COGEL-01956; No of Pages 8 International Journal of Coal Geology xxx (2012) xxx–xxx Contents lists available at SciVerse ScienceDirect International Journal of Coal Geology journal homepage: www.elsevier.com/locate/ijcoalgeo Petrographic characteristics and palaeoenvironmental setting of Upper Triassic Olang coal deposits in northeastern Iran Z. Solaymani, N. Taghipour ⁎ School of Earth Sciences, Damghan University, P.O. Box: 36715–364, Damghan, Iran a r t i c l e i n f o Article history: Received 6 April 2011 Received in revised form 28 December 2011 Accepted 2 January 2012 Available online xxxx Keywords: Coal petrography Depositional environment Olang Iran a b s t r a c t This study investigates the petrographic analysis, microlithotype, and palaeoenviroment of deposition of the upper Triassic Olang coal deposits in northeastern Iran. The average maceral composition of the studied coals consisted of 82.3, 8.9, 0.4 (vol.%), vitrinite, inertinite and liptinite groups, respectively. Vitrinite macerals include equal portions of collotelinite and; collodetrinite and a small quantity of corpogelinite also is present in all coal seams. Semifusinite and fusinite are the most abundant inertinite macerals. The Ground Water Index (GWI) suggests that these coal seams have evolved in a limnic coal facies (a bog palaeomire system) under ombrotrophic hydrological conditions, except the K6G coal seam, which evolved a limnic coal facies (a bog palaeomire system) under mesotrophic hydrological conditions. The Vegetation Index (VI) values are indicative of the dominance of herbaceous plants in the formation of coal seams of the Olang area. © 2012 Elsevier B.V. All rights reserved. 1. Introduction There is little known about the petrography, geochemistry, and mineralogy of Iranian coals. The only petrographical analysis of Iranian coal in the available literature is a photomicrograph in Stach et al. (1982) showing a clarite with liptodetrinite, sporinite, and resinite from a highly volatile Jurassic coal from Zerab. There also is little known about the geochemistry and mineralogy of Iranian coals except for the studies by Stasiuk et al. (2006) on the petrology, rank and liquid petroleum potential of the Central Alborz Region, the geochemical properties of coals in the Lushan coalfield carried out by Yazdi and Shiravani (2004), and a preliminary study of the mineralogy and geochemistry of four coal samples from northern Iran by Goodarzi et al. (2006). Iranian coal resources mostly occur in two main basins, one in northern and another in central Iran, the Alborz and Central basins, respectively. The Alborz basin is subdivided into three regions: western, central and eastern Alborz. Eastern Alborz region coal resources are estimated to be about 1 Gt occurring in two areas, Tazareh and Gheshlagh. The Olang region is located in the Gheshlagh area. In general, coals of the Gheshlagh area are medium volatile bituminous (%VRr: 0.82–0.88) and have variable ash yield (9 to 40 wt.%), volatile matter (26 to 28 wt.%), and sulphur (0.6 to 1.02 wt.%) contents (Razavi-Armagani and Moenoalsadat, 1994). ⁎ Corresponding author. E-mail address: [email protected] (N. Taghipour). Coal petrographic studies are mainly used for determining coal quality, coking properties and composition, palaeodepositional environment, or coal rank (Taylor et al., 1998). This study uses organic petrography to provide detailed maceral composition and hence, reconstruction of the palaeoenvironmental conditions of deposition for 12 coal seams from the Upper Triassic–Lower Jurassic section of the Olang coal deposit in northeastern Iran. 2. Geological setting The Olang region is situated about 70 km northeast of the city of Shahroud, located in northeastern Iran (longitude 55°10′; latitude 36°50′, Fig. 1). This area is part of the Gheshlagh - Olang