REPORT NUMBER 14-252-9648 PAGE 1/4 REPORT DATE SEND TO Sep 09, 2014 22324 ISSUE DATE Sep 09, 2014 ® RECEIVED DATE Sep 05, 2014 13611 “B” Street • Omaha, Nebraska 68144-3693 • (402) 334-7770 • FAX (402) 334-9121 www.midwestlabs.com REPORT OF ANALYSIS SHOW ME ETHANOL LLC PO BOX 9 CARROLLTON MO 64633-0009 For: (22324) SHOW ME ETHANOL LLC WDGS Level Found Analysis As Received Sample ID: W0073 Lab Number: 12319767 Moisture Dry matter Protein (crude) Fat (crude) Fiber (acid detergent) Fiber (crude) Fiber (neutral detergent) Ash Total digestible nutrients Net energy (lactation) Net energy (maint.) Net energy (gain) Digestible energy Metabolizable energy Sulfur (total) Phosphorus (total) Potassium (total) Magnesium (total) Calcium (total) Dry Weight Units Date Sampled: 2014-09-04 55.04 /////// % 44.96 /////// % 14.1 31.3 % 3.14 6.98 % 5.9 13.1 % 2.15 4.78 % 13.5 30 % 3.40 7.56 % 36.0 80.0 % 0.38 0.84 Mcal/lbs 0.39 0.86 Mcal/lbs 0.26 0.58 Mcal/lbs 0.72 1.60 Mcal/lbs 0.65 1.44 Mcal/lbs 0.20 0.44 % 0.68 1.52 % 0.88 1.95 % 0.22 0.49 % 0.01 0.03 % Reporting Limit 0.01 0.010 0.20 0.10 0.5 0.20 1.0 0.10 0.1 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 Method AOAC 930.15 * CALCULATION * AOAC 990.03 * AOAC 945.16 * ANKOM Tech. Method * AOCS Ba 6a-05 * ANKOM Tech. Method * AOAC 942.05 * CALCULATION * CALCULATION * CALCULATION * CALCULATION * CALCULATION * CALCULATION * AOAC 985.01 (mod) * AOAC 985.01 (mod) * AOAC 985.01 (mod) * AOAC 985.01 (mod) * AOAC 985.01 (mod) * AnalystDate VerifiedDate zlk8-2014/09/08 jpt1-2014/09/09 Auto-2014/09/09 Auto-2014/09/09 kfl0-2014/09/08 jpt1-2014/09/09 kfl0-2014/09/09 jpt1-2014/09/09 vrm7-2014/09/08 jpt1-2014/09/09 sdh7-2014/09/09 jpt1-2014/09/09 pgr4-2014/09/08 jpt1-2014/09/09 vrm7-2014/09/09 jpt1-2014/09/09 Auto-2014/09/09 Auto-2014/09/09 Auto-2014/09/09 Auto-2014/09/09 Auto-2014/09/09 Auto-2014/09/09 Auto-2014/09/09 Auto-2014/09/09 Auto-2014/09/09 Auto-2014/09/09 Auto-2014/09/09 Auto-2014/09/09 cvs7-2014/09/09 jpt1-2014/09/09 cvs7-2014/09/09 jpt1-2014/09/09 cvs7-2014/09/09 jpt1-2014/09/09 cvs7-2014/09/09 jpt1-2014/09/09 cvs7-2014/09/09 jpt1-2014/09/09 The result(s) issued on this report only reflect the analysis of the sample(s) submitted. Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. REPORT NUMBER 14-252-9648 PAGE 2/4 REPORT DATE SEND TO Sep 09, 2014 22324 ISSUE DATE Sep 09, 2014 ® RECEIVED DATE Sep 05, 2014 13611 “B” Street • Omaha, Nebraska 68144-3693 • (402) 334-7770 • FAX (402) 334-9121 www.midwestlabs.com REPORT OF ANALYSIS SHOW ME ETHANOL LLC PO BOX 9 CARROLLTON MO 64633-0009 For: (22324) SHOW ME ETHANOL LLC WDGS Level Found Analysis Sample ID: W0073 Sodium (total) Iron (total) Manganese (total) Copper (total) Zinc (total) Starch (total) As Received Lab Number: 12319767 (con't) 0.14 56.2 10.9 4.1 38.4 1.58 Dry Weight 0.31 125 24.3 9.1 85.3 3.51 Units % ppm ppm ppm ppm % Reporting Limit 0.01 5.0 1.0 1.0 1.0 0.10 Method AOAC 985.01 (mod) * AOAC 985.01 (mod) * AOAC 985.01 (mod) * AOAC 985.01 (mod) * AOAC 985.01 (mod) * AACC 76-11 (mod) * AnalystDate VerifiedDate cvs7-2014/09/09 jpt1-2014/09/09 cvs7-2014/09/09 jpt1-2014/09/09 cvs7-2014/09/09 jpt1-2014/09/09 cvs7-2014/09/09 jpt1-2014/09/09 cvs7-2014/09/09 jpt1-2014/09/09 alm0-2014/09/08 mgn8-2014/09/09 ppm = parts per million, ppm = mg/kg Mineral analysis performed by ICAP using a wet digest procedure. Total starch value includes all hydrolyzable carbohydrates. For questions please contact: Lisa Avila Staff [email protected] (402)829-9847 The result(s) issued on this report only reflect the analysis of the sample(s) submitted. Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. REPORT NUMBER 14-252-9648 PAGE 3/4 REPORT DATE SEND TO Sep 09, 2014 22324 ISSUE DATE ® Sep 09, 2014 RECEIVED DATE Sep 05, 2014 13611 “B” Street • Omaha, Nebraska 68144-3693 • (402) 334-7770 • FAX (402) 334-9121 www.midwestlabs.com REPORT OF ANALYSIS SHOW ME ETHANOL LLC PO BOX 9 CARROLLTON MO 64633-0009 For: (22324) SHOW ME ETHANOL LLC WDGS Detailed Method Description(s) Moisture Analysis follows MWL FD PROC 16 which is based on AOAC 930.15. A sample is blended, mixed, or ground to obtain a homogenous sub-sample. The sample aliquot is placed in a pre-weighed tin, weighed to get a sample weight and then placed in a 135 oC convection oven for two (2) hours. The sample is then removed, cooled in a desiccator and reweighed. The loss in weight is reported as % moisture AACC 76-11 (mod) Analysis follows WC PROC 47 which is based on modified AACC-76-11 and YSI Application Note 319. A sample is combined with water and placed in an autoclave. After the autoclave step, buffer and amyloglucosidase enzyme are added and the sample placed in a water bath where the starch is hydrolyzed to glucose. The glucose is then determined using a YSI glucometer. Calculation Analytical results are entered into applicable formulas to provide a calculated result which is reported. Protein (Crude) Analysis follows MWL FD PROC 70 which is based on AOAC 990.03. The sample is placed in a combustion instrument and the amount of nitrogen is obtained. The nitrogen value is multiplied by a factor of 6.25 and that value reported as crude protein. Crude Fat Analysis follows MWL FD PROC 26 which is based on AOAC 945.16. The sample is extracted with drip immersion of the sample in petroleum (pet) ether. The pet ether is poured into a pre-weighed container and then evaporated. The container is re-weighed and the increase in weight is reported as crude fat Acid Detergent Fiber Analysis follows MWL FD PROC 21 which is based on Ankom Technology method. The sample is sealed in a small bag and the bag immersed in a solution that dissolves certain materials. The bag is washed and dried and re-weighed. The material remaining in the bag is reported as acid detergent fiber The result(s) issued on this report only reflect the analysis of the sample(s) submitted. Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. REPORT NUMBER 14-252-9648 PAGE 4/4 REPORT DATE SEND TO Sep 09, 2014 22324 ISSUE DATE ® Sep 09, 2014 RECEIVED DATE Sep 05, 2014 13611 “B” Street • Omaha, Nebraska 68144-3693 • (402) 334-7770 • FAX (402) 334-9121 www.midwestlabs.com REPORT OF ANALYSIS SHOW ME ETHANOL LLC PO BOX 9 CARROLLTON MO 64633-0009 For: (22324) SHOW ME ETHANOL LLC WDGS Crude Fiber Analysis follows MWL FD PROC 039 which is based on AOCS Ba 6a-05. A small amount of sample is weighed and placed in a membrane bag and sealed. The bag and sample are placed in a container that treats the sample with a variety of chemicals to dissolve materials which leach out of the bag. After repeated washing and rinsing, the bag is dried and reweighed. The material remaining in the bag is reported as crude fiber Ash Analysis follows MWL FD PROC 19 which is based on AOAC 942.05. The sample is weighed and placed in a muffle furnace at 600 oC. After a period of time, the sample is removed and the remaining material weighed and reported as ash. Moisture and organic material is driven off. ICP analysis of Feeds Analysis follows MWL ME PROC 29 which is based on AOAC 985.01. Samples have been prepared using MWL ME PROC 69 which is a wet ash procedure that requires mineral acids and heat. Sample analysis involves moving the sample extract into the ICP where it is nebulized and introduced into the high temperature plasma which energizes the electrons of the dissolved minerals/metals. As the energized electrons of the minerals/metals return to ground state, energy is released as light. The emitted wavelength(s) and light intensities are used to identify and quantitate the minerals/metals in the sample The result(s) issued on this report only reflect the analysis of the sample(s) submitted. Our reports and letters are for the exclusive and confidential use of our clients and may not be reproduced in whole or in part, nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
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