MDGS September 2014 Analysis

REPORT NUMBER
14-252-9648
PAGE 1/4
REPORT DATE
SEND TO
Sep 09, 2014
22324
ISSUE DATE
Sep 09, 2014
®
RECEIVED DATE
Sep 05, 2014
13611 “B” Street • Omaha, Nebraska 68144-3693 • (402) 334-7770 • FAX (402) 334-9121
www.midwestlabs.com
REPORT OF ANALYSIS
SHOW ME ETHANOL LLC
PO BOX 9
CARROLLTON MO 64633-0009
For: (22324) SHOW ME ETHANOL LLC
WDGS
Level Found
Analysis
As Received
Sample ID: W0073
Lab Number: 12319767
Moisture
Dry matter
Protein (crude)
Fat (crude)
Fiber (acid detergent)
Fiber (crude)
Fiber (neutral detergent)
Ash
Total digestible nutrients
Net energy (lactation)
Net energy (maint.)
Net energy (gain)
Digestible energy
Metabolizable energy
Sulfur (total)
Phosphorus (total)
Potassium (total)
Magnesium (total)
Calcium (total)
Dry Weight
Units
Date Sampled: 2014-09-04
55.04
///////
%
44.96
///////
%
14.1
31.3
%
3.14
6.98
%
5.9
13.1
%
2.15
4.78
%
13.5
30
%
3.40
7.56
%
36.0
80.0
%
0.38
0.84
Mcal/lbs
0.39
0.86
Mcal/lbs
0.26
0.58
Mcal/lbs
0.72
1.60
Mcal/lbs
0.65
1.44
Mcal/lbs
0.20
0.44
%
0.68
1.52
%
0.88
1.95
%
0.22
0.49
%
0.01
0.03
%
Reporting
Limit
0.01
0.010
0.20
0.10
0.5
0.20
1.0
0.10
0.1
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.01
Method
AOAC 930.15 *
CALCULATION *
AOAC 990.03 *
AOAC 945.16 *
ANKOM Tech. Method *
AOCS Ba 6a-05 *
ANKOM Tech. Method *
AOAC 942.05 *
CALCULATION *
CALCULATION *
CALCULATION *
CALCULATION *
CALCULATION *
CALCULATION *
AOAC 985.01 (mod) *
AOAC 985.01 (mod) *
AOAC 985.01 (mod) *
AOAC 985.01 (mod) *
AOAC 985.01 (mod) *
AnalystDate
VerifiedDate
zlk8-2014/09/08
jpt1-2014/09/09
Auto-2014/09/09
Auto-2014/09/09
kfl0-2014/09/08
jpt1-2014/09/09
kfl0-2014/09/09
jpt1-2014/09/09
vrm7-2014/09/08
jpt1-2014/09/09
sdh7-2014/09/09
jpt1-2014/09/09
pgr4-2014/09/08
jpt1-2014/09/09
vrm7-2014/09/09
jpt1-2014/09/09
Auto-2014/09/09
Auto-2014/09/09
Auto-2014/09/09
Auto-2014/09/09
Auto-2014/09/09
Auto-2014/09/09
Auto-2014/09/09
Auto-2014/09/09
Auto-2014/09/09
Auto-2014/09/09
Auto-2014/09/09
Auto-2014/09/09
cvs7-2014/09/09
jpt1-2014/09/09
cvs7-2014/09/09
jpt1-2014/09/09
cvs7-2014/09/09
jpt1-2014/09/09
cvs7-2014/09/09
jpt1-2014/09/09
cvs7-2014/09/09
jpt1-2014/09/09
The result(s) issued on this report only reflect the analysis of the sample(s) submitted.
Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
REPORT NUMBER
14-252-9648
PAGE 2/4
REPORT DATE
SEND TO
Sep 09, 2014
22324
ISSUE DATE
Sep 09, 2014
®
RECEIVED DATE
Sep 05, 2014
13611 “B” Street • Omaha, Nebraska 68144-3693 • (402) 334-7770 • FAX (402) 334-9121
www.midwestlabs.com
REPORT OF ANALYSIS
SHOW ME ETHANOL LLC
PO BOX 9
CARROLLTON MO 64633-0009
For: (22324) SHOW ME ETHANOL LLC
WDGS
Level Found
Analysis
Sample ID: W0073
Sodium (total)
Iron (total)
Manganese (total)
Copper (total)
Zinc (total)
Starch (total)
As Received
Lab Number: 12319767 (con't)
0.14
56.2
10.9
4.1
38.4
1.58
Dry Weight
0.31
125
24.3
9.1
85.3
3.51
Units
%
ppm
ppm
ppm
ppm
%
Reporting
Limit
0.01
5.0
1.0
1.0
1.0
0.10
Method
AOAC 985.01 (mod) *
AOAC 985.01 (mod) *
AOAC 985.01 (mod) *
AOAC 985.01 (mod) *
AOAC 985.01 (mod) *
AACC 76-11 (mod) *
AnalystDate
VerifiedDate
cvs7-2014/09/09
jpt1-2014/09/09
cvs7-2014/09/09
jpt1-2014/09/09
cvs7-2014/09/09
jpt1-2014/09/09
cvs7-2014/09/09
jpt1-2014/09/09
cvs7-2014/09/09
jpt1-2014/09/09
alm0-2014/09/08
mgn8-2014/09/09
ppm = parts per million, ppm = mg/kg Mineral analysis performed by ICAP using a wet digest procedure.
