Eurofins WEJ Contaminants GmbH Neuländer Kamp 1 D-21079 Hamburg GERMANY Tel: +49 40 49294 2222 Fax: +49 40 49294 2000 Eurofins WEJ Contaminants · Neuländer Kamp 1 · D-21079 Hamburg Valeo Laboratories GmbH attn. Frau Ilonka Paul Zum Westblick 19 25770 Lieth [email protected] www.eurofins.de/wej-contaminants-en - 2902 Person in charge Mrs. S. Maß Mrs. S. Maß - 2902 Client support {235D35B8-0A5B-4CEE-857C-6781FC1EC50D} Report date 06.05.2014 Page 1/3 Analytical report: AR-14-JC-050151-03 This report will replace report number: AR-14-JC-050151-02 Sample Code 706-2014-00146269 Reference Number Amount Reception temperature Ordered by Submitted by Sender Reception date time Packaging Start/end of analyses ÌAR-14-JC-Ç%!SÈ-03\Î 6mg Nicotin 1 1081 g room temperature Frau Ilonka Paul Frau Ilonka Paul DHL 17.04.2014 plastic can with screw closure 19.04.2014 / 06.05.2014 TEST RESULTS ParamMark:(5518751,1224) ParamMark:(5518749,1224) ParamMark:(5518750,1224) ParamMark:(5518752,1224) ParamMark:(5518754,1224) ParamMark:(5518753,1224) ParamMark:(5518761,1224) Physical-chemical Analysis J1001 Sample preparation (#) Method: §64 LFGB L 00.00-19/1, microwave digestion by pressure J8306 Lead (Pb) (#) Method: EN 15763:2009, ICP-MS Lead (Pb) J8308 Cadmium (Cd) (#) Method: EN 15763:2009, ICP-MS Cadmium (Cd) J8312 Arsenic (As) (#) Method: EN 15763:2009, ICP-MS Arsenic (As) JJW2B Copper (Cu) (#) Method: DIN EN ISO 17294-2-E29, ICP-MS Copper (Cu) JJ0CG Chromium (Cr) (#) Method: DIN EN ISO 17294-2-E29, ICP-MS Chromium (Cr) JJ0CM Nickel (Ni) (#) Method: DIN EN ISO 17294-2-E29, ICP-MS Nickel (Ni) JJ0CI Manganese (Mn) (#) Method: DIN EN ISO 17294-2-E29, ICP-MS Manganese (Mn) The results of examination refer exclusively to the checked samples. Duplicates - even in parts - must be authorized by the test laboratory in written form. Eurofins WEJ Contaminants GmbH · Neuländer Kamp 1 · D-21079 Hamburg Place of execution and place of jurisdiction is Hamburg - lower district court Hamburg HRB 106641 General Managers: Dr. Markus Brandmeier, Dr. Robert Gatermann Registered representatives (Prokuristen): Dr. Scarlett Biselli, Dr. Katrin Hoenicke, Dr. Claudia Schulz VAT No.: DE263765651 Nord/LB (BLZ 250 500 00) Konto-Nr. 199 895 004 SWIFT-BIC NOLADE2HXXX IBAN DE 7425 0500 0001 9989 5004 Our General Terms & Conditions, available upon request and online at http://www.eurofins.de/lebensmittel/kontakt/avb.aspx, shall apply. DetailMark:(5518751,1224) MethodMark:(5518751,1224) <0.05 * mg/kg DetailMark:(5518749,1224) MethodMark:(5518749,1224) <0.01 * mg/kg DetailMark:(5518750,1224) MethodMark:(5518750,1224) <0.1 * mg/kg DetailMark:(5518752,1224) MethodMark:(5518752,1224) <0.1 * mg/kg DetailMark:(5518754,1224) MethodMark:(5518754,1224) <0.1 * mg/kg DetailMark:(5518753,1224) MethodMark:(5518753,1224) <0.1 * mg/kg DetailMark:(5518761,1224) MethodMark:(5518761,1224) <0.1 * mg/kg Durch die DAkkS Deutsche Akkreditierungsstelle GmbH akkreditiertes Prüflaboratorium DIN EN ISO/IEC 17025:2005 Die Akkreditierung gilt nur für die in der Urkunde aufgeführten Prüfverfahren. Page 2/3 Analytical