Public Technical Course 1, July 1-2, 2014, Graz, Austria Introduction to the numerical modeling and experimental characterization of porous materials Pr Noureddine Atalla Université de Sherbrooke www.gaus.ca [email protected] References Extended version of this talk and more info about the topic can be found in : • ASME/NCAD workshop : http://files.asme.org/Divisions/NCAD/33112.pdf • Winter school on the Acoustics of Poro-Visco-Elastic Media. Lyon, 12-14 Feb. 2014 ([email protected]) • Allard & Atalla: Propagation of Sound in Porous Media. 2nd Edition, Wiley, 2009 2 Objectives 1. Define sound absorbing materials an their classes 2. Review models of porous materials and methods to measure their input parameters 3. Introduce Transfer Matrix Method based models to simulate the vibration and acoustic response of sound packages 3 4 Outline Sound packages and porous materials Modeling porous materials Experimental characterization of porous materials Transfer Matrix Method based modeling methodology Conclusion 6 Sound packages ? Sound packages are made up from a combination of materials, notably: Porous materials Foams Fibers Felts Carpets Porous films Fabrics Damping materials Limp and elastic (solid) layers 7 Porous materials and their characteristics Porous materials Two phases : solid and fluid Elastic coupling Visco-inertial coupling Fiberglass Urethane What do they do ? The behavior of porous materials depends on their nature, loads and the coupled Transform acoustic energy into heat structures. The selection of a model/methodology should account for this fact How do they dissipate energy ? viscous effect thermal effect structural damping Melamine Double porosity 8 What about their performance? 9 What about their performance? Typical diffuse field results 10 What about their performance? Typical normal incidence results 11 What about their frame ? Elastic frame Rigid frame Limp frame 12 Types of porous materials Glass wool / glass fiber Granular Woven fabrics Felt Rigid Elastic polymeric foams Recycled Perforated Perforated plates Non woven Scims & screens Multilayer / Laminates 13 Outline Objectives Sound packages and porous materials Modeling porous materials Experimental characterization of porous materials Transfer Matrix Method based modeling methodology Conclusion 14 Modeling Porous materials Mechanical model (Equivalent mechanical systems) The membrane mass K=Stiffness of the foam/Fiber c = Kinetic viscous coefficient between moving frame and air Admittance model Example Delaney and Basley model for fibrous materials, …) 0.754 0.732 ρ f ρ f ZC ρ0C0 1 0.0571 0 j 0.087 0 , σ σ ρ f k 1 0.0978 0 C0 σ 0.700 ρ f j 0.189 0 σ 0.595 , Microstructural models (Biot) Rigid/limp frame (Classical codes; …) P j ~o P 0 n Zn Empirical models (limited to certain type of materials and can be inaccurate; D&B, Miki, … (Equivalent fluid models) = Rigide Flexible Elastic frame. Coupled poroelastic models 15 Modeling of porous materials They are modeled at a homogeneous macroscopic scale Elastic or acoustic wave Macroscopic scale H1 h << << 1 HH1 H 1<< 2H << ux h uz H1 Poroelastic material Ux Macroscopic element uy Homogeneous solid phase 2 Uz Uy Homogeneous fluid phase 16 16 Biot based models Example: BIOT (u,p) formulation governs the propagation of the coupled elastic waves (compression and shear) and acoustic wave (compression). Biot's macroscopic parameters 2ρ ~ u γ~ p, ~u λ~ μ ~ u μ ω s i i,jj i j,ij 1 1 p,ii ~ p γ~ u i,i ~ Kf ω2ρ f Elasto-dynamic equation Helmholtz equation u : solid phase macroscopic displacement vectors p : fluid phase macroscopic pressure ~: denotes a complex and frequency dependent quantity (Dynamic properties) , : Effective solid phase Lamé coefficients Kf : Effective fluid phase bulk modulus s : Effective solid phase density f : Effective fluid phase density : Fluid-solid coupling coefficient Ref.: Allard & Atalla: Propagation of Sound in Porous Media. 