FAPAS Proficiency Testing Programme 2015-16 Contents FAPAS® Proficiency Tests 2 4 Nutritional Analysis 5 Nutritional Components 5 Nutritional Components (continued) 6 Nutritional Elements 7 Vitamins 8 Oils & Fats 9 Oils & Fats (continued) 10 Food Ingredients 11 Food Ingredients (continued) 12 Alcoholic Drinks, Fruit Juice & Soft Drinks 13 Alcoholic Drinks, Fruit Juice & Soft Drinks (continued) 14 Honey 15 Feeding Stuffs 16 Authenticity 17 Allergens 18 Allergens (continued) 19 Migration – Overall & Specific 20 Environmental Contaminants 21 Acrylamide, Furan, 3-MCPD, Melamine 22 Nitrate & Nitrite 23 Veterinary Drug Residues 24 Veterinary Drug Residues (continued) 25 Veterinary Drug Category List 26 Mycotoxins – Aflatoxins & Multi-Mycotoxins 27 Mycotoxins – Aflatoxins & Multi-Mycotoxins (continued) 28 Mycotoxins – Patulin 29 Mycotoxins – Ochratoxin A 30 Mycotoxins – Fusarium Toxins / Plant Toxins 31 Metallic Contaminants 32 Metallic Contaminants (continued) 33 Pesticide Residues – Animal Products / Fats and Oils 34 Potential Pesticide Residues and PCBs – List 1 35 Potential Pesticide Residues – List 2 35 Pesticide Residues – Cereals 36 Potential Pesticide Residues – List 3 37 Pesticide Residues – Fresh Fruits, Vegetables, Tea & Herbs 38 Pesticide Residues – Fresh Fruits, Vegetables, Tea & Herbs (continued) 39 Potential Pesticide Residues – List 4 40 Potential Pesticide Residues – List 5, List 6 41 Prices Technical Information 3 42-44 45 Protocols 45 Other technical documents 45 ISO Accreditation 45 FAPAS FAPAS® Proficiency Tests Proficiency Testing in Food Chemistry FAPAS® is an internationally recognised provider of proficiency testing schemes in food chemistry. The scheme has more than 2000 participants in over 90 countries. FAPAS® gives you essential performance data over time, building into a valuable quality control asset. FAPAS® covers chemical analysis of real food samples for a wide range of target analytes including: nutritional components, additives, natural contaminants, pesticide and veterinary medicine residues, and chemical migrants. Participation can be at a level that suits your business – from taking part in one of our scheduled tests through to company-specific closed tests. Quality control materials are available for your own quality checks or for training purposes. Results from each proficiency test receive rigorous statistical analysis, ensuring you have clear feedback on your performance. Comprehensive reports provide information on analytical methods used by other participants. We can provide problem-solving consultancy on your laboratory procedures if required. Participation in FAPAS is easy. Arrangements can be made through our network of agents, or via our website, www.fapas.com. FAPAS follows international guidelines for proficiency testing and is accredited by UKAS to ISO/IEC 17043. 4 FAPAS Nutritional Analysis As nutritional legislation increases, the proficiency of laboratories to provide accurate results to food manufacturers for labelling is critical, to help consumers make informed choices about the food they eat. FAPAS® offers the widest range of analyte/matrix PT combinations for the food sector. Nutritional Components dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 01/04/2015 25130 corn/maize snack food moisture, ash, total fat, nitrogen, sodium & chloride 50 g 16/04/2015 01100 canned meat moisture, ash, total fat, nitrogen, sodium & chloride 150 g 29/04/2015 2461 wheat flour moisture at 130°C, ash, nitrogen & total dietary fibre by AOAC 150 g 26/05/2015 25131 fish paste moisture, ash, total fat, nitrogen, sodium & chloride 150 g 17/06/2015 01101 canned meat meal moisture, ash, total fat, nitrogen, sodium & chloride 150 g 19/06/2015 25132 canned fish total volatile basic nitrogen (TVB-N) 150 g 25/06/2015 2462 porridge oats moisture at 130°C, ash, total fat, nitrogen & total dietary fibre by AOAC 150 g 15/07/2015 01102 canned meat moisture, ash, total fat, nitrogen & hydroxyproline 150 g 30/07/2015 25133 condensed milk moisture, ash, total fat, nitrogen & total sugars 150 ml 11/09/2015 01103 canned meat meal total fat, saturated fatty acids, protein, total sugars & salt 150 g 18/09/2015 25134 milkshake powder fructose, galactose, glucose, lactose, maltose & sucrose 50 g Footnotes total sugars = that measured by a defined titration method (e.g. Lane-Eynon, Luff-Schoorl, Munson Walker) or, if measured by HPLC, the sum of fructose, glucose, sucrose, lactose, galactose and maltose (NB not all sugars may be present). 5 FAPAS Nutritional Components (continued) dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 24/09/2015 2463 cereal moisture at 130°C, ash, nitrogen & total dietary fibre by AOAC 150 g 20/10/2015 25135 chocolate moisture, total fat, nitrogen, butyric acid, lactose & sucrose 150 g 18/11/2015 01104 canned meat moisture, ash, total fat, nitrogen & hydroxyproline 150 g 11/12/2015 25136 milk powder moisture, ash, total fat, nitrogen, titratable acidity & lactose 50 g 13/01/2016 01105 canned meat meal moisture, ash, total fat, nitrogen, sodium, chloride & total sugars 150 g 14/01/2016 2464 breadcrumbs moisture, ash, nitrogen, starch, sodium & total dietary fibre by AOAC 150 g 20/01/2016 25137 infant formula moisture, ash, total fat, nitrogen & lactose 50 g 11/02/2016 25138 cheese & pasta meal moisture, ash, total fat, nitrogen, sodium & chloride 100 g 23/02/2016 25139 butter moisture, total fat, non-fat solids, pH & chloride 200 g 02/03/2016 2465 biscuit (cookie) moisture at 130°C, ash, total fat, nitrogen & total dietary fibre by AOAC 150 g 18/03/2016 25140 canned fish total volatile basic nitrogen (TVB-N) 150 g 23/03/2016 01106 canned meat moisture, ash, total fat, nitrogen, sodium & chloride 150 g F F Footnotes F test incurs courier charges 6 FAPAS Nutritional Elements dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 24/04/2015 1879 canned meat calcium, phosphorus & zinc 150 g 13/08/2015 1880 breakfast cereal calcium, iron, magnesium, phosphorus, potassium, sodium & zinc 50 g 19/11/2015 1881 milk powder calcium, iodine, magnesium, phosphorus, potassium, selenium & sodium 50 g 23/02/2016 1882 nutritional supplement copper, manganese, magnesium, potassium & zinc 30 ml F Footnotes F test incurs courier charges 7 FAPAS Vitamins dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 13/05/2015 2191 breakfast cereal vitamins B1, B2 (total), B6, total niacin & folic acid 50 g Ff fruit purée vitamin C 100 ml F 28/07/2015 2192 09/11/2015 