report: AR-14-JC-050151-03 Sample Code 706-2014-00146269 This report will replace report number: AR-14-JC-050151-02 ParamMark:(5518759,1224) ParamMark:(5518762,1224) ParamMark:(5518790,1224) ParamMark:(5518779,1224) ParamMark:(5518780,1224) ParamMark:(5518781,1224) ParamMark:(5518782,1224) ParamMark:(5518783,1224) ParamMark:(5518767,1224) ParamMark:(5518769,1224) ParamMark:(5518770,1224) ParamMark:(5518771,1224) ParamMark:(5518785,1224) ParamMark:(5518773,1224) ParamMark:(5518775,1224) ParamMark:(5518774,1224) ParamMark:(5518776,1224) ParamMark:(5518786,1224) ParamMark:(5518788,1224) ParamMark:(5518789,1224) ParamMark:(5518787,1224) ParamMark:(5518768,1224) ParamMark:(5518784,1224) ParamMark:(5518765,1224) ParamMark:(5518772,1224) ParamMark:(5518758,1224) ParamMark:(5518777,1224) ParamMark:(5518778,1224) ParamMark:(5518766,1224) ParamMark:(5518764,1224) JJ0CX Antimony (Sb) (#) Method: DIN EN ISO 17294-2-E29, ICP-MS Antimony (Sb) JJ0CK Cobalt (Co) (#) Method: DIN EN ISO 17294-2-E29, ICP-MS Cobalt (Co) JCP00 Preparation PAH (Saponification) (#) Method: Internal method, Saponification JC022 PAH acc. to EPA+EU (#) Method: Internal method, GC-MS Fluorene Phenanthrene Anthracene Fluoranthene Pyrene Benzo(a)anthracene Chrysene Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo-(j)-fluoranthen Benzo(a)pyrene Indeno(1,2,3-cd)pyrene Dibenzo(a,h)anthracene Benzo(ghi)perylene Dibenzo(a,l)pyrene Dibenzo(a,i)pyrene Dibenzo(a,h)pyrene Dibenzo(a,e)pyrene Cyclopenta(c,d)pyrene 5-Methylchrysene Benzo-(c)-fluorene Benzo(e)pyrene Perylene Anthanthrene Coronen Benzo(b)naphtho(2,1-d)thiophene Sum PAH 4 Sum of all positive identified PAH FIN2U Diethylenglycol Method: GC-FID DetailMark:(5518759,1224) MethodMark:(5518759,1224) <0.1 * mg/kg DetailMark:(5518762,1224) MethodMark:(5518762,1224) <0.1 * mg/kg DetailMark:(5518760,1224) MethodMark:(5518760,1224) DetailMark:(5518790,1224) MethodMark:(5518790,1224) 8.2 3.5 2.6 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Inapplicable 14 * * * * * * * * * * * * * * * * * * * * * * * µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg DetailMark:(5518763,1224) MethodMark:(5518763,1224) MethodMark:(5518763,1224) Subcontracted to a Eurofins laboratory ParamMark:(5518763,1224) Diethyleneglycol <20 * mg/kg Microbiological Analysis UMUD8 Aerobic Plate Count 30°C <10 >3000 /g 1 (1) PCA Agar-P-30 ISO 4833-M Method: ISO 4833-1, Microbiological Aerobic Plate Count 30°C < 10 cfu/g UMUDN Aerobic Plate Count 30°C <100 >100000000 /g 2 (1;3) PCA Agar-W-30 ISO 4833-M Method: ISO 4833-2, Microbiological Aerobic Plate Count 30°C < 100 cfu/g UMULU Escherichia Coli <100 >100000000 /g 2 (1;3) TBX Agar-W-44 ISO 16649-2-M The results of examination refer exclusively to the checked samples. Duplicates - even in parts - must be authorized by the test laboratory in written form. Eurofins WEJ Contaminants GmbH · Neuländer Kamp 1 · D-21079 Hamburg Place of execution and place of jurisdiction is Hamburg - lower district court Hamburg HRB 106641 General Managers: Dr. Markus Brandmeier, Dr. Robert Gatermann Registered