TECHNIQUE OF ORGANIC CHEMISTRY Volume I—Part I PHYSICAL METHODS of Organic Chemistry Third Completely Revised and Augmented Edition Editor: ARNOLD WEISSBERGER Authors of Part I A. E. ALEXANDER J. R. ANDERSON J. C. ARTHUR, JR. N. BAUER G. L. BEYER A. H. CORWIN W. D. HARKINS S. Z. LEWIN W. J. MADER H. MARK L. D. MOORE, JR. D. R. SIMONSEN EVALD L. SKAU J. M. STURTEVANT W. SWIETOSLAWSKI J. F. SWINDELLS G. W. THOMSON M. J. VOLD R. D. VOLD R. ULLMAN R. H. WAGNER H. WAKEHAM PART ONE 1959 INTERSCIENCE PUBLISHERS, INC., NEW YORK INTERSCIENCE PUBLISHERS LTD., LONDON T E C H N I Q U E O F O R G A N I C C H E M I S T R Y Volume I PHYSICAL METHODS OF ORGANIC CHEMISTRY CONTENTS Part One Krom the Prefaces to the First and Second Editions I 'refaces to the Third Edition I. Automatic Control. vii viii By JULIAN M. STURTEVANT 1 II. Automatic Recording. By D. R. SIMONSEN III. Weighing. 35 By ALSOPH H. CORWIN IV. Determination of Density. , By NORMAN BAUER and S. Z. LEWIN . . . . 71 131 V. Determination of Particle Size and Molecular Weight. By GEORGE L. BEYER , VI. Temperature Measurement. 191 By JULIAN M. STURTEVANT VII. Determination of Melting and Freezing Temperatures. 259 By EVALD L. SKAU, JETT C. ARTHUR, JR., and HELMUT WAKEHAM 287 VIII. Determination of Boiling and Condensation Temperatures. By W. SWIETOSLAWSKI and JOHN R. ANDERSON 357 IX. Determination of Vapor Pressure. By GEORGE W. THOMSON X. Calorimetry. By JULIAN M. STURTEVANT XI. Determination of Solubility. 401 523 By W. J. MADER, R. D. VOLD, and M. J. VOLD 655 XII. Determination of Viscosity. By j . F. SWINDELLS, R. ULLMAN, and H. MARK 689 XIII. Determination of Properties of Insoluble Monolayers at Mobile Interfaces. By A. E. ALEXANDER 727 XIV. Determination of Surface and Interfacial Tension. WILLIAM D. HARKINS. By the late Revised by A. E. ALEXANDER 757 XV. Determination of Osmotic Pressure. By R. H. WAGNER and L. D. MOORE, J R 815 Index to Part I Part Two XVI. Determination of DifTusivity. By A. L. GEDDES and R. B. PONTIUS XVII. Determinations with the Ultracentrifuge. By J. BURTON NICHOLS and EMERSON D. BAILEY XVIII. Refractometry. By N. BAUER, K. FAJANS, and S. Z. LEWIN XIX. Determination of Crystal Morphology. By the late M. A. PEACOCK, J. D. H. DONNAY, and GABRIELLE DONNAY XX. Crystallochemical Analysis. By J. D. H. DONNAY and GABRIELLE DONNAY XXI. Light Microscopy. By EDWIN E. JELLEY XXII. Microspectroscopy. By ELKAN R. BLOUT XXIII. X-Ray Microscopy. By W. C. NIXON XXIV. Electron Microscopy. By F. A. HAMM XXV. X-Ray Crystallography. By WILLIAM N. LIPSCOMB XXVI. Electron Diffraction by Gases. By L. O. BROCKWAY XXVII. Neutron Diffraction. By J. M. HASTINGS and L. M. CORLISS Index to Part II xi Xll CONTENTS T E C H N I Q U E O F O R G A N I C C H E M I S T R Y Volume I PHYSICAL METHODS OF ORGANIC CHEMISTRY Part Three XXVIII. Spectroscopy and Spectrophotometry in the Visible and Ultraviolet. By W. WEST XXIX. Infrared Spectroscopy. By D. H. ANDERSON, N. B. WOODALL, and W. WEST XXX. Colorimetry and Photometric Analysis. By W. WEST XXXI. Determination of Fluorescence and Phosphorescence. By N. WOTHERSPOON and GERALD OSTER XXXII. Light Scattering. By GERALD OSTER XXXIII. Polarimetry. By W. HELLER and D. D. FITTS XXXIV. Optical Rotatory Dispersion. By W. KLYNE and A. C. PARKER XXXV. Streaming Birefringence. By H. A. SCHERAGA and R. SIGNER XXXVI. The Kerr Effect. By CATHERINE G. L E FEVRE and R. J. W. LE FEVRE XXXVII. Determination of the Faraday Effect. By C. E. WARING and R. L. CtTSTER XXXVIII. Measurement of Dielectric Constant and Loss. By J. G. POWLES and C. P. SMYTH XXXIX. Determination of Dipole Moments. By C. P. SMYTH Index to Part I I I P a r t F o u r XL. XLI. XLII. XLIII. Microwave Spectroscopy. By B. P. DAILEY Nuclear Magnetic Resonance. By H. S. GUTQWSKY Paramagnetic Resonance Absorption. By GEORGE K. FRAENKEL Determination of Magnetic Susceptibility. By P. W. SELWOOD XLIV. Potentiometry. By C. TANPORD and S. WAWZONEK XLV. Conductometry. By T. SHEDLOVSKY XLVI. XLVII. XLVIH. XLIX. Determination of Transference Numbers. By M. SPIRO Electrophoresis. By D. H. MOORE Polarography. By O. H. MULLER Controlled-Potential Electrolysis. By Lotfis MEITES L. Determination of Radioactivity. E. SIRI LI. Mass Spectrometry. Index to Volume By BERT M. TOLBERT and WILLIAM By DAVID M. STEWART
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