2nd Edition, Wiley, 2009 17 Equivalent fluid model Rigid frame (Limit of Biot’s model when frame is motionless) Helmholtz equation with equivalent density and bulk modulus p 2 eq p0 K eq Limp frame (Limit of Biot’s model when frame is limp) Helmholtz equation with equivalent density and bulk modulus e,l p p0 K 2 e e M 02 e,l M e 20 M 1 0 Total apparent mass of the bulk volume Ref.: http://dx.doi.org/10.1121/1.2800895 Panneton: Comments on the limp frame equivalent fluid model for porous media, J. Acoust. Soc. Am. 122 (2007) 18 Equivalent fluid model Equivalent dynamic density • Takes into account viscous and inertial effects • Some recent models: • Johnson et al. (1987) - , , , • Pride et al. (1993) - , , , , 0 e EQ K e K EQ Equivalent dynamic bulk modulus • Takes into account thermal effects • Some recent models: • Champoux and Allard (1991) - , • Lafarge I (1993,1997) - , , k0 • Lafarge II (1993) - , , k0, 0 JCA model JL model Macroscopic parameters - Open porosity - Tortuosity - Static airflow resistivity - Viscous characteristic length 0 - Static viscous tortuosity k0 - Static thermal permeability - Thermal characteristic length 0 - Static thermal tortuosity 19 Input Parameters for the Biot model The Biot-Allard model: 9 parameters Source: GUI from Nova software 20 20 Bulk density [1] Following the Biot theory, the bulk density is the ratio between the in-vacuum mass of the porous aggregate and its bulk volume. M 1 Vt M 1 2 r h r h 21 Open Porosity [] Open porosity is defined as the fraction of the interconnected pore fluid volume to the total bulk volume of the porous aggregate. Vf Vt Vs 1 1 1 s Vt Typical values For perforates : < 50% For light fibrous: ~ 99% For foams: > 90% Vs : Solid phase volume s : Density of solid phase material 22 Static airflow resistivity [] Static airflow resistivity governs the low-frequency viscous effects in open-cell porous media, where the viscous skin depth is of the order of magnitude of the characteristic size of the cells. It is defined as the limit, when flow tends to zero, of the quotient of the air pressure difference across a specimen divided by its thickness and the velocity of airflow through it. P A Q h [Ns/m4 or MKS Rayls/m] P 23 Tortuosity [] Tortuosity accounts for the apparent increase in the fluid density when the fluid saturates a porous structure. It can be seen as the effective length of the path follows by acoustical wave through the material. L L 1 2 Typical values - Low density fibrous: = 1.00 - Mid/High density fibrous: 1.00 1.45 - Reticulated foams: 1.00 2.0 - Partially reticulated foams : 2.0 3.0 24 Thermal characteristic length [] The thermal characteristic length describes the thermal dissipation effects at medium and high frequencies. It is of the order of magnitude of the average radius of the larger cells where thermal losses dominate viscous losses. 2 V dV f dS Vf : Pore volume : Wet surface boundary Typical values From 10 µm to 500 µm 25 Viscous characteristic length [] The viscous characteristic length describes the viscous dissipation effects at medium and high frequencies. It is of the order of magnitude of the average radius of the smaller cells and necks where viscous losses dominate thermal losses. 