representatives (Prokuristen): Dr. Scarlett Biselli, Dr. Katrin Hoenicke, Dr. Claudia Schulz VAT No.: DE263765651 Nord/LB (BLZ 250 500 00) Konto-Nr. 199 895 004 SWIFT-BIC NOLADE2HXXX IBAN DE 7425 0500 0001 9989 5004 Our General Terms & Conditions, available upon request and online at http://www.eurofins.de/lebensmittel/kontakt/avb.aspx, shall apply. MethodMark:(5518757,1224) DetailMark:(5518755,1224) MethodMark:(5518755,1224) MethodMark:(5518755,1224) Subcontracted to a Eurofins laboratory accredited for this test. ParamMark:(5518755,1224) DetailMark:(5518757,1224) MethodMark:(5518757,1224) Subcontracted to a Eurofins laboratory accredited for this test. ParamMark:(5518757,1224) GroupMark:(5518757,1224) DetailMark:(5518756,1224) Durch die DAkkS Deutsche Akkreditierungsstelle GmbH akkreditiertes Prüflaboratorium DIN EN ISO/IEC 17025:2005 Die Akkreditierung gilt nur für die in der Urkunde aufgeführten Prüfverfahren. Page 3/3 Analytical report: AR-14-JC-050151-03 Sample Code 706-2014-00146269 This report will replace report number: AR-14-JC-050151-02 Method: MethodMark:(5518756,1224) ISO 16649-2-M, Microbiological MethodMark:(5518756,1224) Subcontracted to a Eurofins laboratory accredited for this test. ParamMark:(5518756,1224) Escherichia coli < 100 cfu/g UMUMW Coagulase positive Staphylococcus E <100 >100000000 /g (1;3) BP Agar-W ISO 6888-1-M Method: ISO 6888-1-M, Microbiological Coagulase positive staphylococcus < 100 cfu/g UM0FQ Presumptive Bacillus Cereus <100 >15000000 /g 4 (1-4) MYP Agar-S-30 ISO 7932 Method: ISO 7932, Microbiological Presumptive Bacillus cereus DetailMark:(5518793,1224) MethodMark:(5518793,1224) MethodMark:(5518793,1224) Subcontracted to a Eurofins laboratory accredited for this test. ParamMark:(5518793,1224) MethodMark:(5518792,1224) MethodMark:(5518792,1224) Subcontracted to a Eurofins laboratory accredited for this test. ParamMark:(5518792,1224) DetailMark:(5518792,1224) < 100 cfu/g * = Below indicated quantification level (#) = Eurofins WEJ Contaminants GmbH (Hamburg) is accredited for this test. SignatureMark:(5518793,1224) Signature The results of examination refer exclusively to the checked samples. Duplicates - even in parts - must be authorized by the test laboratory in written form. Eurofins WEJ Contaminants GmbH · Neuländer Kamp 1 · D-21079 Hamburg Place of execution and place of jurisdiction is Hamburg - lower district court Hamburg HRB 106641 General Managers: Dr. Markus Brandmeier, Dr. Robert Gatermann Registered representatives (Prokuristen): Dr. Scarlett Biselli, Dr. Katrin Hoenicke, Dr. Claudia Schulz VAT No.: DE263765651 Nord/LB (BLZ 250 500 00) Konto-Nr. 199 895 004 SWIFT-BIC NOLADE2HXXX IBAN DE 7425 0500 0001 9989 5004 Our General Terms & Conditions, available upon request and online at http://www.eurofins.de/lebensmittel/kontakt/avb.aspx, shall apply. Durch die DAkkS Deutsche Akkreditierungsstelle GmbH akkreditiertes Prüflaboratorium DIN EN ISO/IEC 17025:2005 Die Akkreditierung gilt nur für die in der Urkunde aufgeführten Prüfverfahren.
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