3900 GC Keypad Green keys cause changes to take place immediately, for instance pressing NEW LINE will cause a new line to be added to a method time program table. Yellow keys take you to entries that can be changed such as method sections, setup and commands. Blue keys are display actions only. They display status or help navigate the display, they can also be used to cancel an edit before it is accepted by pressing ENTER. LEDs show you the GC run state and which section is shown on the display at a glance. Use + and – to change entry values in editable fields. Use UP LINE to scroll up through the various display pages and to cancel an edit before pressing ENTER. Pressing START will begin automation if present, start a run if no automation is present, or allow you to AutoInject a sample. The STOP key ends a run in progress. READY RUN STAB/EQUIL NOT READY FAULT E N T E R UP LINE Use ENTER to scroll down through display pages and to accept changes made to editable fields (denoted by flashing right cursor). A/S EE START STOP INJ NEW LINE Use the AUTO key to program local automation. AUTO COL DELETE LINE Pressing STATUS allows you to view the actual conditions being used by the 3900 GC. Use NEW LINE and DELETE LINE to add and remove program lines to Method time program tables. DET STATUS SETUP Press SETUP to change instrument basic configuration settings such as: • Column dimensions • Carrier Gas • Perform IEFC and DEFC Autocalibration • Perform Septum Purge calibration • Calibrate A/S vial and injector positions COMMAND Press COMMAND to perform actions that are not part of a method time program. Examples of these imperative actions are: • Turn column oven on or off. • Activate, copy, or preset a method. • Detector ignite, autozero now, or clear autozero. • AutoSampler change syringe, reset plunger counter, tower home, beeper on/off. • Remote or local mode operation (with Ethernet communications Option). Hint: Commands are grouped according to the operation being performed, press COMMAND multiple times to jump between sections. Use either ENTER or UP LINE to step through the various entries one at a time. Pressing A/S EE displays the AutoSampler and External Events methods for editing. AutoSampler must be present to edit A/S method sections. Pressing INJ allows you to turn the injector oven on and off and displays the injector (temperature and split ratio), and carrier gas (pressure or constant flow modes) methods for editing. Pressing COL allows you to edit and build column oven temperature programs and set the stabilization time. Pressing DET allows you to turn the detector oven and detector electronics on and off, and displays the detector time program allowing you to set temperature, detector range, attenuation, and time programmed AutoZero events. 03-914885-00:Rev. 3 Preset Method The 3900 GC uses a Preset Method compatible with light hydrocarbon samples (C-14, C-15, and C-16 such as found in the FID and TCD Test Mix). The preset conditions on power-up are: Injector =140 ºC Split ratio set to 50 Flow rate set to 2 mL/min Column oven set to 80 ºC for 0.5 minutes ramping to 160 ºC at 20 ºC/min and holding for 2 minutes Detector set to 200 ºC Inject the Test Mix 1. Make certain an appropriate column is installed. 2. Make certain the correct gasses are connected and turned on. 3. Ensure the GC is powered up and the Star Workstation or a data acquisition system is connected. 4. Perform an Inject Single Sample action if you are using the Star Workstation, or wait for the data system to be ready to acquire data. 5. Finally, make your injection. Modify the Preset Method if the conditions are not appropriate for your sample. To return to preset conditions, press the COMMAND key on the keypad and select Preset Method. 3900 GC Features Full access to the injector Hinged detector cover Septum purge cover snaps off Access to detector Injector cover rolls back Septum purge adjustment Septum purge cover off 03-914885-00:Rev. 3
© Copyright 2024 ExpyDoc