Praehistorische Zeitschrift; 2014; 89(2): 337–370 Abhandlung Jan Bemmann, Eva Lehndorff, Riccardo Klinger, Sven Linzen, Lkhagvardorj Munkhbayar, Martin Oczipka, Henny Piezonka, Susanne Reichert Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun, Orkhon Valley, Mongolia DOI 10.1515/pz-2014-0022 Zusammenfassung: Zur Nutzungsanalyse großer ovaler, erstmalig entdeckter und dokumentierter von einem niedrigen Graben-Wall-System umgebener Anlagen wurden Bodenproben auf spezifische Lipide untersucht, die Hinweise auf die Anwesenheit – hinterlassene Verdauungsreste – bestimmter Nutztierarten und Menschen in den beprobten Bereichen geben könnten. Wahrscheinlich dienten die Anlagen dem Gartenbau, sicherlich nicht der Viehhaltung; in den angrenzenden Dachziegel und Keramikscherben aufweisenden viereckigen, deutlich kleineren umwallten Anlagen siedelten Menschen. Solche ovalen Anlagen sind in der Mongolei bisher nur aus dem Umfeld der uighurischen Hauptstadt Karabalgasun bekannt geworden, deren Stadtgebiet eine deutlich größere Fläche einnimmt als bisher angenommen wurde und vielteiliger sowie funktioJan Bemmann: Rheinische Friedrich-Wilhelms-Universität Bonn, Vor- und Frühgeschichtliche Archäologie, Regina-Pacis-Weg 7, 53113 Bonn. E-Mail: [email protected] Eva Lehndorff: Rheinische Friedrich-Wilhelms-Universität Bonn, Institute of Crop Science and Resource Conservation, Soil Science & Soil Ecology, Nussallee 13, 53115 Bonn. E-Mail: [email protected] Riccardo Klinger: Geolicious GbR, Binzstraße 48, 13189 Berlin. E-Mail: [email protected] Sven Linzen: Leibniz-Institut für Photonische Technologien e. V., Albert-Einstein-Straße 9, 07745 Jena. E-Mail: [email protected] Lkhagvardorj Munkhbayar: Institute of Archaeology, Mongolian Academy of Science, Jukov Street 77, Ulaanbaatar 51. E-Mail: [email protected] Martin Oczipka: Fakultät Geoinformation, Hochschule für Technik und Wirtschaft Dresden, Friedrich-List-Platz 1, 01069 Dresden. E-Mail: [email protected] Henny Piezonka: Deutsches Archäologisches Institut, Eurasienabteilung, Im Dol 2–6, 14195 Berlin. E-Mail: [email protected] Susanne Reichert: Rheinische Friedrich-Wilhelms-Universität Bonn, Vor- und Frühgeschichtliche Archäologie, Regina-Pacis-Weg 7, 53113 Bonn. E-Mail: [email protected] nal gegliedert ist. Dieses erste stichpunktartige Ergebnis zeigt das Potential der Lipidanalysen, frühere Landnutzung zu rekonstruieren, beispielsweise Viehhaltung von acker- oder gartenbaulicher Nutzung zu unterscheiden. Gerade dieser viel zu wenig erforschte Aspekt ist für die Einschätzung der häufig postulierten ‚Abhängigkeit‘ der Nomaden von ackerbautreibenden Gesellschaften von zentraler Bedeutung. Schlüsselworte: Lipidanalyse; Nomaden; Mongolei; Gartenbau; umwallte Bereiche Résumé: Un échantillonnage du sol à peu de profondeur de la surface du terrain actuel a été effectué afin de déterminer à quoi servaient les grandes enceintes ovales, cernées d’un mur bas et d’un fossé, découvertes et relevées récemment en Mongolie. L’échantillonnage avait pour but l’analyse de lipides spécifiques à certaines espèces; en effet les données provenant de résidus de digestion fournissent de précieuses indications sur les concentrations d’animaux d’élevage spécifiques dans les zones étudiées. Les enceintes ont fort probablement été utilisées à des fins horticoles, et certainement pas pour le bétail. L’habitat humain, documenté par des trouvailles de tuiles et de céramique, se situait dans des enclos carrés et bien plus petits à proximité de ces enceintes. Les enceintes ovales n’ont été repérées en Mongolie que dans les environs de la capitale Ouïghoure de Karabalghasun. L’étendue de cette capitale est de toute évidence bien plus grande que l’on ne l’avait pensé jusqu’à présent, et la zone d’occupation avait été subdivisée en divers secteurs d’activité. Les premiers résultats de notre échantillonnage démontrent que l’analyse des lipides donne l’occasion d’aborder l’étude de la culture des céréales et des légumes sous un nouvel angle. Etant donné le peu de recherches conduites dans ce domaine, cet aspect est particulièrement important pour l’évaluation d’une ‘dépendance’ des nomades envers les sociétés agraires si souvent invoquée. Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM 338 Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun Mots-clefs: analyse des lipides; nomades; Mongolie; horticulture; enceintes murées Abstract: In order to investigate the use to which recently discovered and recorded large oval enclosures surrounded by a low wall and ditch were put, a series of topsoil samples were taken and subjected to an analysis of specific lipids; such soil chemical evidence from human and domesticated animal faeces can provide significant insights into the land use history of the areas sampled. The enclosures are likely to have been used for horticulture, and certainly not for keeping livestock. Human settlement, as attested by the presence of roof tiles and ceramic sherds, was in square, enclosed compounds nearby, and these were clearly smaller. Oval complexes have so far only been documented in Mongolia in the vicinity of the Uyghur capital of Karabalgasun. Karabalgasun was evidently much greater in extent than had hitherto been assumed and it was divided into a number of functional areas. Initial results from our targeted samples show that the analysis of lipids has much potential, offering new opportunities to elucidate land use, e.g. the cultivation of cereals and vegetables in contrast to livestock keeping. It is precisely this aspect, so far largely neglected by research, which will allow us to assess the oft-claimed ‘dependence’ of the nomads on agricultural communities. Keywords: lipid analysis; nomads; Mongolia; gardening; walled enclosures Introduction In the time of the Turco-Mongol empires the Orkhon Valley, a ritual landscape charged with meaning, achieved the status of a space legitimising power (see Allsen 1996 and Dobrovits 2012 for essential literature). For numerous peoples of the steppes, the Orkhon Valley was the centre of the world, accommodating two capital cities of two great empires – Karabalgasun and Karakorum (Fig. 1). The great quantity, diversity and size of the monuments in the Orkhon Valley reflect this enormous importance. A particularly strong concentration of walled enclosures, possibly indicating permanent settlement structures in the region, was already impressively documented in the first compilation by Radloff (1893, pl. 82) and in Maidar’s map (1970b, map 1), which was based on the work of Perlee. However, since the initial inventories of Perlee (1961/2012) and Maidar (1970a; 1970b), the walled sites of Mongolia have attracted little research interest, with the exception of the four known urban complexes of Avraga (Shiraishi/ Tsogtbaatar 2009), Chin Tolgoi (Kradin et al. 2011; Enkthur et al. 2011; Senda 2012), Karakorum (Bemmann et al. 2010; Franken 2012) and Karabalgasun (Hüttel/Dähne 2012)¹. Complexes surrounded by a wall, which can be understood as temples, residences, cities, settlements, military camps, enclosed monumental burial grounds or memorial complexes, among other interpretations, have been attested from the Xiongnu period up to recent times. These sites vary considerably in form, inner subdivision, size, wall construction, orientation, topographic location and gate construction. Since such sites are not thought to have existed in the time span from the Stone Age to the Early Iron Age, research is not concerned with their causal association with the origins and organisational structure of the nomadic empires of Inner Asia. This article presents an interpretation for the use of a specific type of walled enclosures. During preparations for a reconnaissance trip, which Jan Bemmann and Ernst Pohl of the University of Bonn, together with geographers of the Free University in Berlin, undertook in August 2006, the evaluation of Russian aerial photographs from 1972 revealed an unusually high concentration of walled complexes in the area to the north-west of the so-called citadel of Karabalgasun and to the south-east of the Spring Palace of Ögödei qaghan (reigned 1229–1241 CE) (Fig. 2). One particular feature, hitherto unknown in Mongolia, are large oval structures, several of which were located in this area. These structures are scarcely noticeable on the ground itself, given their extremely low elevation; they can only be clearly seen from the air. The project “Geoarchaeology in the steppe – reconstruction of cultural landscapes in the