2 v dV 2 Vf v dS 2 Vf : Pore volume : Wet surface boundary Typical values From 10 µm to 500 µm 26 Microstructure based models Alternative models microstructure based: needed to optimize foam’s fabrication process to target specific vibroacoustic applications (dash insulator, floor insulator,…) link micro/macro for polyurethane foams Chemists Fabrication Microstructure cell size,… Acousticians Non-Acoustic properties porosity, tortuosity,… Acoustic behavior absorption, transmission,… 27 Microstructure based models An example: semi-empirical model* Fabricatio n Microstructure cell size,reticulation rate Non-Acoustic properties Acoustic behavior porosity, tortuosity,… absorption, transmission,… 2 t C C 2 l Polyurethane foam • Tetrakaidecahedra Unit cell Cell size (Cs) Ligament length (l ) Ligament thickness (t) • Reticulation rate (Rw) 2V Sound JCA model Absorption f A (1 R ) A S w w 0.676 close pore ligament 0.380 1 Rw 1.05 ' Cell size 1.116 1 Rw open pore 1 ' / 1.55 Rw 2 t 1C l *O. Doutres, N. Atalla, “A semi-empirical model to predict the acoustic behavior of fully and partially reticulated polyurethane foams based on microstructure properties” Acoustics 2012 28 Microstructure based models Validation Foam P2: CS= 616 ± 36 m l = 209 ± 14 m t =50 ± 4 m Rw= 32 ± 11 % Foam P3: CS=1710 ± 161 m l = 554 ± 39 m t =151 ± 8 m Rw=5 ± 2 % simulation expanded uncertainty measurements 29 Predictive methods for porous media Accuracy Mechanical Admittance Empirical Limp Rigid Poroelastic Assumptions Set up, Needed parameters and computation time 30 Experimental characterization of porous materials 31 Characterization Methods Direct Viscous length Thermal length Tortuosity Resistivity Porosity Bulk density Young’s modulus Poisson’s ratio Loss factor Inversion Time Viscous length Thermal length Tortuosity Resistivity Porosity Frequency Ultrasound Viscous length Thermal length Tortuosity Good compromise easy/robust Number of searched parameters Accuracy Audio Iterative Direct impedance tube transmission tube Viscous length Thermal length Tortuosity Resistivity Porosity Viscous length Thermal length Tortuosity Resistivity Number of searched parameters Accuracy 32 Measurement of Open porosity and bulk density Method: Pressure/Mass method Perfect gas law Assume isothermal process Heavier gas reduces uncertainty: Air, Argon, Krypton, Xenon Uncertainty mainly control by bulk volume of porous aggregate Bulk volume larger than 350 cm for absolute error less than 1% RT m2 m1 m4 m3 1 Vt P2 P1 P4 P3 m3 m1 1 Vt Air Vacuum PVacuum 1 , m1 ,V P1, m1, V Argon GAS High pressure P2 , m 2 ,V P2, m2, V M1 M2 Air Vacuum P3 , m3 ,V Vs Argon GAS P4 , m4 ,V Vs Vs Vs M3 M4 Ref.: http://dx.doi.org/10.1063/1.2749486 Salissou and Panneton: Pressure/mass method to measure open porosity of porous solids, J. Appl. Phys. 101 (2007) 33 Measurement of Static airflow resistivity Direct method based on ASTM C522 or ISO 9053 Ideally on 100-mm diameter specimen Minimum of 3 specimens If pressure drop too small, stack specimens up to maxium of 5 Measurement at 0.5 mm/s (~ sound pressure of 80 dB-ref20µPa) or stepwise down to lower limit of system and extrapolated to 0.5 mm/s. 0.5 mm/s correspond to a flow of 240 CCM for 100-mm diameter Special cares to prevent leaks P Q P A Q h Wall of mounting rings should be thin; however diameter correction may be applied in the calculations 34 Tortuosity measurements Principle of the transmission method Transducer Source Transducer Receiver Without sample With sample t (1) Awo Aw (2) 0 d L L time (s) Refraction index nr ( ) c0 c 1 c0 t ( ) d 1 1 nr2 ( ) 1 B M = n f f ( ) 2 0 = 1 Viscous layer thickness f 35 Tortuosity measurements Principle of the reflection method: Measure the reflection coefficient at various angles r t, Am (t , ) Ar (t , ) Transducer Receiver With rigid