2193 liquid vitamin supplement vitamins B1, B2 (total) & B6 40 ml 15/01/2016 2194 milk powder vitamins A & D3 50 g 11/03/2016 2195 powdered baby food vitamins A, B12, C & E 100 g Footnotes F test incurs courier charges f test has a shortened timescale 8 FAPAS Oils & Fats The rancidity of fats and oils is determined by the level of oxidation in a sample. There are various forms of rancidity testing which are tested through the FAPAS® range of proficiency tests. Testing is important to demonstrate the quality and shelf life of a product. dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 15/04/2015 14144 edible oil saturates, mono-unsaturates & poly-unsaturates 30 ml 01/05/2015 14145 infant formula (may contain LC-PUFAs) total fat, saturates, mono-unsaturates, poly-unsaturates, total trans fatty acids (& possibly individual fatty acids: linoleic acid, a-linolenic acid (ALA), ARA & DHA ) 50 g Ff olive oil peroxide value, acidity, anisidine value & iodine value 100 ml F mixed fat spread total fat, saturates, mono-unsaturates, poly-unsaturates & total trans fatty acids 50 g Ff olive oil peroxide value, acidity, K232 & K270 100 ml F 01/06/2015 14146 11/08/2015 14147 17/08/2015 14148 28/09/2015 14149 mixed fat spread (may contain LC-PUFAs) saturates, mono-unsaturates, poly-unsaturates, total trans fatty acids, total omega-3 & total omega-6 series fatty acids, (& possibly individual omega-3 & omega-6 fatty acids) 50 g 15/10/2015 14150 vegetable oil saturates, mono-unsaturates & poly-unsaturates & limited fatty acid profile 30 ml 24/11/2015 14151 mixed fat spread total fat, butyric acid & cholesterol 50 g 14/12/2015 14152 fish oil omega-3 & omega-6 series fatty acids 30 ml olive oil peroxide value, acidity, anisidine value & iodine value 100 ml 05/01/2016 F Ff 14153 Footnotes F test incurs courier charges f test has a shortened timescale 9 FAPAS Oils & Fats (continued) dispatch date dd/mm/yyyy test details code matrix analyte approximate quantity Ff biscuit (cookie) saturates, mono-unsaturates & poly-unsaturates, total trans fatty acids & butyric acid 50 g Ff olive oil peroxide value, acidity, K232 & K270 100 ml 15/02/2016 14154 08/03/2016 14155 Footnotes F test incurs courier charges f test has a shortened timescale 10 FAPAS Food Ingredients dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 22/04/2015 20116 tomato sauce brix, pH, total acidity, sodium, chloride & benzoic acid 150 g 18/05/2015 20117 meat sulphur dioxide 100 g 10/06/2015 20118 jam brix, pH, benzoic acid, citric acid & sorbic acid 70 g 31/07/2015 20119 chocolate cake mix caffeine, sorbic acid, theobromine & total sugars (expressed as sucrose) 50 g 24/08/2015 20120 F dried apricot (water/fruit slurry) sulphur dioxide 100 g 21/10/2015 20121 § sugar confectionary (boiled sweets) permitted colours up to 4 selected from the following list: Allura Red, Brilliant Blue FCF, Carmoisine, Erythrosine, Green S, Indigo Carmine, Patent Blue V, Ponceau 4R, Quinoline Yellow, Sunset Yellow FCF, Tartrazine 50 g 25/11/2015 20122 oil antioxidants: total BHA (E320), BHT (E321) & propyl gallate (E310) 50 ml F Footnotes F test incurs courier charges total sugars = that measured by a defined titration method (e.g. Lane-Eynon, Luff-Schoorl, Munson Walker) or, if measured by HPLC, the sum of fructose, glucose, sucrose, lactose, galactose and maltose (NB not all sugars may be present) § both qualitative & quantitative results can be submitted 11 FAPAS Food Ingredients (continued) dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 14/12/2015 20123 F dried apple (water/fruit slurry) sulphur dioxide 100 g 03/03/2016 20124 § hot pepper sauce (or similar) non-permitted colours (illegal dyes) high level, up to 4 selected from the following list: Butter Yellow (Dimethyl Yellow), Orange II, Para Red, Rhodamine B, Sudan I, Sudan II, Sudan III, Sudan IV, Sudan Black B, Sudan Orange G, Sudan Red B, Sudan Red 7B, Sudan Red G, Toluidine Red 50 ml Footnotes F test incurs courier charges § both qualitative & quantitative results can be submitted 12 FAPAS Alcoholic Drinks, Fruit Juice & Soft Drinks Drinks contain a variety of additives used to enhance flavour, shelf life or nutritional composition. Some additives are undesirable, including artificial colours, excess sugar or processing by-products. These proficiency tests support analyses carried out by the drinks industry and regulators. dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 13/05/2015 1374 whisky alcoholic strength, ethanal (acetaldehyde), ethyl acetate, methanol, propan-1-ol, 2-methylpropanol & 2methylbutanol + 3-methylbutanol (sum) 200 ml 15/05/2015 0856 apple juice brix, pH, total acidity, total sugars, magnesium, potassium & sodium 250 ml 28/05/2015 03122 cola drink benzoic acid, caffeine, acesulfame-K & saccharin 150 ml 10/07/2015 03123 ground coffee caffeine (2 test materials supplied ,one regular, one decaffeinated) 2 x 30 g 14/08/2015 03124 soft drink brix, pH, citric acid, sorbic acid, cyclamate, saccharin & benzoic acid 150 ml 09/09/2015 0857 orange juice brix, pH, citric acid, fructose, glucose, sucrose & total sugars 250 ml 14/10/2015 1375 brandy alcoholic strength, butan-1-ol, ethanal (acetaldehyde), ethyl acetate, methanol, propan-1-ol, 2-methylpropanol & 2methylbutanol + 3-methylbutanol (sum) & ethyl carbamate 200 ml 16/10/2015 03125 soft drink up to 4 colours from the following list: Allura Red, Brilliant Blue FCF, Carmoisine, Erythrosine, Green S, Indigo Carmine, Patent Blue V, Ponceau 4R, Quinoline Yellow, Sunset Yellow FCF, Tartrazine 150 ml § Footnotes total sugars = that measured by a defined titration method (e.g. Lane-Eynon, Luff-Schoorl, Munson Walker) or, if measured by HPLC, the sum of fructose, glucose, sucrose, lactose, galactose and maltose (NB not all sugars may be present) 13 FAPAS Alcoholic Drinks, Fruit Juice & Soft Drinks (continued) dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 03/12/2015 03126 cola drink caffeine, benzoic acid, total sugars & phosphoric acid (as P2O5) 150 ml 14/01/2016 0858 grapefruit juice brix, pH, total acidity, total sugars, calcium, magnesium & potassium 250 ml 22/01/2016 1376 wine alcoholic strength, total SO2, total acidity & volatile acidity 220 ml 12/02/2016 03127 tonic water benzoic acid, quinine, acesulfame-K & aspartame 150 ml 02/03/2016 0859 cranberry juice brix, pH, total acidity, total sugars, phosphorus & potassium 250 ml 03/03/2016 03128 soft drink sweeteners: acesulfame-K, aspartame, cyclamate, steviol glycosides (E960) & saccharin 150 ml Footnotes total sugars = that measured by a defined titration method (e.g. Lane-Eynon, Luff-Schoorl, Munson Walker) or, if measured by HPLC, the sum of fructose, glucose, sucrose, lactose, galactose and maltose (NB not all sugars may be present) 14 FAPAS Honey Honey intended for human consumption must meet a specific composition detailed in the EU Honey Directive. The analytes listed below are important determinands in evaluating the quality of honey. dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 30/06/2015 2831 F honey moisture, fructose, glucose, sucrose, hydroxymethylfurfural (HMF) & diastase 100 g 16/11/2015 2832 honey fructose, glucose, sucrose, hydroxymethylfurfural (HMF), diastase, electrical conductivity & pH 100 g 01/03/2016 2833 honey moisture, fructose, glucose, sucrose, hydroxymethylfurfural (HMF), diastase, free acid & water-insoluble solids 100 g F F A Footnotes F test incurs courier charges A this test material may be adulterated honey 15 FAPAS Feeding Stuffs Please note that there are other proficiency tests in the Programme with animal feed as the matrix: 3058, 02280, 04265, 04272, 04275, 17159, 22125 & 22128. dispatch date 16 test details dd/mm/yyyy code matrix analyte approximate quantity 22/05/2015 10125 dairy ration moisture, ash, total oil, protein, crude fibre, iron, lead, magnesium, manganese & selenium 225 g 09/07/2015 10126 sheep feed moisture, ash, total oil, protein & copper 150 g 17/09/2015 10127 pig ration moisture, ash, total oil, protein, crude fibre, aNDF, vitamin E & zinc 150 g 04/12/2015 10128 poultry ration moisture, ash, total oil, protein, crude fibre, starch, total sugars, calcium & phosphorus 225 g 24/02/2016 10129 premix calcium, magnesium, manganese, phosphorus, sodium & zinc 150 g 24/02/2016 10130 premix vitamin A, D3 & E 150 g 23/03/2016 10131 soya bean meal (extracted) moisture, ash, protein, total oil & crude fibre 150 g FAPAS Authenticity With food authenticity under the spotlight, consumers are demanding assurance that their food is what it says it is. Is that burger really beef? The ability to determine the authenticity of foods can prevent mislabelling, substitution of cheaper ingredients, and adulteration. All of which are risks in the supply chain. All of the meat based authenticity tests are qualitative tests (presence/absence) to determine whether adulteration/contamination of any other species has occurred. dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 08/04/2015 2963 D chicken one or more from: beef, lamb, pork or turkey 30 g 16/07/2015 2964 D lamb one or more from: beef, chicken, goat or pork 30 g 26/10/2015 2965 F fish identification of unknown fish (3 samples) selected from the following list: Gadus macrocephalus, (Telesius 1810) Gadus morhua, (Linnaeus 1758) Hippoglossus hippoglossus, (Linnaeus 1758) Limanda limanda, (Linnaeus 1758) Melanogrammus aeglefinus, (Linnaeus 1758) Merlangius merlangus, (Linnaeus 1758) Merluccius merluccius, (Linnaeus 1758) Pangasius hypophthalmus, (Sauvage 1878) Pleuronectes platessa, (Linnaeus 1758) Pollachius virens, (Linnaeus 1758) Theragra chalcogramma, (Pallas 1814) 3 x 10 g 10/02/2016 2966 D beef one or more from: chicken, horse, lamb or pork 30 g Footnotes D freeze dried matrix, to be reconstituted (by participants) prior to testing F test incurs courier charges 17 FAPAS Allergens As the number of people with life-threatening allergies increases and international legislation on allergen management increases, the requirement to demonstrate your allergen testing capabilities increases. Testing for food allergens is essential for protecting consumers and verifying the allergen status of food ingredients and products. dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 01/04/2015 27153 § infant soya formula milk (casein) 2 x 20 g § 23/04/2015 27154 cake mix egg, egg white protein 2 x 20 g 06/05/2015 27155 canned fish histamine (high level, >50 mg/kg) 145 g 29/05/2015 27156 infant soya formula gluten 2 x 20 g 26/06/2015 27157 instant soup powder celery, mustard 2 x 20 g 24/07/2015 27158 § chocolate peanut, peanut protein 2 x 20 g § infant soya formula milk (BLG) 2 x 20 g § 07/08/2015 § ♦ 27159 26/08/2015 27160 cake mix gluten 2 x 20 g 10/09/2015 27161 canned fish histamine (low level, <50 mg/kg) 145 g 30/09/2015 27162 § chocolate hazelnut, hazelnut protein 2 x 20 g 26/10/2015 27163 F jam sulphites 20 g ‡ cake mix gluten, milk and egg 30 g § wheat flour soya, soya protein 2 x 20 g 13/11/2015 03/12/2015 27164 27165 Footnotes § two test materials supplied and both qualitative & quantitative results can be submitted ♦ qualitative assessment only F test incurs courier charges ‡ both qualitative & quantitative results can be submitted 18 FAPAS Allergens (continued) dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 06/01/2016 27166 chocolate contamination (presence/absence) of matrix with one or more from the following list: Almond, (Amygdalus communis L.) Hazelnut, (Corylus avellana) Walnut, (Juglans regia) Cashew, (Anacardium occidentale) Pecan nut, (Carya illinoinensis (Wangenh.) K. Koch)) Brazil nut, (Bertholletia excelsa) Pistachio nut, (Pistacia vera) Macadamia/Queensland nut, (Macadamia ternifolia) Peanut, (Arachis hypogaea) 50 g 27/01/2016 27167 canned fish histamine (high level >50 mg/kg) 145 g 17/02/2016 27168 § oat based foodstuff gluten 2 x 20 g 16/03/2016 27169 § chocolate almond, almond protein 2 x 20 g flour lupin 2 x 20 g cooked biscuit hazelnut, peanut 50 g 17/03/2016 30/03/2016 ♦ ♦ 27170 ‡ 27171 Footnotes ♦ qualitative assessment only § two test materials supplied and both qualitative & quantitative results can be submitted ‡ both qualitative & quantitative results can be submitted 19 FAPAS Migration – Overall & Specific Foods are packaged in materials intended to protect the product, increase its shelf life and make it more attractive to the consumer. Those same packaging materials, however, could actually leach undesirable chemicals into the food. Bisphenol A has received a lot of media attention due to its presence in products intended for use by infants. dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 23/04/2015 1268 food simulant (oil) phthalates 2 x 50 ml 30/04/2015 1150 nylon film overall migration into ethanol by total immersion 40 cm x 22 cm 15/07/2015 1269 food simulant (3% w/v acetic acid in water) melamine 50 ml 06/08/2015 1270 food simulant (50% w/v ethanol) bisphenol A 50 ml 25/09/2015 1271 food simulant (3% w/v