Orkhon Valley, Central Mongolia”² finally gave us the means and the cooperation of partners to carry out intensive research in this area and on its complexes. This took place from July 2008 to June 2011 (Bemmann et al. 2011). One of the project’s aims – under the auspices of the priority research programme “Wechselwirkungen zwischen Natur- und Geisteswissenschaften” (“Interaction between Natural Sciences and the Humanities”), funded by the Federal Ministry of Education and Research (Bundesministerium für Bildung und Forschung, BMBF) – was to determine the intensity of settlement activity within individual 1 The barely noticed publication concerning the enclosed sites dated to Kitan times located along the river Tuul River (Ochir et al. 2005, 87 ff.), which are of international significance, should also be mentioned. 2 Our expedition of 2006 was undertaken in preparation for this joint project. Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun 339 Fig. 1: a) Map of Mongolia, with the middle Orkhon Valley marked with a box; black line = modern state border. b) the Orkhon Valley showing the main sites: 1 MOR-13, 2 Karabalgasun, 3 Khöshöö Tsaidam, 4 Spring Palace of Ögödei qaghan, 5 Karakorum (graphics: Gisela Höhn and Susanne Reichert) MOR-13 Fig. 2: Walled enclosures northwest of the so-called Citadel of Karabalgasun and south-east of the Spring Palace of Ögödei qaghan. Russian airphotograph N-289, dated 24. 08. 1972, 616, with additions Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM 340 Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun periods and to investigate the relationships between cities and their surroundings. Our intentions were not only to measure the newly-discovered monuments, record them accurately in plan and 3D, and date them, but also to gain information about their construction, their use and their function. By applying the most modern techniques and the most recent analytical procedures we have made great strides (see Grützner et al. 2012; Oczipka et al. 2009). A remarkable amount of information about numerous complexes is thus available for the first time. Our aim here is to reconstruct the land use in one of the double complexes that are typical for this region; they consist of a rectangular and a bordering oval surrounding wall. We have designated that particular double complex with our own project identification code MOR-13. The surface features were identified by remote sensing and dated on the basis of pottery sherds and 14C dating; the use of the complex could be determined through the geochemical analysis of biomarkers in soil samples. We assumed at the outset that the oval features served to keep animals and that the remains of buildings were inside the rectangular features. Consequently, the biomarker analysis focused on searching for animal and human organic material preserved in the soil. Indeed biomarker analyses comprise the characterisation of remains of vegetation (plant waxes, n-alkanes) and of faeces (steroids). By combining this geochemical approach with the dates obtained and information from written sources we hope to present more detailed evidence about the land use of such structures. (J. B.) The oval enclosure, land use and function As an initial working hypothesis we assumed that the oval complexes that did not yield any surface finds were places in which livestock was gathered or kept, or – conversely – which served as a barrier to keep livestock out. One indication that this was the case is provided by the description of modern-day fences in Inner Mongolia, in which a comparable ditch-and-wall system is present (Williams 2002, 136 fig. 6,3; see also Endicott 2012 on land use in general). In order to verify this, soil samples were taken and analysed by Eva Lehndorff and her team; in doing so they introduced the analysis of lipids as a significant scientific method for archaeological research in Mongolia. A further clue is provided by a passage in The Secret History of the Mongols. In § 281 Ögödei accuses himself of making four mistakes: the last mistake he mentions is: “… being greedy and saying to myself ‘What if the wild animals born with their destiny ordained by Heaven and Earth go over to the territory of my brothers?’ I had fences and walls built of pounded earth to prevent the animals from straying” (Rachewiltz 2006, 218; 1037 p.). Persian written sources also report that Ögödei had a hunting park built in the vicinity of his winter quarters on the river Ongqin (Allsen 2006, 43 p.). Since the oval enclosures discussed here are located only a few kilometres south-east of Ögödei’s Spring Palace, ‘Gegen Chagan’, and since his sojourns in that palace were primarily for hunting (Allsen 2006, 195), some of the many walls could have been built on these occasions as enclosures for wild animals. But, if the dating of the MOR-13 square complex could also be applied to the oval enclosure associated with it, then a date in the time of the Mongol empire could at least be excluded. Determining the function of MOR-13 could provide indications of land use during the 8th century CE. Written sources mention that crops were cultivated in the vicinity of both Karabalgasun and Karakorum (see for example Barkmann 2000, 53). Several bountiful harvests are mentioned along the rivers Orkhon und Kerulen for the period from 982 to 1013 CE, when the Kitans ruled the Mongolian steppe (Wittfogel/Feng 1949, 556). It is generally assumed that nomads in Mongolia consistently grew and harvested cereals, albeit to a limited extent (Di Cosmo 1994, 1094; 1100 pp.; Fletcher 1986, 13), as Róna-Tas (1959) describes in an ethnographic study. The accounts in written sources find some support in the pollen profile from the Orkhon lowlands south of Karakorum, published by Frank Lehmkuhl et al. in 2011, in which there are two significant occurrences of cereal pollen. (J. B.) The topography of MOR-13 The wall systems of MOR-13 lie at 1367 m asl, some 900 m west of the stream Zharamt and the flood plain of the river Orkhon, at a distance of 6 km west of the present-day course of the Orkhon. They are located in Khotont sum, which belongs to Arkhangai aimag³. Almost square in shape with sides measuring c. 200 × 200 m, the complex is oriented in a northwest-southeast direction, so that the four corners point almost exactly to the four cardinal directions (Fig. 3). At least four artificial rises are located in the inner area of the square complex. The highest lies not quite in the centre and shows the strongest magnetic anomalies (Figs. 3–6). Since a high concentration of roof tiles was observed there, it is presumed that a building with a roof in Chinese style 3 Location: N 47°30’56.3’’ E 102°34’27.8’’ (UTM 48 T 317378 5265319). Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun 341 Fig. 3–4: 3 – Three-dimensional representation of the terrain profile of MOR-13 scanned with the SQUID system (graphics: IPHT Jena, Sven Linzen); 4 – 3D digital surface model (DSM) of MOR-13 (image: DLR, Martin Oczipka) once stood on this platform. In addition, higher sections of wall and platforms are recognisable on aerial photographs and on the ground as anomalies in the vegetation; they are overgrown with grass of the species Achnatherum splendens (Trin.) Nevski (Fig. 7)⁴. The wall varies in its state of preservation, and reaches a maximum height of 1 m. In some places it is so strongly eroded that the potential location of an entrance cannot be clearly determined. In the 4 Anne Zemmrich and Susanne Starke, University of Greifswald, kindly identified the plant species. southern and western corners the wall of the oval enclosure joins that of the square enclosure (Fig. 8), but because its height is so insignificant, it is only recognisable on the ground if its presence is already known to the viewer. It was only after we had undertaken a new survey flight in June 2011 and obtained new aerial photographs of the area that it became clear that the site was far more complex than had been assumed previously from inspection on the ground and from older aerial photographs and satellite imagery (Fig. 8). An oval structure directly adjoins MOR-13 on its north-eastern side; its wall is so low that it does not even show up in high-resolution elevation models. A rectangular Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM 342 Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun Fig. 5–6: 5 – SQUID magnetogram of MOR-13. Blue circles mark anomalies, which can be interpreted as building remains (graphics: IPHT Jena, Sven Linzen); 6 – Combination of magnetic and topographic data, both recorded by the SQUID system. (The magnetogram illustrated in Fig. 5 was overlaid with the altitude information illustrated in Fig. 3; brighter colour = higher altitude) (graphics: IPHT Jena, Sven Linzen) Fig. 7: Part of the wall of MOR-13 overgrown with Achnatherum splendens (Trin.) Nevski (photograph: Institute of Prehistory and Early Historical Archaeology, Bonn University) Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun 343 Fig. 8: Aerial image of MOR-13, June 2011 (image: GEOSAN and DLR). The main walls are marked with a red dashed line wall-and-ditch system that runs over a distance of 85–95 m parallel to the south-western wall of MOR-13 is also visible on aerial photographs. A wall runs from the northern corner of this wall-and-ditch, evidently connecting it with MOR-13. Possibly the rougher relief of the terrain northwest and south-east of this connecting wall indicates the presence of further anthropogenic structures. Two further oval structures are located to the north and north-west of MOR-13, at a distance of 220 m and 420 m (Fig. 24); to the west, outside the oval but connected with it, is yet another, almost rectangular complex with sides measuring 190 × 300 × 118 × 265 m. Yet more sections of wall are observable inside and to the south and south–southwest of the large oval enclosure, which cannot so far be reconstructed as connected or interrelated structures. Description of the fieldwork An intensive field survey of the square complex was conducted in September 2008, when diagnostic pottery sherds and roof tiles were collected. No artefacts were found within the oval enclosure. At the same time photogrammetric measurements were carried out, directed by Martin Oczipka, then a member of the Deutsches Zentrum Luft- und Raumfahrt (DLR) (German Aerospace Centre) in Berlin. A small drone (unmanned aerial vehicle, UAV), a so-called ‘octocopter’ (from the number of propellers) weighing less than 5 kg (Oczipka et al. 2009) was used in this survey. The geometric resolution of the ortho-images lies at 2.5–5 cm/pixel. On the basis of these vertical aerial images and with the use of photogrammetric software, Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM 344 Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun digital surface models (DSMs) and (true) ortho-photographs were created. The individual ortho-photos were combined into a continuous ortho-photo mosaic of the respective sites, and the surface models were transferred into an interactive 3D model (Fig. 4). Riccardo Klinger and Brigitta Schütt, geographers at the Free University in Berlin, drilled a deep core in one of the platforms inside the square complex (Figs. 9; 11). The core RK15 was analysed for its layer composition, soil matrix and structure. The ages of several sections of the core were determined by 14C dating on bulk and micro samples (Fig. 9). In view of the core’s 2 m length we can assume that the cultural horizon was penetrated. This is supported by the presence of a charcoal-enriched layer at a depth of 1.2 to 1.7 m beneath the present surface level of the building remains. The dating of this layer (HV-25929, marked in grey in the lowest section of the core) is in agreement with the dating of the surface finds. The date for the ancient surface provides a terminus post quem for activities at the site; we can thus reasonably assume that the platform was built in the 8th century CE. The three 14C dates from the uppermost packet of layers from the platform show a range of dates from the end of the 7th to the middle of the 9th century CE, thus circumscribing the time span in which the buildings stood or were erected on the platform. In May 2009 Sven Linzen, of the Institute of Photonic Technology (IPHT) in Jena, conducted a geomagnetic survey using the SQUID system (Superconducting QUantum Interference Device; see Linzen et al. 2009 for the system). The instrument is based on SQUID gradiometer sensors, which provide the highest magnetic field gradient resolution even at high scanning speeds over the ground. Combined with a metal-free measuring cart drawn by an all-terrain vehicle, a measurement speed of up to 60 km/h can be attained. The