Total starch value includes all hydrolyzable carbohydrates.
For questions please contact:
Lisa Avila
Staff
[email protected] (402)829-9847
The result(s) issued on this report only reflect the analysis of the sample(s) submitted.
Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
REPORT NUMBER
14-252-9648
PAGE 3/4
REPORT DATE
SEND TO
Sep 09, 2014
22324
ISSUE DATE
®
Sep 09, 2014
RECEIVED DATE
Sep 05, 2014
13611 “B” Street • Omaha, Nebraska 68144-3693 • (402) 334-7770 • FAX (402) 334-9121
www.midwestlabs.com
REPORT OF ANALYSIS
SHOW ME ETHANOL LLC
PO BOX 9
CARROLLTON MO 64633-0009
For: (22324) SHOW ME ETHANOL LLC
WDGS
Detailed Method Description(s)
Moisture
Analysis follows MWL FD PROC 16 which is based on AOAC 930.15. A sample is blended, mixed, or ground to obtain a homogenous sub-sample. The sample aliquot is
placed in a pre-weighed tin, weighed to get a sample weight and then placed in a 135 oC convection oven for two (2) hours. The sample is then removed, cooled in a
desiccator and reweighed. The loss in weight is reported as % moisture
AACC 76-11 (mod)
Analysis follows WC PROC 47 which is based on modified AACC-76-11 and YSI Application Note 319. A sample is combined with water and placed in an autoclave.
After the autoclave step, buffer and amyloglucosidase enzyme are added and the sample placed in a water bath where the starch is hydrolyzed to glucose. The glucose is
then determined using a YSI glucometer.
Calculation
Analytical results are entered into applicable formulas to provide a calculated result which is reported.
Protein (Crude)
Analysis follows MWL FD PROC 70 which is based on AOAC 990.03. The sample is placed in a combustion instrument and the amount of nitrogen is obtained. The
nitrogen value is multiplied by a factor of 6.25 and that value reported as crude protein.
Crude Fat
Analysis follows MWL FD PROC 26 which is based on AOAC 945.16. The sample is extracted with drip immersion of the sample in petroleum (pet) ether. The pet ether
is poured into a pre-weighed container and then evaporated. The container is re-weighed and the increase in weight is reported as crude fat
Acid Detergent Fiber
Analysis follows MWL FD PROC 21 which is based on Ankom Technology method. The sample is sealed in a small bag and the bag immersed in a solution that dissolves
certain materials. The bag is washed and dried and re-weighed. The material remaining in the bag is reported as acid detergent fiber
The result(s) issued on this report only reflect the analysis of the sample(s) submitted.
Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
REPORT NUMBER
14-252-9648
PAGE 4/4
REPORT DATE
SEND TO
Sep 09, 2014
22324
ISSUE DATE
®
Sep 09, 2014
RECEIVED DATE
Sep 05, 2014
13611 “B” Street • Omaha, Nebraska 68144-3693 • (402) 334-7770 • FAX (402) 334-9121
www.midwestlabs.com
REPORT OF ANALYSIS
SHOW ME ETHANOL LLC
PO BOX 9
CARROLLTON MO 64633-0009
For: (22324) SHOW ME ETHANOL LLC
WDGS
Crude Fiber
Analysis follows MWL FD PROC 039 which is based on AOCS Ba 6a-05. A small amount of sample is weighed and placed in a membrane bag and sealed. The bag and
sample are placed in a container that treats the sample with a variety of chemicals to dissolve materials which leach out of the bag. After repeated washing and rinsing, the
bag is dried and reweighed. The material remaining in the bag is reported as crude fiber
Ash
Analysis follows MWL FD PROC 19 which is based on AOAC 942.05. The sample is weighed and placed in a muffle furnace at 600 oC. After a period of time, the
sample is removed and the remaining material weighed and reported as ash. Moisture and organic material is driven off.
ICP analysis of Feeds
Analysis follows MWL ME PROC 29 which is based on AOAC 985.01. Samples have been prepared using MWL ME PROC 69 which is a wet ash procedure that requires
mineral acids and heat. Sample analysis involves moving the sample extract into the ICP where it is nebulized and introduced into the high temperature plasma which
energizes the electrons of the dissolved minerals/metals. As the energized electrons of the minerals/metals return to ground state, energy is released as light. The emitted
wavelength(s) and light intensities are used to identify and quantitate the minerals/metals in the sample
The result(s) issued on this report only reflect the analysis of the sample(s) submitted.
Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.