acetic acid in water) formaldehyde 50 ml 28/10/2015 1151 plastic film overall migration into olive oil by total immersion 40 cm x 22 cm 20/11/2015 1272 food simulant (3% w/v acetic acid in water) total primary aromatic amines >300 ml B Footnotes B includes blank matrix 20 FAPAS Environmental Contaminants The occurrence of Polycyclic Aromatic Hydrocarbons (PAHs) in foodstuffs is a major source of exposure to these carcinogenic compounds for humans. Given the risk to human health from PAHs in food, the European Commission established maximum levels for PAHs and identified a group of 4 PAHs as indicators based on occurrence and toxicity in EC 1881/2006. These include benzo[a]pyrene (BaP), benz[a]anthracene (BaA), benzo[b]fluoranthene (BbF) and chrysene (CHR). dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 29/04/2015 0662 palm oil PAHs (including PAH4 sum) 30 ml 08/07/2015 0663 cocoa butter PAHs (including PAH4 sum) 50 g 27/10/2015 F 0664 smoked fish product PAHs (including PAH4 sum) 50 g 15/12/2015 0665 olive oil all 16 EU priority PAHs (including PAH4 sum) 30 ml Footnotes F test incurs courier charges 21 FAPAS Acrylamide, Furan, 3-MCPD, Melamine Industrial chemicals such as acrylamide and melamine are known to be harmful to human health if consumed and are strictly regulated. There have been cases of adulteration where melamine has been added to food to artificially increase its apparent protein content. Therefore, the ability to accurately measure its presence is important to retailers and consumers. dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 08/04/2015 3055 milk powder melamine & cyanuric acid (> 5 mg/kg) 50 g 21/05/2015 3056 crispbread acrylamide 50 g 12/06/2015 2645 soy sauce 3-MCPD & 1,3-DCP 40 g 06/08/2015 3057 potato crisps acrylamide 50 g 23/09/2015 2646 vegetable oil ester bound 3-MCPD & glycidol 50 ml 14/10/2015 3058 animal feed melamine & cyanuric acid 50 g 25/11/2015 3059 biscuit (cookie) acrylamide 50 g 13/01/2016 3060 milk powder melamine & cyanuric acid (low levels, <5 mg/kg) 50 g 04/02/2016 3061 coffee acrylamide 50 g 04/03/2016 2647 soy sauce 3-MCPD & 1,3-DCP 40 g coffee furan 50 g 07/03/2016 Ff 3062 Footnotes F test incurs courier charges f test has a shortened timescale 22 FAPAS Nitrate & Nitrite These are chemicals used in fertilisers and as food preservatives and are often detected in contaminated drinking water, cured meat products as well as in fruit and vegetables. Exposure at high levels can result in severe health issues particularly with infants, where they can be exposed through drinking water in infant formula. dispatch date dd/mm/yyyy 02/04/2015 test details code matrix analyte approximate quantity meat nitrate as NaNO3 & nitrite as NaNO2 25 g milk powder nitrate as NaNO3 & nitrite as NaNO2 (high level) 40 g F cabbage purée nitrate 70 g F lettuce purée nitrate 70 g DDf meat nitrate as NaNO3 & nitrite as NaNO2 25 g F rocket (rucola) purée nitrate 70 g F meat nitrate as NaNO3 & nitrite as NaNO2 25 g DDf spinach purée nitrate 70 g DDf 15103 28/05/2015 15104f 28/07/2015 15105 01/09/2015 15106 23/10/2015 15107 03/11/2015 15108 06/01/2016 15109 14/03/2016 15110 Footnotes DD freeze dried matrix, not to be reconstituted (by participants) prior to testing f test has a shortened timescale F test incurs courier charges 23 FAPAS Veterinary Drug Residues Veterinary drugs are frequently used to treat disease and promote healthy livestock to improve the quality or yield of meat and animal products. This introduces the risk of veterinary drug residues and their metabolites entering the food chain if they persist in the animal products and their presence is tightly regulated. We intend to use material containing incurred residues wherever possible. Refer to the list on page 18 for details of potential residues in tests where only general categories are stated. dispatch date dd/mm/yyyy test details code matrix analyte approximate quantity 21/04/2015 02262 Ff fish muscle (oily fish) leucomalachite green & total malachite green 20 g 15/06/2015 02263Ff# bovine liver avermectins 20 g 23/06/2015 02264Ff# fish muscle quinolones & fluoroquinolones 20 g 20/07/2015 02265F honey chloramphenicol 20 g 20/07/2015 02266F# honey sulfonamides 20 g 27/07/2015 02267Ff# chicken eggs coccidiostats 20 g 27/07/2015 02268Ff# chicken eggs nitroimidazoles 20 g 04/08/2015 02269Ff# chicken eggs nitrofuran metabolites 20 g 18/08/2015 02270F# honey tetracyclines 20 g 14/09/2015 02271Ff# pig liver β-agonists 20 g 14/09/2015 02272Ff bovine milk chloramphenicol & thiamphenicol 25 ml 22/09/2015 02273Ff# fish muscle illegal dyes (veterinary drugs) 20 g 28/09/2015 02274Ff# bovine milk NSAIDs (nonsteroidal anti-inflammatory drugs) 20 ml 13/10/2015 02275Ff# bovine urine synthetic hormones 25 ml Footnotes F test incurs courier charges f test has a shortened timescale # test includes identification and quantification of analytes 24 FAPAS Veterinary Drug Residues (continued) dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 11/11/2015 02276F# honey quinolones & fluoroquinolones & macrolides 40 g 11/11/2015 02277F# honey nitrofuran metabolites 20 g 16/11/2015 02278 Ff pig kidney antimicrobial screen (presence/absence) 5 x 20 g 08/12/2015 02279Ff# bovine milk β-lactams (penicillins & cephalosporins) 25 ml 08/12/2015 02280# animal feed coccidiostats (carry-over concentrations) 50 g 04/01/2016 02281Ff# pig kidney sulphonamides 20 g 04/01/2016 02282Ff# pig kidney tetracyclines 20 g 26/01/2016 02283Ff# prawns nitrofuran metabolites 20 g 09/02/2016 02284Ff fish muscle chloramphenicol 20 g 15/02/2016 02285Ff# chicken eggs quinolones & fluoroquinolones & macrolides 40 g 14/03/2016 02286Ff turkey muscle chlortetracycline 20 g 14/03/2016 02287Ff# prawns tetracyclines 20 g Footnotes F test incurs courier charges # test includes identification and quantification of analytes f test has a shortened timescale 25 FAPAS Veterinary Drug Category List Potential veterinary drug residues in tests where only general categories are stated. β-agonists bromobuterol, cimaterol, cimbuterol, clenbuterol, clenpenterol , clenproperol, hydroxyclenbuterol, mabuterol, mapenterol, ractopamine, salbutamol, salmeterol, terbutaline, tulobuterol, zilpaterol avermectins abamectin, doramectin, emamectin, eprinomectin, ivermectin, moxidectin cephalosporins cefalexin, cefalonium, cefapirin, desacetylcefapirin, cefazolin, cefoperazone, cefquinome coccidiostats