syncline with a NS-SW axis with respect to the Alborz coalfield. Coal-bearing strata of this region are part of the Shemshak group which occurs between dolomitic limestones of the Elica Formation and the underlying limestones of the Lar Formation (Fig. 2). The Shemshak Group (Assereto, 1966; Fürsich et al., 2009; Shekarifard et al., 2011) is a siliciclastic succession with immense thicknesses up to 4000 m, widely distributed across central and northern Iran (Fig. 1), the so-called Iran Plate. Commonly the Shemshak Group is regarded as the product of the erosion of the Cimmerides, deposited in a foreland basin (Alavi, 1996; Assereto, 1966; Seyed-Emami, 2003; Seyed-Emami and Alavi-Naini, 1990). Fürsich et al. (2009) consider the Shemshak Group as the result of syn- and post-collisional processes of the Eo-Cimmerian orogeny. The Shemshak Group consists almost exclusively of fine- to coarse-grained siliciclastic sediments that are accompanied by numerous coal seams and carbonaceous shales at different stratigraphic levels. The 0166-5162/$ – see front matter © 2012 Elsevier B.V. All rights reserved. doi:10.1016/j.coal.2012.01.003 Please cite this article as: Solaymani, Z., Taghipour, N., Petrographic characteristics and palaeoenvironmental setting of Upper Triassic Olang coal deposits in northeastern Iran, Int. J. Coal Geol. (2012), doi:10.1016/j.coal.2012.01.003 2 Z. Solaymani, N. Taghipour / International Journal of Coal Geology xxx (2012) xxx–xxx Fig. 1. Locality map with outcrop distribution of the Shemshak Formation in the Alborz Mountains, northern Iran. The Olang area is marked with an arrow (modified after Seyed-Emami, 2006). age of the Shemshak Group ranges from Late Triassic to Early Bajocian (Fürsich et al., 2005, 2009; Seyed-Emami, 2003; Seyed-Emami et al., 2001, 2005, 2006; Vollmer, 1987). Its depositional palaeoenvironment includes fluvial, swamp and lake systems, as well as shallow to deeper marine environments with local oxygen-deficient conditions leading to the deposition of organic Fig. 2. Lithostratigraphy of Shemshak Group in the Alborz Region (Shekarifard et al., 2011). Please cite this article as: Solaymani, Z., Taghipour, N., Petrographic characteristics and palaeoenvironmental setting of Upper Triassic Olang coal deposits in northeastern Iran, Int. J. Coal Geol. (2012), doi:10.1016/j.coal.2012.01.003 Z. Solaymani, N. Taghipour / International Journal of Coal Geology xxx (2012) xxx–xxx 3 Fig. 3. Lithostratigraphic column of the coal seams in the Olang region, northeastern Iran. Coal seam studies (K4, K13, K14, K15 of the Melech Aram mine, and K6 of the Granite mine, K18, K19, K20, K21 of the Alborzegan mine and K30, K31, K32 of the Razi mine) are indicated. carbon-rich sediments (Baudin and Teherani, 1991; Fürsich et al., 2005; Rad, 1982, 1986; Seyed-Emami et al., 2006; Shekarifard et al., 2009, 2011; Stampfli, 1978; Fig. 2). Based on a regional classification, the Shemshak Formation in Eastern Alborz consists of the Akrasar, Lalleh band, Kalariz, Alasht, Shirin Dasht and Dancerit formations. Olang coal-bearing strata occur in the Kalariz formation (Rethian to Hettangian), which consists mainly of coal seams, siltstone, fine grained sandstone and locally coarse grained sandstone (Fig. 3). excitation used for recognition and differentiation of liptinite macerals). The terminology used to identify and describe the organic matter particles is the one proposed by the International Committee for Coal and Organic Petrology (ICCP, 1998, 2001) as well as Scott and Glasspool (2007) and Taylor et al. (1998). In order to characterise the palaeomires, the petrographic indices such as Vegetation Index (VI) and Groundwater Influence Index (GWI) of Calder et al. (1991) were considered. 