22 Micro and Nanosystems, 2009, 1, 22-29 Modeling, Design and Experimental Characterization of Bending Resonant Circular Nano Cantilevers N. Lobontiu*,1, B. Ilic2, T. Reissman2, E. Garcia2, Y. Nam3 and H.G. Craighead2 1 University of Alaska Anchorage, USA; 2 Cornell University, USA; 3Kangwon National University, Korea Abstract: This work reports on a new type of nano cantilever, the symmetric circular one, and provides results of its outof-plane bending natural frequency by means of analytical modeling and experimental testing. The cantilever, with a 225 nm thickness and planar dimensions smaller than 10 m, can be implemented in dynamic nano electromechanical applications such as atomic force microscopy, surface topology characterization or resonance-shift mass detection. An analytic model is proposed that considers the distributed stiffness and inertia properties through an accurate distribution function. The model also captures the short-beam character of this structure and the related shear effects. Several silicon nitride nano cantilevers have been surface-micromachined and tested by using in-vacuum laser excitation and interferometric measurement of the bending resonant response. The model predictions and the experimental results indicated minimal errors. Based on this agreement, the analytical model was utilized to further analyze the influence of the basic geometric parameters on the cantilever’s natural frequency. Keywords: MEMS, NEMS, cantilever, circular, resonator, bending. 1. INTRODUCTION This report presents results on the modeling, design, experimental and simulation of the out-of-plane bending natural frequency for a novel nano cantilever design, the constant-thickness circular cantilever, which can be implemented in a variety of applications, such as resonant detection of minute amounts of attached substance or dynamic atomic force microscopy (AFM) transduction. The main advantage of this specific cantilever over existing designs consists in its ability to produce a wide range of resonant frequencies by changes in the circular notch radius and in the notch center position. Another advantage is the analytical model, which takes into consideration the short-beam character of this particular design by means of the exact deformation distribution function, and thus enables accurate simulation to be performed. At micro and nano scale, under specified fabrication constraints, and for a given geometrical envelope, say of rectangular shape, the main modality of altering a cantilever’s natural frequency is through shape modification. Shapes that can be described by analytical curves present the advantage that closed-form equations, which are often times sufficiently-accurate for conducting first-stage model simulation, can be obtained for the amount of interest of a given structure, be it the stiffness in a static application, or a certain resonant frequency in a dynamic problem. The procedure of selecting specific geometric shapes is therefore extremely important in producing designs that are capable of matching pre-defined performance criteria (such as specified static deflections or natural frequencies), as well as in refining the geometrical set of parameters in view of optimizing the structural response. Cantilevers with dimensions in the micrometer and nanometer range have been used lately for substance characterization or recognition through dynamic operation in viscous fluids [1-4], for imaging/sensing, data writing/storage *Address correspondence to this author at the University of Alaska Anchorage, USA; E-mail: [email protected] 1876-4029/09 $55.00+.00 or material properties evaluation through scanning-probe microscopy, atomic-force microscopy [5-10] or model identification [11]. Two physical principles are usually being applied in micro/nano-scale cantilever-based transduction: (a) the deflection change is statically monitored; or (b) the shift in a relevant natural frequency (most often the one corresponding to the out-of-plane, weak-axis vibrations) is determined [12, 13]. The cantilever deflection alters as a result of a variety of external factors such as microtemperature variation, molecular adsorption, microcorrosion, phase change or stress-induced surface property changes [14-17]. Natural frequency shift methods have successfully been applied in detecting the quantity (to the level of attogram) and position of matter that deposits on a cantilever [18-30] or in physical/chemical sensors [31, 32]. Fig. (1). Three-dimensional view of a