clopidol, decoquinate,diclazuril, , DNC, halofuginone, lasalocid, maduramycin, monensin, narasinrobenidine, salinomycin, semduramycin, toltrazuril sulfone illegal dyes (veterinary drugs) malachite green, leucomalachite green, total malachite green, crystal violet, leucocrystal violet, total crystal violet, brilliant green macrolides erythromycin, josamycin, lincomycin, oleandamycin, rifampicin, spiramycin, tilmicosin, tylosin A, tylosin B, virginiamycin nitrofuran metabolites AHD (bound), AHD (total), AOZ (bound), AOZ (total), AMOZ (bound), AMOZ (total), SEM (bound), SEM (total) nitroimidazoles dimetridazole, 2-hydroxydimetridazole, ipronidazole, 2-hydroxyipronidazole, metronidazole, 2-hydroxymetronidazole, ronidazole nonsteroidal anti-inflammatory diclofenac, 5-hydroxyflunixin, ibuprofen, meloxicam, naproxen, phenylbutazone drugs (NSAIDs) penicillins amoxicillin, ampicillin, benzylpenicillin (Penicillin G), Penicillin V, cloxacillin, dicloxacillin, nafpicillin, oxacillin quinolones & fluoroquinolones flumequine, nalidixic acid, oxolinic acid, ciprofloxacin, danofloxacin, difloxacin, enrofloxacin, marbofloxacin, norfloxacin, sarafloxacin sulfonamides sulfachloropyridazine, sulfadiazine, sulfadimethoxine, sulfadimidine (sulfamethazine), sulfadoxine, sulfaguanadine, sulfamerazine, sulfamethizole, sulfamethoxazole, sulfamethoxypyridazine, sulfamonomethoxine, sulfamoxole, sulfanilamide, sulfapyridine, sulfaquinoxaline, sulfathiazole, sulfisoxazole synthetic hormones α-boldenone, methylboldenone, diethylstilbestrol (DES), dienestrol, hexoestrol, methyltestosterone, α-nortestosterone, stanozolol, 16β-hydroxystanozolol, trenbolone, zeranol tetracyclines chlortetracycline (total), doxycycline, oxytetracycline (total), tetracycline (total) 26 FAPAS Mycotoxins – Aflatoxins & Multi-Mycotoxins Mycotoxins are toxic secondary metabolites produced by fungi on agricultural commodities in the field or during storage. It is estimated that 25% of the world’s food crops are affected, resulting in large commercial losses. FAPAS® has introduced multi-mycotoxin proficiency tests as well as those for emerging mycotoxins. Mycotoxins – Aflatoxins & Multi-Mycotoxins dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 09/04/2015 04260 maize aflatoxin B1 &/or total, DON, ZON & OTA 150 g 01/05/2015 04261 maize aflatoxins B & G &/or total 55 g F 05/05/2015 04262 pistachio (water/nut slurry) aflatoxins B & G &/or total 100 g 20/05/2015 04263 milk powder aflatoxin M1 55 g 04/06/2015 04264 chilli powder aflatoxins B & G &/or total 55 g 19/06/2015 04265 animal feed (cereal based) aflatoxins B & G &/or total 55 g 14/07/2015 04266 peanut (water/nut slurry) aflatoxins B & G &/or total 100 g 23/07/2015 04267 infant food contamination of matrix with two or more from the following list: aflatoxins B & G &/or total, OTA, ZON, DON, FB1 & FB2 & total fumonisins (as a sum of FB1 & FB2) & T-2 & HT-2 toxins & as sum of T-2 & HT-2 toxins 200 g 04/08/2015 04268 almond (water/nut slurry) aflatoxins B & G &/or total 100 g 21/08/2015 04269 maize aflatoxin B1, DON, ZON, OTA, FB1 & FB2 & total fumonisins (as a sum of FB1 & FB2), T-2 & HT-2 toxins & as sum of T-2 & HT-2 toxins 200 g 02/09/2015 04270 milk powder aflatoxin M1 55 g F F Footnotes F test incurs courier charges 27 FAPAS Mycotoxins – Aflatoxins & Multi-Mycotoxins (continued) dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 29/09/2015 04271 hazelnut (water/nut slurry) aflatoxins B & G &/or total 100 g 09/10/2015 04272 animal feed (cereal based) contamination of matrix with two or more from the following list: aflatoxin B1, OTA, ZON, DON, FB1 & FB2 & total fumonisins (as a sum of FB1 & FB2) 200 g 22/10/2015 04273 maize aflatoxins B & G &/or total 55 g 06/11/2015 04274 chilli powder aflatoxins B & G &/or total & OTA 100 g 26/11/2015 04275 animal feed (cereal based) aflatoxins B & G &/or total 55 g 09/12/2015 04276 maize aflatoxin B1, DON, ZON & OTA 150 g 20/01/2016 04277 rice aflatoxins B & G &/or total 55 g 03/02/2016 04278 peanut flour aflatoxins B & G &/or total 55 g 17/02/2016 04279 paprika aflatoxins B & G &/or total & OTA 100 g 01/03/2016 04280 dried figs (water/fruit slurry) aflatoxins B & G &/or total & OTA 150 g 18/03/2016 04281 milk powder aflatoxin M1 55 g F F Footnotes F test incurs courier charges 28 FAPAS Mycotoxins – Patulin dispatch date test details dd/mm/yyyy code 29/06/2015 1656 21/09/2015 1657 08/02/2016 matrix analyte approximate quantity F apple juice (clear) patulin 50 ml F apple purée patulin 60 g F apple juice (cloudy) patulin 50 ml 1658 Footnotes F test incurs courier charges 29 FAPAS Mycotoxins – Ochratoxin A dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 06/05/2015 17149 wheat flour ochratoxin A 55 g 01/06/2015 17150 dried vine fruit (raisin) (water/fruit slurry) ochratoxin A 100 g 08/07/2015 17151 barley flour ochratoxin A 55 g 12/08/2015 17152 green coffee ochratoxin A 55 g 16/09/2015 17153 paprika ochratoxin A 55 g 29/10/2015 17154 instant coffee ochratoxin A 55 g 06/11/2015 17155 cocoa ochratoxin A 55 g 09/12/2015 17156 wine ochratoxin A 55 ml 08/01/2016 17157 maize flour ochratoxin A 55 g 05/02/2016 17158 roasted coffee ochratoxin A 55 g 05/02/2016 17159 animal feed ochratoxin A 55 g 10/03/2016 17160 grain (as flour) ochratoxin A & citrinin 100 g F Footnotes F test incurs courier charges 30 FAPAS Mycotoxins – Fusarium Toxins / Plant Toxins dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 17/04/2015 22119 maize flour deoxynivalenol (DON) 55 g 17/04/2015 22120 infant food deoxynivalenol (DON) 55 g 03/06/2015 22121 breakfast cereal deoxynivalenol (DON) & zearalenone (ZON) 100 g 16/07/2015 22122 oat flour T-2 & HT-2 toxins & as a sum of T-2 & HT-2 toxins 55 g 27/08/2015 22123 maize flour FB1 & FB2 and total fumonisins (as a sum of FB1 & FB2) 55 g 07/10/2015 22124 maize flour trichothecenes: nivalenol, DON, 3 Ac DON, 15 Ac DON, T-2 & HT-2 toxins & as a sum of T-2 & HT-2 toxins 150 g 04/11/2015 22125 animal feed deoxynivalenol (DON) & zearalenone (ZON) 100 g 07/01/2016 22126 rye flour ergot alkaloids: contamination of matrix with two or more from ergometrine, ergotamine, ergosine, ergocristine, ergocryptine & ergocornine & their related-inines 55 g 15/01/2016 22127 wheat flour deoxynivalenol (DON) & zearalenone (ZON) 100 g 12/02/2016 22128 animal feed T-2 & HT-2 toxins & as a sum of T-2 & HT-2 toxins 55 g 08/03/2016 22129 herbal tea pyrrolizidine alkaloids 25 g 30/03/2016 22130 biscuit (cookies) deoxynivalenol (DON) & zearalenone (ZON) 100 g F Footnotes F test incurs courier charges 31 FAPAS Metallic