3. Sampling and methodology 4. Coal petrography A total of 120 blocks of coal samples were collected from freshly mined coal from 12 coal seams of 4 active coal mines (Razi, Melech Aram, Alborzegan and Granite) for petrography and palaeoenviromental study in Olang coal deposits (Fig. 3 and 4b). All samples were collected and stored in plastic bags to prevent contamination and weathering. Samples were prepared for microscopic analysis by reflected light following ASTM Standard D2797-04. For microscopic study, coal samples were crushed to b 1-mm size fraction (18 mesh size), mounted in epoxy resin and polished. Three polished samples were prepared for each coal seam. The petrographic composition was obtained by maceral analyses under standard conditions (ISO 7404/3 (2009) for maceral analysis). Maceral point counting (based on 400 points) analyses were performed using an Olympus BX51 reflected light microscope and Leitz MPV-SP reflected light microscope equipped with photometer– photomultiplier and white and ultra-violet light sources (blue light 4.1. Vitrinite The vitrinite maceral group is dominant in all coal seams (57.7– 94 vol.%; Table. 1) and includes collodetrinite, collotelinite, and corpogelinite macerals. Collotelinite (35.2–72.8 vol.%) occurs as a structureless, homogeneous mass in thin and thick bands, and also as isolated irregular fragments of different dimensions (Fig. 5a). The inclusion of liptinite within the collotelinite is very common. Secondary infilling of mineral matter also occurs in cracks and cavities of collotellinite. Collodetrinite macerals are present as mottled vitrinitic groundmass binding other coal components (maceral and mineral) and often shows lower reflectance than associated collotelinite (Fig. 5a, b). Collodetrinite is the most abundant maceral of the vitrinite group, except the K30R coal seam, in which collotelinite is the most abundant maceral. Very small percentages of corpogelinite are observed in only 8 coal seams of this area. This maceral occurs mostly as fillings in the cell cavities of fusinite and semifusinite (Fig. 5c). Please cite this article as: Solaymani, Z., Taghipour, N., Petrographic characteristics and palaeoenvironmental setting of Upper Triassic Olang coal deposits in northeastern Iran, Int. J. Coal Geol. (2012), doi:10.1016/j.coal.2012.01.003 4 Z. Solaymani, N. Taghipour / International Journal of Coal Geology xxx (2012) xxx–xxx Fig. 4. a) Coal-bearing strata of Iran (modified after Yazdi and Sheivani, 2004). b) Geological map showing locations of studied coal mines in the Olang area (modified after Zahrab, 2004). 4.2. Inertinite Inertinite contents range from 4.2 to 23.1 vol.% of the studied coal samples. Fusinite (15.7 to 51.4 vol.%; Table. 1) is present in all coal seams. Cell cavities of fusinite are filled mostly by corpogelinite and clay minerals (Fig. 5c). Semifusinite occurs in appreciable concentrations (1.1 to 12 vol.%) with a reflectance between collotelinite and fusinite in the same coal. Cell lumens of semifusinite are filled (partly or completely) with mineral matter, mostly argillaceous in composition (Fig. 5b). Macrinite (0.1 to 1 vol.%) occurs as amorphous (nongranular) and structureless bands or lenses. Inertodetrinite (0.1 to 0.7 vol.%) is observed as discrete small fragments of varying shape with high reflectance (higher than the associated vitrinite of the same sample). Micrinite is observed as granular aggregates and it is rare (Fig. 5b). Secretinite (nil to 0.2 vol.