circular nano cantilever. Studied here is a new cantilever design, the symmetric circular nano cantilever, which is pictured in the threedimensional rendering of Fig. (1). For a specified thickness, this configuration provides dimensional and therefore operational variability through modifications of a few geometric parameters, as it will be discussed shortly. Particular emphasis of this research falls on the out-of-plane bending resonant frequency (about the y-axis, the weak axis), which is investigated through a mathematical model and experimental testing. © 2009 Bentham Science Publishers Ltd. Circular Nano Cantilevers Fig. (2) shows the top-view schematic of a generic circular nano cantilever that is defined by the radius R, the minimum thickness wmin, the start angle min and the end angle max. Fig. (2). Schematic top view of a generic circular nano cantilever with geometry and dimensions. A large variety of circular geometric configurations can be generated from a given rectangular plate of dimensions L and W – see Fig. (3) – by modifying only three geometric parameters pertaining to two identical circular regions that are placed symmetrically with respect to the plate longitudinal direction, namely: the radius R, minimum transverse distance wmin and common longitudinal position L0. Fig. (4) shows three limit designs that can be realized by only chang- Micro and Nanosystems, 2009 Vol. 1, No. 1 23 ing the value of the longitudinal parameter L0 of Fig. (3), which results in alterations of the limit angles min and max. The right corner-filleted design of Fig. (4a) is wellknown – it was first analyzed in terms of analytical compliances (the inverses of stiffnesses) in [33] in the 1960s and more recently in [34], amongst others. Two other configurations, the half-length circular one and the symmetric design, are shown in Figs. (4b and 4c). The method of calculating the out-of-plane bending natural frequency is based on Rayleigh’s principle for conservative systems, which yields the resonant frequency as the solution to an equation comprising the elastic potential energy and the kinetic energy. The calculation method that we utilize herein is compact as it expresses both stiffness and inertia properties of a vibrating continuous, beam-like structure by means of a unique function: the deflection distribution function. In the majority of similar research reports, the simplified form of the distribution function corresponding to a constant cross-section cantilever has been utilized. This work employs the actual, exact-form distribution function which depends on the particular geometry of the studied structure by also taking into consideration the shearing effects (due to the short length of the circular cantilever) – and these represent novel features of this report. The distribution function can be expressed generically in terms of compliances for any cantilever profile which is expressed by an analytical function. Experimental testing has been conducted on several surface-micromachined circular-cantilever samples and comparison between experimental data and analytic model simulation revealed good correlation. Subsequent numerical simulations, based on the analytical model, have also been performed in order to derive conclusions on the relationship between geometric parameters and the out-of-plane bending natural frequency of the circular nano cantilever. Fig. (3). Generation of a circular cantilever from a blank rectangular plate of dimensions L x W and two identical circles of radii R. 24 Micro and Nanosystems, 2009 Vol. 1, No. 1 Lobontiu et al. Fig. (4). Limit configurations of circular cantilevers: (a) Right circular (corner-filleted) design (min = 0o, max = 180o); (b) Half-length circular design (min = 0o, max = 90o); (c) Symmetric profile (min + max = 180o). 2. ANALYTIC MODEL OF OUT-OF-PLANE BENDING NATURAL FREQUENCY A generic model is first derived of the out-of-plane bending natural frequency for a single-profile cantilever and then specific geometry is used to calculate the bending natural frequency of the circular cantilever design. 2.1. Generic Model for a Generic Single-Profile Cantilever The out-of-plane bending natural frequency is formulated in this section based on the cantilever model which is shown in Fig. (5), and which represents the circular design reported herein. The slopes and deflections are identified in Fig. (5) that correspond to the free end – y and uz – and to a generic point of abscissa x – y(x) and uz(x), respectively. Axial deformations (ux(x) at the generic point of abscissa x and ux at the free end) are produced by the force Fx, but these deformations are not shown in Fig. (5). 