Contaminants The presence of metals such as arsenic, cadmium, lead and mercury in food is of particular concern due to their toxicity. These naturally occurring chemicals can occur as residues in food by a range of mechanisms such as their natural presence in the environment or contamination during food processing and storage. Their accumulation in the body can lead to harmful effects over time and their presence in foodstuffs is strictly regulated. dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 02/04/2015 07233 milk powder arsenic (total), cadmium, lead & mercury (total) (all natural/low levels) 50 g 22/04/2015 07234 soft drink antimony, arsenic (total), cadmium, chromium, copper & zinc (all high levels) 50 ml 14/05/2015 07235 canned crab meat arsenic (total), arsenic (inorganic), cadmium & mercury (total) (all natural levels) 150 g 02/06/2015 07236 tomato paste cadmium, iron, lead & tin (all high levels) 50 g 01/07/2015 07237 canned fish arsenic (total), cadmium & mercury (total) (all natural levels) 150 g 22/07/2015 07238 infant formula aluminium, cadmium, chromium, iodine, molybdenum & selenium (all natural/low levels) 50 g 05/08/2015 07239 chilli powder arsenic (total), cadmium & lead (all high levels) 50 g 19/08/2015 07240 chilli sugar paste lead 25 g 19/08/2015 07241 powdered brown rice arsenic (inorganic), arsenic (total), cadmium, lead & mercury (total) (natural/low levels) 50 g 02/09/2015 07242 edible oil arsenic (total), copper, iron & lead (all high levels) 50 ml F Footnotes F test incurs courier charges 32 FAPAS Metallic Contaminants (continued) dispatch date dd/mm/yyyy 23/09/2015 test details code DD 07243 matrix analyte approximate quantity offal (liver) arsenic (total), cadmium, lead & mercury (total) (all high levels) 50 g 08/10/2015 07244 milk powder arsenic (total), cadmium, lead & mercury (total) (all natural/low levels) 50 g 29/10/2015 07245 infant cereal cadmium, chromium, lead, mercury (total) & selenium (all natural/low levels) 50 g 12/11/2015 07246 wine pH, cadmium, copper & lead 50 ml 26/11/2015 07247 canned fish arsenic (total), cadmium, mercury (total) (all natural levels) 150 g 10/12/2015 07248 soya flour aluminium, arsenic (total), cadmium, lead & mercury (total) (all high levels) 50 g 11/01/2016 07249 fruit juice cadmium, iron, lead, & tin (all high levels) 50 ml 21/01/2016 07250 chocolate cadmium & lead 50 g 16/02/2016 07251 vegetable purée cadmium, lead & tin (all high levels) 50 g 25/02/2016 07252 powdered rice arsenic (inorganic), arsenic (total),cadmium, lead & mercury (total) (all high levels) 50 g 09/03/2016 07253 canned fish arsenic (total), mercury (total) & methyl mercury (all natural levels) 150 g 29/03/2016 07254 grapefruit cadmium, lead, iron & tin (all high levels) 50 g F F F Footnotes DD freeze dried matrix, not to be reconstituted (by participants) prior to testing F test incurs courier charges 33 FAPAS Pesticide Residues – Animal Products / Fats and Oils In order to ensure good agricultural practice, pesticide residues are under strict legislation worldwide. Some pesticide residues exhibit bioaccumulation and build up to harmful levels in the body and environment. FAPAS® offers pesticide residues PTs for a range of matrices. Each test material (except test 05110) will contain any number of the pesticides given in List 1. dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 09/04/2015 05104 hydrogenated vegetable oil selection from List 1 50 g 05104b blank hydrogenated vegetable oil BLANK (only available if ordered with test 05104) 50 g 05105 milk powder selection from List 1 50 g 05105b blank milk powder BLANK (only available if ordered with test 05105) 50 g 05106 olive oil selection from List 1 50 g 05106b blank olive oil BLANK (only available if ordered with test 05106) 50 g 05107 rapeseed oil selection from List 1 50 g 05107b blank rapeseed oil BLANK (only available if ordered with test 05107) 50 g oily fish selection from List 1 50 g blank oily fish BLANK (only available if ordered with test 05108) 50 g animal (pork) fat selection from List 1 50 g 05109b blank animal (pork) fat BLANK (only available if ordered with test 05109) 50 g 05110 infant formula (powdered) selection from List 1 & List 2 (low level – based on EU-MRLs) 50 g 05110b blank infant formula (powdered) BLANK (only available if ordered with test 05110) 50 g 27/05/2015 29/07/2015 16/09/2015 09/11/2015 F 05108 F 05108b 19/01/2016 F 05109 F 19/02/2016 Footnotes F test incurs courier charges 34 FAPAS Potential Pesticide Residues and PCBs – List 1 Potential pesticide residues and PCBs (parent compound only unless otherwise stated) aldrin cyproconazole fenthion cis-heptachlor epoxide pyrazophos azinphos-ethyl pp¢-DDE fenthion sulfone trans-heptachlor epoxide quintozene bifenthrin pp¢-DDD (TDE) fenthion sulfoxide indoxacarb spinosad (spinosyn A + spinosyn D) boscalid op¢-DDT fenvalerate metazachlor tebuconazole cis-chlordane pp’-DDT flauzifop-P-butyl (fluazifop acid) methacrifos tecnazene trans-chlordane deltamethrin fluquinconazole methidathion thiacloprid oxychlordane diazinon flusilazole 4,4’-methoxychlor triazophos chlorfenvinphos dieldrin formothion nitrofen vinclozolin chlorobenzilate alpha-endosulfan (endosulfan I) haloxyfop parathion-ethyl PCB 28 chlorpropham beta-endosulfan (endosulfan II) hexachlorobenzene (HCB) parathion-methyl PCB 52 chlorpyrifos-ethyl endosulfan sulfate alpha-hexachlorocyclohexane (a-HCH) pendimethalin PCB 101 chlorpyrifos-methyl endrin beta-hexachlorocyclohexane (b-HCH) permethrin (sum isomers) PCB 118 cyfluthrin (sum isomers) epoxiconazole gamma- hexachlorocyclohexane (lindane) pirimiphos-methyl PCB 138 lambda-cyhalothrin famoxadone delta-HCH (δ-HCH) prochloraz PCB 153 cypermethrin fenpropimorph heptachlor profenofos PCB 180 Potential Pesticide Residues – List 2 Potential pesticide residues cadusafos fentin (as cation) disulfoton fipronil (parent only) disulfoton sulfoxide omethoate disulfoton sulfone oxydemeton-methyl ethoprophos terbufos fensulfothion terbufos sulfone fensulfothion sufone terbufos sulfoxide fensulfothion oxon 35 fensulfothion oxon sulfone demeton-S-methyl sulfone FAPAS Pesticide Residues – Cereals Each test material (except test 0996) will contain any number of the pesticides given in List 3. dispatch date dd/mm/yyyy code matrix analyte approximate quantity 24/04/2015 0994 maize flour selection from list 3 50 g 0994b blank maize flour BLANK (only available if ordered with test 0994) 50 g 0995 wheat flour selection