%) is very common in these coal seams. It occurs as large size oval to rounded bodies with un-oriented vesicles Table 1 Maceral composition analysis and mineral content of the coals seams of the Olang area (in vol%). Sample CT Cg V-G Sp Cu Re LD L-G Alborzegan Mine 60.1 K18A K19A 76.3 K20A 67.5 K21A 68.0 CD Fu 14.6 15.4 15.2 26.0 1.3 0.1 0.2 0.0 76.0 91.8 82.9 94.0 0.5 0.4 2.5 0.2 0.4 0.3 1.0 0.1 0.0 0.0 0.0 0.0 0.2 0.3 0.3 0.0 1.1 1.0 3.8 0.3 1.6 2.8 4.2 0.7 Razi Mine K30R K31R K32R 35.3 59.3 50.4 48.6 13.4 20.4 0.3 0.4 0.8 84.2 73.1 71.6 0.0 0.0 0.1 0.0 0.1 0.3 0.0 0.1 0.0 0.0 0.1 0.3 0.0 0.3 0.7 Melech Aram Mine 50.7 K4M K13M 72.8 K14M 63.0 K15M 69.0 11.7 4.9 20.1 14.4 0.3 0.0 0.0 0.1 62.7 77.7 83.1 83.5 2.2 1.2 1.7 0.4 0.5 0.3 0.3 0.4 0.1 0.1 0.0 0.0 0.4 1.1 0.8 0.0 Granite Mine 52.0 K6G 5.7 0.0 57.7 0.9 0.3 0.1 0.0 Sf Ma In Fg Sc I-G Mm 5.8 2.8 2.5 3.5 0.5 0.2 1.0 0.7 0.7 0.5 0.1 0.4 0.1 0.1 0.0 0.1 0.1 0.2 0.0 0.0 8.8 6.6 7.8 5.4 14.1 0.6 5.5 0.3 8.4 10.2 5.6 7.0 10.3 9.2 0.2 0.0 0.1 0.1 0.2 0.1 0.0 0.0 0.0 0.0 0.2 0.2 15.7 20.9 15.2 0.1 5.7 12.5 3.2 2.7 2.8 0.8 9.6 3.5 5.2 4.6 12 1.1 2.4 2.7 0.8 0.6 0.7 0.9 0.5 0.1 0.1 0.2 0.1 0.1 0.0 0.3 0.1 0.2 0.1 0.2 23.1 5.6 8.5 8.9 11.0 14.0 5.6 6.8 1.3 2.3 2.8 0.4 0.7 0.0 0.1 6.3 34.7 CD = collodetrinite; CT = collotelinite; Cg = corpogelinite; V-G = vitrinite group total; Sp = spornite; Re = resinite; LD = liptodetrinite; L-G = liptinite group total; Fu = fusinite; Sf = semifusinite; Ma = macrinite; In = inertinite; Fg = funginite; Sc = secretinite; I-G = inertinite group total; Mm = mineral matter. Please cite this article as: Solaymani, Z., Taghipour, N., Petrographic characteristics and palaeoenvironmental setting of Upper Triassic Olang coal deposits in northeastern Iran, Int. J. Coal Geol. (2012), doi:10.1016/j.coal.2012.01.003 Z. Solaymani, N. Taghipour / International Journal of Coal Geology xxx (2012) xxx–xxx 5 Fig. 5. Photomicrographs of macerals in the Olang coal seams in white reflect light. a) Collotelinite and collodetrinite with funginite (Fg) in semifusinite groundmass. b) Macrinite (Ma) and inertodetrinite (In) in collodetrinite groundmass. c) Fusinite where cell lumens are filled with corpogelinite (Cg) and argillaceous mineral matter. d) Associations of micrinite and pyrite in collotelinite. e) Secretinite (Sc). f) Funginite (Fg), macrinite (Ma), semifusinite and inertodetrinite in collodetrinite groundmass. and very high relief (Fig. 5e). Funginite (nil to 0.2 vol.%) occurs as single or multi-celled bodies filled by clay minerals and resinite (Fig. 5c). The presence of funginite indicates aerobic conditions that occurred at least intermittently in the peat environment of the Olang coal seams. 4.3. Liptinite Sporinite is the dominant maceral in the liptinite group (nil to 2.5 vol.%) and occurs as elongated thread-like or spindle-shaped bodies (Fig. 6a, b). This maceral occurs as microspores and megaspores. The microspores are high in concentration and dark grey to black in white reflected light. Megaspores are comparatively low in concentration, commonly dark brown to black in white reflect light and are mostly thin walled. Cutinite (nil to 2.1 vol.%) is observed as elongated thread like structures with one end serrated (Fig. 6c, d). Resinite (nil to 2.2 vol.%) occurs as round to oval bodies and as fillings of the cell cavities of fusinite, semifusinite and funginite (Fig. 6e, f). Liptodetrinite (nil to 1.1 vol.%) is observed in all of the coal seams of the Olang area. 4.4. Mineral matter The mineral matter content of most of the Olang coal seams varies between 0.1 and 14.1 vol.% and only one sample from the Granite mine has mineral matter content of 34.7 vol.% (Table 1). Mineral matter occurs as primary ground mass or secondary cavity filling form and includes clay minerals, carbonate and sulphide. Carbonate minerals (siderite) occur as re-precipitated small irregular bodies or patches, and fissure and cell cavity fillings of vitrinite macerals. Pyrite is observed as syngenetic (framboidal) and epigenetic (filling of the cell cavity, vein, and veinlet) mineral. Pyrite occurs in several forms such as disseminated particles, blebs, discrete grains, framboidal bodies, massive replacement and fissure fillings (Fig. 7). 