plate With sample Transducer Source d Arigid Amaterial Amplitude L 0 z2 1 2 L time (s) 2 2 1 r 1 sin with z 1 r cos z Necessitates the value of the porosity 36 Characteristic lengths estimation Based in the transmission method in two gases Transducer Source Transducer Receiver Without sample With sample t (1) Aw o Aw (2) 0 time (s) L L d Measure equivalent lengths in air (gas 1) and argon (gas 2) and solve: 1 1 1 1 2 1 Pr1 1 1 Leq ,1 Pr 2 1 1 Leq ,2 However, the only robust method for the characterization of tortuosity and characteristic lengths is iterative inversion 37 Iterative method Optimization process Iteratively adjust model parameters so that the model predicts impedance tube measurements Poro‐acoustical model direct ’ inverse Direct characterization optional Inverse characterization Acoustical model Acoustical indicator Impedance tube Ref.: http://www.mecanum.com/files/InversePaper.pdf Y. Atalla, R. Panneton: Inverse Acoustical Chararacterization…, Canadian Acoustics 33 (2001) 38 But rules must be observed For inverse (iterative or direct) characterizations, impedance tube measurements must verify following tests : 1. Sample is saturated by air at rest. 2. Linear acoustics 3. The resistivity and open porosity of the sample are known. 4. Acoustical response mostly follows that of an equivalent fluid. 5. All the physics is captured by the absorption curves. 6. Sample is homogeneous (~symmetric). 7. Boundary conditions do not influence tube measurements. 39 Quality of test sample 40 Is all the physics captured in the absorption curves? Large number of open-cell porous media follow this typical behavior Exception: high resistivity materials, where viscous length dominate viscous forces over resistivity Zones I + II are necessary Zone III is highly recommended for accurate estimations of the parameters 41 Is the material homogeneous along thickness (through-thickness symmetry) ? x RD Z AB Z BA max Z AB , Z BA Z AB Non symmetric Z BA Ref.: http://dx.doi.org/10.1121/1.2947625 Salissou, Panneton: Quantifying through-thickness asymmetry of sound absorbing materials, JASA 124 (2008) 42 Is the material homogeneous along thickness (through-thickness symmetry) ? Example : ok Cast foam Face A versus Face B < 10 % 43 Are measurements too sensitive to boundary conditions in tube ? What is done What we want to measure Acoustical measurements in the Standing Wave Tube (SWT) What we actually measure or 2) or 1) or 1) Check for sensitivity to edge constraints 2) Check for sensitivity to edge acoustical leaks Ref.: http://dx.doi.org/10.1121/1.2947625 Pilon, Panneton, Sgard: Behavioral criterion quantifying …, JASA 124 (2008) 44 44 Effects of mounting conditions Experimental results Transfer Matrix Method Axisymmetric Biot (u,P) model: Bonded all around difficulty of Tube based methods to determine mechanical properties 45 Effects of lateral gaps (leaks) The effect of lateral air gaps (leaks) are important for thick highly resistive materials An axisymetric finite element solver helps to verify this effect or used for design. No leak With 1% leak Air gap Rigid backing F. Castel, Ph.D. thesis, Sherbrooke (2005) 46 Elastic properties [E,,] Young’s modulus [Pa], Poisson’s ratio and damping loss factor follow the same definitions as for elastic materials. Porous materials are generally not isotropic. Most of the time, only the normal properties (under tension or compression) are used. F Typical values - Low density fibrous: - Mid/High density fibrous: - Elastic foams : - Rigid foams : - Metal foams : E 10 kPa; =0 10 kPa E 150 kPa 50 kPa E 500 kPa 500 kPa E 2 Mpa E 30 MPa F 47 Measurement of Elastic properties