2 2u ( x ) E I y ( x) z 2 dx x 2 = 0 l A( x)u z2 ( x)dx l (1) 0 where Iy(x) and A(x) are the variable cross-sectional moment of inertia and area that are measured at the generic abscissa x – Fig. (5), and are expressed as: w( x)t 3 I y ( x) = 12 A( x) = w( x)t (2) with w(x) being the variable width and t the constant thickness. The deflection at an arbitrary abscissa, uz(x), is expressed in terms of the free-end deflection uz by means of a distribution function f(x) as: u z ( x) = f ( x)u z (3) In this case, Rayleigh’s quotient – Eq. (1) becomes: 2 d 2 f ( x) E I y ( x) dx dx 2 2 0 = l 2 A( x) [ f ( x) ] dx l (4) 0 Fig. (5). Bent cantilever with representative slopes and deflections. The circular nano cantilever is a single-profile configuration, as its variable width can be defined by one analytical curve (the circular one). In the case of a variable crosssection beam, the out-of-plane bending natural frequency is expressed by means of Rayleigh’s quotient as: Eq. (4) is quite versatile as it enables calculating the outof-plane bending resonant frequency of both cantilevers (fixed-free beams) and bridges (fixed-fixed beams) whose cross-section can vary continuously – their cross-sectional dimensions (width and thickness) are defined each by a single analytical curve, such as line segment, circular, elliptic or other planar curve’s profile equation. The other prerequisite in using Eq. (4) is knowledge of the bending-related distribution function f(x). In our case, the nano resonators are mod- Circular Nano Cantilevers Micro and Nanosystems, 2009 Vol. 1, No. 1 25 eled and fabricated as cantilevers that have one end built-in (anchored to the substrate) and the other end free. The compliances which are relevant in expressing the bending distribution function of Eq. (6) are calculated as: The distribution function can be determined by applying a force at the cantilever’s free end and by calculating the maximum deflection at the same location, uz, as well as the deflection at a generic point on the cantilever, uz(x), which, by elimination of the force, results in a relationship of the type shown in Eq. (3). Another way of finding the distribution function is to apply a uniformly-distributed load along the full-length cantilever in order to express the connection of Eq. (3). The two approaches result in predictions that yield little variations – see [35], and this is particularly valid for constant cross-section members. The present work is concerned with the concentrated-force approach of determining the bending distribution function. l x2 = C x ( ) l x EI y ( x) dx l 1 Ca ( x) = x EA( x) dx l x C ( x) = x EI y ( x) dx c l x2 dx Cl = EI y ( x) 0 For a constant cross-section cantilever, the bendingrelated distribution function is simply: The compliance Cl is the linear compliance, and is calculated as the ratio between the free-end, out-of-plane deflection and the corresponding force applied at the same point about the same direction; Cl(x) is another linear compliance that is calculated as the ratio of the out-of-plane deflection at a generic point of abscissa x to the force that is applied at the cantilever free end; Cc(x), the cross compliance, is the ratio of the slope (rotation angle) of the deformed cantilever being measured at the point of abscissa x to the free-end, out-ofplane force. Ca(x), the axial compliance, represents the ratio between the axial displacement at a point of abscissa x and the axial force that would be applied at the cantilever free end. The compliances Cr(x) and Cr, which enter Eqs. (7) and (8), but which do not influence the distribution function of Eq. (6), are rotary compliances; they relate the slopes at a generic abscissa x and at x = 0 to the free-end moment My. f * ( x) = 1 3 x 1 x3 + 2 l 2 l3 (5) However, when the cantilever cross-section varies, Eq. (5) is valid as an approximation only. The procedure of determining the bending distribution function in this case still follows the approach described previously for the situation where a point load is applied about the z-direction (out of the plane) at the cantilever free end. It can be shown, see [34] for more information, that the distribution function can generically be expressed in terms of compliances as: f ( x) = Cl ( x) + E Ca ( x) xCc ( x) G Cl (6) 2.2. Model of the Circular Cantilever where E and G are the Young’s and