-suspended lockm lever (5), for holding or loosening the hinged cover. The hinged cover is opened by manipulating the lever so that the contents of the filling device discharge into the measuring cylinder. ing CAUTION - lt is important that those Parts of the apparatus which are in contact with the fertilizer are made of corrosion-resistant material (glass, plastics, etc.). cylinder 5.2.2 Measuring 1 000 cm3 + 5 cm3. - (1) 3 of capacity of 5.2.3 lntermediate piece (2) with hinged cover (3). 1 l ISO 7837:1992(E) 5.3 Spatula, other suitable 6 approximateiy scraper. Preparation 200 mm x 20 mm, or P=T of test Sample Prepare the test Sample by the methods given in ISO 7742 and ISO 8358, ensuring that the Sample is sufficient to carry out two separate determinations. 7 m m is the mass, in grams, of the test Portion; V is the volume up to the brim, in cubic centimetres, of the measuring cylinder. Take as the resuit the arithmetic mean of the two determinations provided that the requirement for repeatability (see 8.2) is satisfied. Procedure Pour the fertiiizer into the filiing device (5.2.1) up to the brim. Open the hinged cover by manipuiating the iocking lever. After 2 min, remove the empty fiiiing device and the intermediate piece (5.2.3) from the measuring cylinder (5.2.2). Scrape away the Surplus fertilizer from the measuring cylinder using the spatula or other suitabie tool (5.3). Weigh the contents of the measuring nearest 1 g. cyiinder to the 8.2 Repeatability The differente between the results of two determinations, carried out in rapid succession by the Same Operator using the Same apparatus, shall not exceed 0,02 g/cm3. 9 Test report i The test report shaii inciude lars: the following Carry out two determinations, in rapid succession, on separate test portions taken from the Same test Sample. a) identification 8 c) the resuit and the method of expression; Expression of results b) reference particu- of the Sample; to the method used; d) any un usuai features noted during the determi8.1 Method of calculation The buik density (loose), ~3,of the fertiiizer, in grams per cubic centimetre, is given by the equation 2 nation; e) any Operation not included in this International Standard or regarded as optional. t i l ISO 7837:1992(E) b) Open posltlon a) Closed posftlon 1 Measurlng cyllnder lnternal dIameter Internal helght dl- 87mm*lmm hi correspondlng to a capaclty of 1000 cm3 * 5 cm3 2 Intermedla te plece Internat dlameter helght dz= 87mm*lmm =l35mm*lmm .h2 3 Hlnged cover 4 Ftlling devtce Lower lnternal dlameter upper Internal dlameter helght 5 Sprlng-suspended Figure 1 - Apparatus d3= 79 mm * ‘l mm dr= 99mm*lmm h,=l99mm*lmm locklng lever for determination of bulk density (loose) of fine-grained ferMizers 3 ISO 7837:1992(E) -------------- UDC 631.8:531.755.22 Descriptors: fertilizers, Price based on 3 pages fines, tests, determination, bulk density, density measurement.
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