5. Coal facies There are a number of models available to reconstruct the palaeoenviromental conditions of swamps using petrographic facies indices calculated from maceral analyses. A facies model based on quantitative relationships of macerals has been proposed by Calder et al. (1991). This model interprets coal facies on the basis of a Ground Water Index (GWI) and Vegetation Index (VI), the fundamentals of which are very close to the GI and TPI indices of Diessel (1986). The parameters applied in the reconstruction of peat lands (peat land = marsh + swamp) are the degree of groundwater control, relative rainfall (Kalkreuth et al., 1991; Ligouis and Doubinger, 1991), changes in groundwater level, vegetation, mineral matter content and degree of preservation of maceral precursors (Calder et al., 1991). Please cite this article as: Solaymani, Z., Taghipour, N., Petrographic characteristics and palaeoenvironmental setting of Upper Triassic Olang coal deposits in northeastern Iran, Int. J. Coal Geol. (2012), doi:10.1016/j.coal.2012.01.003 6 Z. Solaymani, N. Taghipour / International Journal of Coal Geology xxx (2012) xxx–xxx Fig. 6. Photomicrographs of macerals in the Olang coal seams; white reflect light (a, c, e), under oil immersion at 120 × and (d, e, f) under fluorescent illumination, oil immersion. a) Sporinite in collodetrinite groundmass. b) Cutinite with macrinite and vitrinite. c) Resinite. VI similar to the TPI of Diessel (1996): Ground Water Index (GWI) of these coal seams is lower than 0.5 except for the K6G coal seam, in which GWI indices are greater than 0.5 (0.6 vol.%, Table 2). The coal seams of Olang area, except the K6G coal seam, show low GWI ratios related to higher contents of detrovitrinite, suggesting a limnic coal facies (a bog palaeomire system) under ombrotrophic hydrological conditions. Values lower than 0.5 are related to wet mires maintained by rainfall only without influence of the groundwater level (Calder et al., 1991). The high GWI of the K6G coal seam is related to higher content of mineral matter (34.7 vol.%), suggesting a limnic coal facies (a bog palaeomire system) under mesotrophic hydrological conditions. The lower VI ratios are linked to an increase of semifusinite and fusinite contents, suggesting a relatively higher oxygen access during peat accumulation, and also to an increase of collodetrinite and other detritic-macerals. In contrast, the higher VI ratios suggest an increase in preservation of vegetal tissues under relatively more acid and reducing conditions, favourable for vitrinite formation. The very low values (VI b 1) indicate also a marginal aquatic/herbaceous source, which confirms previous studies (Jasper et al., 2006; Kalaitzidis et al., 2010; Picarelli and Marques-Toigo, 1985), suggesting a predominantly herbaceous vegetation as precursor material for the Olang coal seams (Fig. 8). VI ¼ Collotelinite þ Semifusinite þ Fusinite þ Resinite=Collodetrinite þ Inertodetrinite þ Liptodetrinite þ Spornite þ Cutinite 6. Conclusions The results of GWI and VI indices using the coal facies diagram from Calder et al. (1991) are shown in Fig.8. All coal maceral groups are present in coal seams of the Olang area. Vitrinite is the most important maceral group and its volume Based on GWI and VI parameters, Calder et al. (1991) identified major mire palaeoenvironments such as limnic (open water marsh), swamp, fen, and bog (Fig. 8), along with an indication of the hydrological conditions in terms of rheotrophic, mesotrophic, and ombrotrophic mires. In fact, in this diagram, the distinction between rheotrophic and ombrotrophic palaeomires is evaluated by the GWI that relates the degree of gelification with the water supply and includes mineral matter as an important indicator of groundwater. On the other hand, the above-mentioned palaeomires can be subdivided on the basis of vegetation type