shear modulii of the cantilever material and x is the abscissa of a generic point along the longitudinal axis of the cantilever that is measured from the free end. Eq. (6) takes into consideration that the symmetric circular cantilever is essentially a short beam (as its length – an amount less than 2R – is not 3-5 times larger than the largest cross-sectional dimension, which is the root width, equal to R). The short-beam character of this structure is modeled through the constant , which, for a rectangular cross-section, is =5/6. The compliances (or spring constants) of Eq. (6) – see [34] for more details – relate the cantilever deformations (slope and deflection) at the generic point of abscissa x to the free-end force Fz and moment My of Fig. (5) in the following manner: 0 Fz u z ( x) Cl ( x) Cc ( x) 0 M y y ( x) = Cc ( x) Cr ( x) u ( x ) 0 0 Ca ( x) Fx x Cc Cr 0 0 Fz 0 M y Ca Fx The symmetric-profile circular cantilever that is represented in Fig. (6) has been selected for modeling, microfabrication and experimental characterization. (7) Similarly, the free-end point deformations and loads are connected by the relationship: u z Cl y = Cc u 0 x (9) (8) Fig. (6). Top view of circular symmetric cantilever with geometry. Equations (4), (6) and (9) are valid for any variable crosssection cantilever which is formed of a single profile (defined by a unique geometric curve). For the symmetric circular cantilever of Fig. (6), the limit configuration occurs for 26 Micro and Nanosystems, 2009 Vol. 1, No. 1 Lobontiu et al. min = 0o and max = 180o, as indicated in Fig. (4a). It can be seen that two basic parameters fully define the planar configuration of a generic symmetric circular cantilever, as the one of Fig. (6), namely: the radius R and the minimum width wmin. Alternatively, the start and end angles min and max, as well as the length l can be used to uniquely define a circular cantilever; the latter parameters can be found from the basic ones as: 2 3R 2 2 Rwmin wmin min = cos 1 2R max = min 2 2 l = 3R 2 Rwmin wmin cromachining were utilized to produce the circular resonators. The excitation was generated by a diode laser system and the motion detection was performed by using an interferometric system - [36], the testing being performed in vacuum in order to avoid air damping losses and the corresponding inaccuracies. Figs. (8 and 10) show the experimentally-determined bending natural frequencies (resonant peaks) that have been detected for two of the fabricated specimens which have been tested. (10) The moment of inertia and cross-sectional area are variable for the cantilever configuration analyzed here, and they are expressed as: w( )t 3 I y ( ) = 12 A( ) = w( )t (11) Fig. (7). Tilted photograph of a fabricated symmetric circular nano cantilever with R = 7 m, wmin = 0.2 m and t = 225 nm. where: w( ) = wmin + 2 R (1 sin ) (12) The abscissa x can be expressed as: x= 1 2 3R 2 2 Rwmin wmin R cos 2 (13) and therefore the differential involved in all compliance integrals is: (14) dx = R sin d In working with the second derivative of the distribution function – as required by Rayleigh’s quotient of Eq. (4) – the chain rule of differentiation (Leibniz’s rule) has to be used: df d df df 1 1 df dx = d dx = d dx = R sin d d d 2x 2 d2 f d2 f 1 1 1 d f df d 2 df = 2 2 2 = 2 2 2 dx tan d d dx d R sin d dx d d Fig. (8). Experimental resonant peak for the nano cantilever of Fig. (7). (15) The exact (analytical) distribution function is not provided here as its expression is quite lengthy. Subsequent formal complications arise when expressing the out-of-plane bending resonant frequency of Eq. (4), which however results in a closed-form equation, not being furnished herein because of its exceeding length, but which is used for further analytical calculations that are reported further on. 3. FABRICATION AND EXPERIMENTAL TESTING OF CIRCULAR NANO CANTILEVERS Several circular nano cantilevers of double symmetry have been microfabricated, such as the ones photographed in Figs. (7 and 9). Low-stress silicon nitride and surface mi- Fig. (9). Tilted photograph of another fabricated symmetric circular nano cantilever with R = 7 m, w min = 1 m and t = 225 nm. Micro and Nanosystems, 2009 Vol. 1, No. 1 Circular Nano Cantilevers 27 loss mechanisms that lower the experimental natural frequency. It can also be seen that the predictions by the simplified model – Eq. (5) are always larger than the ones of the full model – Eq. (6), which is also a pertinent conclusion, as the full model will generate lower stiffnesses (through consideration of the shear effects) compared to the simplified model. Errors as large as 11.6% are registered between the two models’ results, the average relative error being 7.5%. The relative errors between the experimental data and the simplified model results can be as large as 13.5% (with a 10.5% error average), whereas the maximum error between experimental and full model data is 6.4%, with an average of 3.2%. 