from list 3 50 g 0995b blank wheat flour BLANK (only available if ordered with test 0995) 50 g 0996 oats chlormequat, mepiquat & glyphosate 100 g 0996b blank oats BLANK (only available if ordered with test 0996) 100 g 0997 brown rice selection from List 3 50 g 0997b blank brown rice BLANK (only available if ordered with test 0997) 50 g 0998 infant food selection from list 3 50 g 0998b blank infant food BLANK (only available if ordered with test 0998) 50 g 0999 wheat flour selection from list 3 50 g 0999b blank wheat flour BLANK (only available if ordered with test 0999) 50 g 24/06/2015 20/08/2015 30/09/2015 11/12/2015 18/02/2016 36 test details FAPAS Potential Pesticide Residues – List 3 Potential pesticide residues (parent compound only unless otherwise stated) 2-phenylphenol demeton-S-methyl sulfone fenthion sulfoxide methacrifos pyraclostrobin acephate diazinon fenthion sulfone methamidophos pyridaphenthion atrazine dichlorvos fenvalerate (sum of isomers) methomyl pyrimethanil azinphos-methyl difenoconazole fipronil metribuzin quinoxyfen azoxystrobin diflubenzuron fludioxonil omethoate quintozene bifenthrin dimethoate fluquinconazole oxydemeton-methyl (demeton-S-methyl sulfoxide) spiroxamine boscalid dimoxystrobin flusilazole paclobutrazole tebuconazole bromophos-ethyl disulfoton flutriafol parathion(-ethyl) tebufenozide captan disulfoton sulfoxide fonofos parathion-methyl terbufos carbaryl disulfoton sulfone formothion penconazole terbufos sulfone carbendazim alpha-endosulfan (endosulfan I) alpha-hexachlorocyclohexane (a-HCH) pendimethalin terbufos sulfoxide carbofuran beta-endosulfan (endosulfan II) beta-hexachlorocyclohexane (b-HCH) permethrin (sum) tetrachlorvinphos 3-hydroxycarbofuran endosulfan sulfate gamma-HCH (lindane) phorate thiabendazole carboxin epoxiconazole hexaconazole phorate sulfoxide thiacloprid chlorfenvinphos ethion imazalil phorate sulfone thiamethoxam chlorothalonil ethoprophos imidacloprid phosalone thiodicarb chlorpropham etrimfos iprodione phosmet tolclofos-methyl chlorpyrifos-ethyl fenamiphos isofenphos-methyl phosphamidon triadimefon chlorpyrifos-methyl fenamiphos sulfoxide isoprothiolane piperonyl butoxide triadimenol clothianidin fenamiphos sulfone isoproturon pirimicarb triazophos cyfluthrin (sum of isomers) fenbuconazole kresoxim-methyl desmethyl-pirimicarb tricyclazole lambda-cyhalothrin fenhexamid linuron pirimiphos-methyl trifloxystrobin cypermethrin fenitrothion malaoxon prochloraz trifluralin 37 cyproconazole fenpropidin malathion procymidone triticonazole cyprodinil fenpropimorph metconazole propiconazole vinclozolin deltamethrin fenthion FAPAS Pesticide Residues – Fresh Fruits, Vegetables, Tea & Herbs The fruit, vegetable and herb test matrices will be prepared from fresh fruit, vegetables or herbs that have been made into a purée. Each test material will contain any number of the pesticides given in List 4, except tests: 19196 (salad leaves) which will contain any number of the pesticides given in List 5, 19198 (cauliflower) and test 19203 (black tea) which will contain any number of the pesticides given in List 6 and test 19204 which is for a single residue. Test 19205 (peas with pods) also allows reporting of dithiocarbamates. dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 27/04/2015 19191 apple pesticide residues from List 4 90 g blank apple BLANK 90 g table grapes pesticide residues from List 4 90 g 19192b blank table grapes BLANK 90 g F sweet bell peppers pesticide residues from List 4 90 g blank sweet bell peppers BLANK 90 g tomato pesticide residues from List 4 90 g blank tomato BLANK 90 g lettuce pesticide residues from List 4 90 g 19195b blank lettuce BLANK 90 g F salad leaves quaternary ammonium compounds (biocides) from List 5 90 g 19196b blank salad leaves BLANK 90 g F strawberry pesticide residues from List 4 90 g blank strawberry BLANK 90 g F F 19191b 27/04/2015 F 19192 F 18/05/2015 19193 F 19193b 15/06/2015 F 19194 F 19194b 10/08/2015 F 19195 F 10/08/2015 19196 F 21/09/2015 19197 F 19197b Footnotes F test incurs courier charges 38 FAPAS Pesticide Residues – Fresh Fruits, Vegetables, Tea & Herbs (continued) dispatch date test details dd/mm/yyyy code matrix analyte approximate quantity 21/09/2015 19198 cauliflower pesticide residues from List 6 90 g blank cauliflower BLANK 90 g peach pesticide residues from List 4 90 g blank peach BLANK 90 g cucumber pesticide residues from List 4 90 g blank cucumber BLANK 90 g basil (herb) pesticide residues from List 4 90 g blank basil (herb) BLANK 90 g mango pesticide residues from List 4 90 g 19202b blank mango BLANK 90 g 19203 tea (black) pesticide residues from List 6 50 g 19203b blank tea (black) BLANK 50 g red grape ethephon (single residue) 90 g blank red grape BLANK 90 g peas (with pods) pesticide residues from List 4 plus dithiocarbamates 2 x 90 g blank peas (with pods) BLANK 90 g potato pesticide residues from List 4 90 g blank potato BLANK 90 g orange pesticide residues from List 4 90 g blank orange BLANK 90 g F F 19198b 19/10/2015 F 19199 F 19199b 19/10/2015 F 19200 F 19200b 23/11/2015 F 19201 F 19201b 23/11/2015 F 19202 F 07/01/2016 25/01/2016 Ff 19204 F 19204b 22/02/2016 F 19205 F 19205b 22/02/2016 F 19206 F 19206b 29/03/2016 F 19207 F 19207b Footnotes F test incurs courier charges 39 FAPAS Potential Pesticide Residues – List 4 2-phenylphenol acephate cyproconazole cyprodinil acetamiprid acetochlor pp’-DDD (TDE) pp’-DDE acrinathrin aldicarb aldicarb sulfone (aldoxycarb) aldicarb sulfoxide aldrin allethrin atrazine azinphos-methyl azoxystrobin benalaxyl bendiocarb bifenthrin bitertanol boscalid bromopropylate bromuconazole (sum of isomers) bupirimate buprofezin cadusafos carbaryl carbendazim carbofuran 3-hydroxy carbofuran carbosulfan chlorantraniliprole chlorbufam cis-chlordane trans-chlordane chlorfenapyr chlorfenvinphos (sum of isomers) chlorobenzilate chlorpropham chlorpyrifos-ethyl chlorpyrifos-methyl chlorthal-dimethyl clofentezine clothianidin coumaphos cyfluthrin (sum of isomers) lambda-cyhalothrin cypermethrin 40 methiocarb methiocarb sulfone pyrimethanil pyriproxyfen methiocarb sulfoxide methomyl quinalphos quinoxyfen op’-DDT pp’-DDT fenthion sulfone fenvalerate (sum of all isomers) flonicamid flauzifop-P-butyl (fluazifop acid) flubendiamide flucythrinate 4,4’-methoxychlor methoxyfenozide deltamethrin fludioxonil mevinphos quintozene spinosad (spinosyn A + spinosyn D) spirodiclofen demeton-S-methyl sulfone desmethyl-pirimicarb diazinon diafenthiuron dichlorvos