using the VI, which is calculated by the ratio between macerals of forest affinity and those of herbaceous and aquatic affinity. In the present study, the VI is equivalent to the petrographic index proposed by Calder et al. (1991) with the exclusion of suberinite and alginite which are not present in the studied coals: The GWI is calculated using vitrinite and mineral matter and shows the ratio between strongly gelified material plus mineral matter and weakly gelified tissues (Jasper et al., 2010): GWI ¼ Gelovitrinite þ Mineral matter=Collotelinite þ Collodetrinite Please cite this article as: Solaymani, Z., Taghipour, N., Petrographic characteristics and palaeoenvironmental setting of Upper Triassic Olang coal deposits in northeastern Iran, Int. J. Coal Geol. (2012), doi:10.1016/j.coal.2012.01.003 Z. Solaymani, N. Taghipour / International Journal of Coal Geology xxx (2012) xxx–xxx 7 Fig. 7. Photomicrographs of representative pyrite types in the Olang coals under reflected white light. a) Anhedral pyrite (Py) with siderite and clay mineral. b) Subhedral pyrite. c) Layer and spray pyrite with collotelinite. d) Pyrite as fillings of the cell cavities of fusinite. e) Fromboidal pyrite. f) Subhedral pyrite coverted by mineral matter. percentage varies between 82.9 and 95.5 vol.% (average 82.3 vol.%) in the different coal seams. Inertinite group macerals have concentrations of up to more than 15 vol.% and the average is 8.9 vol.%. The concentration of liptinite is very low and the average for all coal seams is 0.4 vol.%. Macerals of the vitrinite group include collotelinite, collodetrinite and corpogelinite with collotelinite and collodetrinite present in approximately equal content with a very small percentage of corpogelinite. The inertinite macerals consist of fusinite, semifusinite, secretinite, inertodetrinite, macrinite, micrinite and funginite. Semifusinite and fusinite are the most abundant in this group. Table 2 Petrographic indices for coal seams of the Olang area. Samples Fig. 8. GWI/VI mire palaeoenvironment diagram of the coal seams of the Olang area (modified from Calder et al., 1991). (1. K18A, 2: K19A, 3: K20A, 4: K21A, 5: K30R, 6: K31R, 7: K32R, 8: K4M, 9: K13M, 10: K14M, 11: K15M, 12: K6G). Petrographic indices GWI VI Alborzegan mine K18A K19A K20A K21A 0.21 0.001 0.07 0.003 0.36 0.27 0.30 0.44 Razi mine K30R K31R K32R 0.005 0.08 0.2 1.8 0.57 0.7 Melech Aram mine K4M K13M K14M K15M 0.2 0.2 0.07 0.08 0.6 0.1 0.4 0.3 Granit mine K6G 0.6 0.2 Please cite this article as: Solaymani, Z., Taghipour, N., Petrographic characteristics and palaeoenvironmental setting of Upper Triassic Olang coal deposits in northeastern Iran, Int. J. Coal Geol. (2012), doi:10.1016/j.coal.2012.01.003 8 Z. Solaymani, N. Taghipour / International Journal of Coal Geology xxx (2012) xxx–xxx Sporinite, cutinite and resinite macerals of the liptinite group are present in all coal seams. The Ground Water Index (GWI) suggests that these coal seams have evolved in a limnic coal facies (a bog palaeomire system) under ombrotrophic hydrological conditions, except the K6G coal seam, which evolved under mesotrophic hydrological conditions The Vegetation Index (VI) values, are indicative of the dominance of herbaceous plants in the formation of coal seams of the Olang area. Acknowledgements This study originated as part of the first author's M.Sc. dissertation at Damghan University, Iran. The authors would like to thank the Eastern Alborz company employees for providing access to mines of the Olang area and sampling. We appreciate Hamed Sanei from Geological Survey of Canada and Paul Hackley from U.S. Geological Survey for helpful reviews and very constructive suggestions. 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(2012), doi:10.1016/j.coal.2012.01.003
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