5. ANALYTIC MODEL SIMULATION The analytical model has further been utilized to study the relationships between the two defining planar geometric parameters, the radius R and the minimum width wmin, and the natural frequency of interest. Fig. (11) is the twodimensional plot of the out-of-plane bending natural frequency as a function of R when considering that wmin = 0.5 m, in addition to t = 225 nm, E = 160 GPa, = 2100 kg/m3 and = 0.25. As shown in Fig. (11), the natural frequency decreases non-linearly with the increase of R for constant minimum width and thickness. Fig. (10). Experimental resonant peak for the nano cantilever of Fig. (9). 4. COMPARISON OF ANALYTICAL MODEL AND EXPERIMENTATION RESULTS The analytical model predictions and the experimental results that have been obtained for several circular nano cantilevers are now being compared. Fig. (12) shows the variation of the out-of-plane bending natural frequency with wmin for a constant radius of R = 8m and all the other numerical values mentioned above. It can be seen that for the 0.1 m – 1 m range of wmin, the natural frequency increases in an almost linear fashion, whereas for wmin > 1 m, the increase of fn is nonlinear. As a combined conclusion, in order to increase the out-of-plane bending natural frequency of symmetric circular cantilevers it is necessary to decrease the circular radius R and to increase the minimum width wmin. Table 1 comprises experimental data and analytic model results of the out-of-plane bending natural frequency of several symmetric circular nano cantilever designs. The thickness of all microfabricated samples was t = 225 nm and the material properties for low-stress silicon nitride that were used for the analytic simulation are: Young’s modulus, E = 160 GPa, mass density, = 2100 kg/m3 and Poisson’s ratio = 0.25. Table 1 presents analytical results obtained both by using the simplified distribution function of Eq. (5) and the precise (full-model) one of Eq. (6) – which takes into consideration the cross-section variation and the shear effects produced by the cantilever’s short length. As Table 1 shows, the predictions by the analytical models are higher than the experimental results, and this is consistent with the various Table 1. 5. CONCLUSIONS The work introduces the new symmetric circular nano cantilever, which is defined by a constant thickness in the Experimental and Analytical Natural Frequencies (AF- Full Analytic Model Data, AS – Simplified Analytic Model Data, E – Experimental Data) Design R wmin # [μm] [μm] Resonant Frequency [MHz] Experimental Relative Errors [%] Analytic Simplified Full AF-AS E-AS E-AF 1 6 0.2 3.99 4.52 4.02 11.6 11.7 0.7 2 6 0.5 4.53 4.81 4.65 3.3 5.8 2.6 3 6 1 4.72 5.27 4.90 7.0 10.4 3.7 4 7 0.2 2.92 3.31 3.00 9.4 11.8 2.7 5 7 0.5 3.37 3.72 3.48 6.5 9.4 3.2 6 7 1 3.60 3.95 3.73 5.6 8.9 3.5 7 8 0.2 2.62 3.03 2.80 7.6 13.5 6.4 8 8 0.5 2.91 3.25 2.99 8.0 10.5 2.7 9 8 1 2.83 3.22 2.94 8.7 12.1 3.7 28 Micro and Nanosystems, 2009 Vol. 1, No. 1 Fig. (11). Natural frequency as a function of the notch radius. order of 200 nm and with planar dimensions that do not exceed 10 m. In its out-of-plane (weak-axis) bending mode vibration, the cantilever can be utilized as a dynamic transducer in atomic force microscopy, surface topology characterization or resonance-shift mass detection applications. An analytic model that gives the out-of-plane bending natural frequency is derived by taking into consideration several factors which contribute to generating an accurate model such as: the variable geometry of the planar profile, the distributed stiffness and inertia properties (by means of a precise deflection distribution function), and the inherent shortbeam nature of this cantilever design together with the associated shear deformations. Silicon nitride nano cantilevers have been surface-micromachined and subsequently tested in a vacuum environment by applying laser excitation and interferometric detection of the out-of-plane bending resonant response. 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