dicloran dicrotophos dieldrin flufenoxuron fluopicolide fluquinconazole flusilazole flutolanil flutriafol fosthiazate furathiocarb spiroxamine tebuconazole tebufenozide tebufenpyrad tecnazene teflubenzuron tefluthrin terbuthylazine diethofencarb difenoconazole diflubenzuron dimethoate dimethomorph (sum of isomers) diniconazole diphenylamine alpha-endosulfan (endosulfan I) beta-endosulfan (endosulfan II) endosulfan sulfate HCB (hexachlorobenzene) alpha-HCH beta-HCH gamma-HCH (lindane) heptenophos monocrotophos monolinuron myclobutanil omethoate oxadiazon oxadixyl oxamyl oxydemeton-methyl (demeton-S-methyl sulfoxide) oxyfluorfen paclobutrazol parathion (-ethyl) parathion-methyl penconazole hexaconazole hexythiazox imazalil pencycuron pendimethalin pentachloroaniline thiamethoxam thiodicarb tolclofos-methyl imidacloprid tolfenpyrad endrin EPN epoxiconazole ethion ethirimol ethoprophos etofenprox famoxadone fenamidone indoxacarb (sum isomers) iprodione iprovalicarb isocarbofos isofenphos isofenphos-methyl isoprocarb isoproturon kresoxim-methyl lenacil permethrin (sum of isomers) phenthoate phosalone phosmet pirimicarb pirimiphos(-ethyl) pirimiphos-methyl prochloraz procymidone profenofos promecarb triadimefon triadimenol triallate triazophos trifloxystrobin triflumuron trifluralin triticonazole vinclozolin fenarimol fenazaquin fenbuconazole fenhexamid fenitrothion fenoxycarb fenpropathrin fenpropimorph fenpyroximate linuron lufenuron mandipropamid mecarbam mepanipyrim metalaxyl metalochlor metamitron metconazole prometryn propamocarb propargite propiconazole propoxur propyzamide prothiofos pymetrozine pyraclostrobin zoxamide fenthion fenthion sulfoxide methamidophos methidathion pyrazophos pyridaben tetraconazole tetradifon tetramethrin thiabendazole thiacloprid tolylfluanid FAPAS Potential Pesticide Residues – List 5 benzalkonium chloride (BAC-10; BAC-12; BAC-14; BAC-16) didecyldimethylammonium chloride (DDAC-C10) Potential Pesticide Residues – List 6 acetamiprid diazinon beta-endosulfan (endosulfan II) bifenthrin dicofol endosulfan sulfate chlorfenvinphos dimethoate ethion chlorothalonil pp’-DDD (TDE) fenazaquin chlorpyrifos-ethyl pp’-DDE fenitrothion lambda-cyhalothrin op’-DDT fenpropathrin cypermethrin (sum isomers) pp’-DDT fenpropimorph deltamethrin alpha-endosulfan (endosulfan I) fenvalerate (sum isomers) 41 HCB (hexachlorobenzene) alpha-HCH gamma-HCH (lindane) imidacloprid linuron malathion methomyl monocrotophos phenthoate phosalone pirimiphos-methyl procymidone propargite pyridaben pyrimethanil quinalphos terbuthylazine trifloxystrobin FAPAS Prices in € PROFICIENCY TESTS 01100, 01101, 01102, 01103, 01104, 01105, 01106 02262, 02263, 02264, 02265, 02266, 02267, 02268, 02269, 02270, 02271, 02272, 02273, 02274, 02275, 02276, 02277, 02279, 02281, 02282, 02283, 02284, 02285, 02286, 02287 02278 02280 03122, 03123, 03124, 03125, 03126, 03127, 03128 04260 04261 04262 04263, 04264, 04265 04266 04267 04268 04269 04270 04271 04272 04273 04274 04275 04276 04277, 04278 04279 04280 04281 05104, 05105, 05106, 05107 05108, 05109 05110 0662, 0663, 0665 0664 07233, 07234, 07235 07236 07237, 07238, 07239, 07240, 07241, 07242, 07243, 07244, 07245, 07246, 07247, 07248 07249 07250 42 Courier F F F F F F F F F F F Round Blank Test Materials 241 66 330 476 330 95 171 95 241 419 241 241 241 241 419 241 585 241 241 419 241 322 241 419 241 322 322 241 253 253 322 458 458 241 241 66 132 66 66 66 66 132 66 171 66 66 132 66 95 66 132 66 95 95 66 66 66 95 171 171 66 66 241 241 241 66 66 66 FAPAS 07251, 07254 07252, 07253 0856, 0857, 0858, 0859, 0994, 0995, 0996, 0997, 0998, 0990 10125, 10128 10126, 10127, 10129, 10130, 10131 1268, 1269, 1270, 1271, 1272 1374, 1375, 1376 14144, 14145, 14150, 14152 14146, 14147, 14148, 14149, 14151, 14153, 14154, 14155 15103, 15104, 15107, 15109 15105, 15106, 15108, 15110 1656, 1657, 1658 17149, 17151, 17152, 17153, 17154, 17155, 17156, 17157, 17158, 17159 17150 17160 1879, 1880, 1881 1882 19191, 19192, 19193, 19194, 19195, 19196, 19197, 19198, 19199, 19200, 19201, 19202, 19206, 19207 19203 19204 19205 20116, 20118, 20119, 20121, 20122, 20124 20117, 20120, 20123 2191, 2194, 2195 2192, 2193 22119 22120 22121 22122, 22123 22124 22125, 22127 22126 22128 22129 22130 2461, 2462, 2463 2464, 2465 25130, 25131, 25132, 25133, 25134, 25136, 25137, 25138, 25140 25135, 25139 2645, 2646, 2647 43 F F F F F F F F F F F F F 241 241 66 66 241 458 253 241 330 241 66 132 66 66 95 66 241 241 241 241 66 66 66 66 241 241 270 241 241 66 66 95 66 66 241 241 322 322 66 66 95 95 241 241 253 253 241 241 322 241 585 322 538 241 538 322 241 66 66 66 66 66 66 95 66 171 95 171 66 171 95 66 241 241 253 66 66 66 FAPAS 27153, 27154, 27155, 27156, 27157, 27158, 27159, 27160, 27161, 27162 27163 27164, 27166, 27171 27165, 27167, 27168, 27169, 27170 2831, 2832, 2833 2963, 2964, 2966 2965 3055, 3056, 3057, 3058, 3059, 3060, 3061 F F F 3062 F 253 253 322 253 241 253 253 66 66 95 66 66 66 66 241 66 241 66 DISCOUNTS applicable to above prices 0-20 tests 0% 21-45 tests 5% 46-70 tests 10% 71 tests or more 20% ADDITIONAL ITEMS Price EUR (€) Blank Material 77 Phytosanitary certificate 58 Additional Customs documentation e.g. declaration letter 45 CARRIAGE CHARGES Price EUR (€) EU Courier Charge 85 Non-EU Courier Charge 100 All prices incl. German tax. 44 FAPAS Technical Information Protocols · Protocol part 1: Generic [English] [Espanol] · Protocol part 2: FAPAS [English] [Espanol] Other technical documents · Example Report · On line results submission instructions [English] [Espanol] · Terms & Conditions ISO Accreditation The proficiency testing schemes FAPAS®, FEPAS®, GeMMA and LEAP® are accredited by UKAS, Proficiency Testing Provider No. 0009. 0009 · UKAS Accreditation Certificate This accreditation confirms that we comply with the requirements of International Standard ISO/IEC 17043:2010 In addition, Fera is accredited by other external bodies to other internationally recognised standards including ISO 9001:2008. · Fera's Quality Documentation FAPAS (and other proficiency testing schemes) does not award accreditation. That is the responsibility of national accreditation bodies. A list of national and international accreditation bodies can be found at www.fasor.com/iso25. Results of proficiency testing are used by laboratory accreditation bodies as part of the process to assess the ability of laboratories to perform analytical tests for which accreditation is required. 45
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