MEGA-DEX G-01 chiral column performances

MEGA-DEX G-01
chiral test
Column: MEGA-DEX G-01 - 0.15mm, 0.15µm, 25m
!Catalog Code: DEX-G01-015-015-25
New Column
1.
2.
3.
4.
5.
4
2
2-Octanol enantiomers
Linalyl Aceate enantiomers
Menthol enantiomers
Isobornyl Acetate enantiomers
Camphor enantiomers
5
1
3
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43 min
Acknowledgments: many thanks to Dr. Cecilia Cagliero and Prof. Carlo Bicchi, Università di Torino, Dipartimento di Scienza e Tecnologia del Farmaco, Via P. Giuria, 9, Torino, Italy.
www.mega.mi.it
MEGA s.n.c - Via Plinio, 29 - 20025 Legnano (MI) - Italy - Tel./fax: +39 0331.54.79.24 - [email protected] - Since 1980
Bornyl and Isobornyl Acetate
chiral separation
uV(x1,000)
Chromatogram
Column: MEGA-DEX G-01 - 0.15mm, 0.15µm, 25m
!Catalog Code: DEX-G01-015-015-25
1.50
Bornyl Acetate (S) (95%)
1.25
1.00
0.75
New Column
Bornyl Acetate (R) (5%)
Isobornyl Acetate (+,-)
Conditions:
!Injection: Split, 250°C. 0.50
Detector: FID 250°C. 0.25
Oven Program: 70°C, 1°C/min.
0.00
30.50
30.75
31.00
31.25
31.50
31.75
32.00
32.25
32.50
32.75
33.00
min
uV(x100)uV(x1,000)
Chromatogram
8.0 Chromatogram
1.25
7.0
1.00
6.0
5.0
0.75
4.0
0.50
3.0
0.25
2.0
Bornyl Acetate (S)
Bornyl Acetate (R)
R=1.52
Column: MEGA-DEX G-01 - 0.20mm, 0.20µm, 30m
!Catalog Code: DEX-G01-020-020-30
Isobornyl Acetate (+,-)
New Column
R=1.72
Conditions:
!Injection: Split, 250°C. 0.00
1.0
47.0
47.5
48.0
48.5
49.0
49.5
50.0
50.5
51.0
51.5
52.0
52.5
53.0
min
Detector: FID 250°C. 0.0
Oven Program: 83°C isothermal.
uV(x1,000)
1.25
-1.0
33.5
1.00
0.75
Carrier Gas: Hydrogen, 0.6mL/min constant flow.
Bornyl 34.0
34.5
Acetate (S) (95%)
35.0
35.5
Isobornyl Acetate
36.5
37.0
36.0
Bornyl Acetate (R) (5%)
38.0
38.5
39.0
39.5
min
Carrier Gas: Hydrogen, 0.8mL/min constant flow.
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0.50
R=1.72
R=1.42
0.25
(+,-) 37.5
Acknowledgments: many thanks to Dr. Cecilia Cagliero and Prof. Carlo Bicchi, Università di Torino, 0.00
47.5
48.0
48.5
49.0
49.5
50.0
50.5
51.0
51.5
52.0
min
Dipartimento di Scienza e Tecnologia del Farmaco, Via P. Giuria, 9, Torino, Italy.
www.mega.mi.it
MEGA s.n.c - Via Plinio, 29 - 20025 Legnano (MI) - Italy - Tel./fax: +39 0331.54.79.24 - [email protected] - Since 1980
contact us: [email protected]
follow us @MEGAColumns
www.mega.mi.it
MEGA s.n.c - Via Plinio, 29 - 20025 Legnano (MI) - Italy - Tel./fax: +39 0331.54.79.24 - [email protected]

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