Method: Based on compression tests using disk shaped samples Properties: Gives true elastic properties (E,,) Account for boundary conditions Excitation frequencies below 1st resonance of the system (5Hz - 60Hz) A minimum of two (2) samples of different shape factors are required R L s R 2L Ref.: http://dx.doi.org/10.1121/1.1419091 Langlois, Panneton, Atalla: Mechanical characterization of poroelastic materials, J. Acoust. Soc. Am. 110 (2001) 48 Direct measurement of Elastic properties Method: The compression test yields the mechanical impedance Z of the sample From Z, loss factor and apparent Young’s modulus are found F Z K jX u Im( Z ) Re( Z ) KL F E A E K Re L A u Apparent Young’s modulus 49 A large correction is needed for large shape factors or large Poisson’s ratio. Measured (Apparent) True P(s,) E E P( s, ) Bulge out effect Shape factor - s The correction factor P depends on: -Shape factor “s=R/2L” -Boundary conditions -Poisson’s ratio “” An Axisymmetrical high-order solid FEM model of the experimental set-up is used to solve and tabulate the correction factors for various (s,). 50 Measuring mechanical impedance on two samples with different shape factors yields… E1 E2 0 P( s1 , ) P( s2 , ) 1 equation 1 unknown () From the Tabulated Correction Values, and polynomial curvefits, the correction factors Ps1 and Ps2 are found. E1 E2 E or P ( s1 , ) P( s2 , ) 51 Transfer Matrix Method based modeling methodology 52 52 Modeling sound packages Noise control materials models are usually implemented using the Transfer Matrix Method (TMM) for planar multilayer systems and FE/BEM approach for general configurations FE module FEM/BEM TMM module Finite size correction for the transfer matrix method Generalized Transfer matrix method (TMM) with size effects Hierarchical finite element for speed and accuracy LF MF HF 53 Principle of Transfer Matrix Method - Assumes planar infinite systems (1D problems) - The global matrix is constructed from constituent transfer matrices, the coupling conditions and the termination conditions : Fluid 1 [ D ]V 0 Structure Thin panel Solid Septum Sandwich General laminates (1) (2) (n) ... A M1 M2 M3 M4 M2n-1 M2n Porous layer Rigid /limp frame Porous-elastic Perforated plates & screens Double porosity … … 54 Example : TMM modeling of sound absorbers (equivalent fluid models) Single layer – Transfer Matrix Method (TMM) p a b p v front c a v back Multilayer – TMM in series p A B p v C D v front back A B a b a b a b a b a b C D c a c a c a c a c a 1 2 3 4 5 55 Transmission of a layer (equivalent fluid) 1 p1 v1 p p 2 3 4 p2 v2 p3 v3 p4 v4 p x Ae jk1x Be jk1x v x x x1 0 A jk1x B jk1x e e Z1 Z1 p1 p 0 A B v1 v 0 1 A B Z cos k1h1 p1 1 v1 j sin k1h1 Z1 … k1 : Complex wave number of medium 1 Z1 : Characteriztic impedance of medium 1 p2 p x1 Ae jk1x1 Be jk1x1 v2 v x1 A jk1x1 B jk1x1 e e Z1 Z1 jZ1 sin k1h1 p2 cos k1h1 v2 p1 p2 T 1 v v 1 2 56 Transmission through a series of layers (multilayer) 1 p1 v1 p p 0 p1 p2 T 1 v1 v2 x1 2 3 4 p2 v2 p3 v3 p4 v4 x2 p3 p2 T 2 v2 v3 p2 p4 T1T2 T3 v2 v4 … x3 x p3 p4 T 3 v4 v3 Transfer matrix combined in series p2 p4 T G v2 v4 57 Use of the Transfer Matrix Method Calculation of vibroacoustic indicators under various excitations: • Impedance / Absorption • Transmission Loss • Added damping • Radiation efficiency • Acoustic/Vibration transmissibility •… Can also be used within SEA framework to handle complicated geometries and systems Principle: assumes the sound package planar and uses TMM to correct (i) non-resonant path; (ii) radiation efficiency; (iii) absorption and (iv) added damping 58 58 Typical application TMM can account Absorption Problem:for Size effects (FTMM) for TL and Absorption predictions 4 Z A lim Z A Z R ,avg 0 f , st ,avg lim 0 1 Z R ,avg 2 2 sin d cos sin d 2 0 Z R , d Transmission Problem: 2 diffuse max 0 min ( , ) Re ZR c cos sin cos d d 2 0 ZR ik S S S e jk sin cos x0 sin y0 1 Z R ,avg 2 0 max 0 sin cos d d min G ( M , M 0 )e 2 jk sin cos x sin y Z R , d dS M 0 dS M Z R ,avg 0 c0 cos Double surface Integral to evaluate ZR is shown to reduce to 1D quick estimation 59 Illustration of size correction 60 Absorption of Multilayer systems Experimental validation for multilayer system with impervious film (septum) . Plane wave Fibrous Septum Foam 2 Rigid wall 61 Absorption of foam-screen systems Perforated screen (h=0.47 mm =137700 Nsm-4 ; =0.08) M3 M1 Screen (=17000 Nsm-4 ;=0.059) 1 Coefficient d'absorption 0,9 0,8 0,7 0,6 0,5 M1 (25.06 mm) écran poreux (0.79 mm) M3 (12.57 mm) 0,4 0,3 Fond rigide 0,2 Prédiction 0,1 0 100 Mesure 1100 2100 3100 4100 5100 6100 Frequences (Hz) Use of an equivalent fluid model for the perfortaed facing Good agreement using tortuosity correction formulation (Atalla & Sgard. JSV 2005) 62 Modeling DWL systems Transmission Loss estimation of a DWL system 2 mm AL 25 mm Foam 1mm AL 38 mm Air Excellent agreement (the challenge is rather the test reduce flanking paths) 63 Radiation of a piston in a Tube Vibrating Piston 283 mm 400 mm Microphone Anechoic termination 20 10 0 Bare Piston Piston with Foam (test) Analysis (IL) -10 -20 -30 -40 -50 -60 20 120 220 320 420 520 620 720 64 Double porosity materials Allows for materials with two scales of porosity (e.g. perforated foams). 65 Patch-work type materials Allows for non-homogenous materials (patch-works) and parallel assemblies using an advanced Parallel/Series implementation of the TMM. Verdiere et al. (2013) Transfer matrix method applied to the parallel assembly of sound absorbing materials. JASA 134(6). 66 Embedded resonators 67 Transmission through mounts Validation vs. FE & Tests for a point load (ROF) excitation Excitation: ROF Metric: Acoustical to Meahanical Conversion Efficiency (AMCE) 2in FG Sandwich trim Stiffened panel Rigid or flexible (mount) connection AMCE 10log10 in rad 68 Conclusion Use of Biot based models for porous material is nowadays widely in industry Many Direct and iterative (Indirect) methods exist for the characterization of the 9 material properties Fine characterization depends on many factors: Quality of specimens (geometry, homogeneity, …) Control of edge effects Expertise of experimenter Perspectives: Need for standards for full poroelastic characterization: Impedance, absorption measurement (Ok but not complete) Resistivity (Ok) The rest of the properties (standards & QA needed) 69 Conclusion TMM based models are Quick & accurate enough to be used for design and what if questions… Comparison with Tests & FE simulations show that they are even acceptable for large curved panel (aerospace applications; low ring frequency) and various types of excitations Perspectives: • More studies with various panel constructions, radius of curvatures & excitations (DAF & TBL) • Efficient combination with FE models hybrid models (see my keynote presentations at ISNVH14) • Accounting for input parameters variance, anisotropy and mounting conditions 70 References Extended version of this talk and more info about the topic can be found in : • ASME/NCAD workshop : http://files.asme.org/Divisions/NCAD/33112.pdf • Winter school on the Acoustics of Poro-Visco-Elastic Media. Lyon, 12-14 Feb. 2014 ([email protected]) • Allard & Atalla: Propagation of Sound in Porous Media. 2nd Edition, Wiley, 2009 71
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