concurrent collection of altitude-data by means of a high precision Differential Global Positioning System (DGPS) allowed us to compute a model of the terrain without vegetation (Fig. 3). Still in 2009 Norbert Klitzsch (Rheinisch-Westfälische Technische Hochschule Aachen) conducted geoelectric and georadar investigations in order to record additional data of parts of the monuments (see Storandt 2011, 45–49). Fig. 9: Core RK 15 with radiocarbon dates. Layer from surface to depth of 80 cm: CL-Si, randomly embedded and solidifying S-mg (focal point at a depth of 25 cm), 10YR5/2–4/4 (deposit with 10YR7/2 at a depth of 67–80 cm), HCL++, Org+, dry, not rollable; deposit from 80 to 105 cm: Si-fS, cG rarely embedded, 10YR7/3, HCL+, Org+, very dry, not rollable; deposit from 105 to 120 cm: Si-fS, well rounded mG-cG, 10YR7/2, HCL+, Org+, roots, dry, not rollable; deposit 120 to 170 cm; Si-fS, rare well rounded mG, 10YR6/2–4/2 8 darkening, monotonically 145–170 cm), HCL+ (decreasing), Org(+), charcoal-layer at 158 cm, dry, not rollable; deposit from 170 to 205 cm: Si-fS, well rounded mG (decreasing diameter), 10YR7/3, HCL++, Org 0, slightly layered in colour, dry, not rollable; deposit 7 from 205 to 210 cm: Si-fS, rare fG, 10YR6/6, HCL+-, Org 0, dry, not rollable (graphics: Riccardo Klinger) Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun 345 directed by Jan Bemmann and Martin Oczipka in June 2011 in collaboration with the company Geosan in Ulaanbaatar. It must be stressed that it is the interplay between different prospection techniques that enabled us to succeed in producing an almost entirely non-destructive, initial assessment of hitherto unknown archaeological monuments. (J. B.; R. K.; S. L.; M. O.) Magnetic SQUID prospection of MOR-13 Fig. 10: Taking a soil sample with a bulb digger for biomarker analysis (photograph: Institute of Prehistory and Early Historical Archaeology, Bonn University) In May 2010 archaeologists of Bonn University and the Mongolian Academy of Science (MAS) took soil samples for lipid analysis, following the guidelines of Eva Lehndorff, Institute of Crop Science and Resource Conservation (INRES) in Bonn. Sediment samples were taken with a bulb digger and put in plastic containers (Fig. 10). Four samples were taken in each of five places, inside and outside the two complexes which we had identified by that time (Fig. 11). The processing and analysis of the samples were carried out in the laboratory of the INRES in Bonn. Lastly, in September 2010, a small section was cut through the wall of the large oval complex and a further trench was cut through the rectangular complex MOR-13 from the wall’s crown down to the ditch, to ascertain how the wall was constructed and to gain information for optically stimulated luminescence (OSL) sampling⁵. The work on the wall trenches and the recording of the profiles were in the hands of Lkhagvardorj Munkhbayar, Institute of Archaeology, MAS, and Henny Piezonka, fellow employee of the project. Because the size and complexity of the immediately adjacent complexes were unknown to us at the time, we limited the number of soundings to these two trenches. We could nevertheless show without any doubt that the oval enclosures were low, now extremely flattened, bank-and-ditch constructions and hence were man-made. Valuable supplementary information for the interpretation of the complexes and their integration in the region were gained from aerial photography; this was achieved in a project funded by the Gerda Henkel Foundation and 5 The OSL samples are being processed and analysed by Dr Saran Solongo of the Mongolian Academy of Science in the Institute of Geography, University of Köln, in collaboration with Dr Daniela Hülle and Prof Dr Helmut Brückner. An area of 300 × 300 m covering the MOR-13 walled enclosure was prospected with the motorised SQUID system within five hours of measurement on one day in May 2009. MOR-13 was one of several walled enclosures, which were investigated with the system in different regions of the middle Orkhon Valley. The recorded magnetic maps of the enclosures differ strongly in terms of the signatures of the ramparts and the enclosed inner areas. The magnetogram of MOR-13 is for the most part dominated by a grainy structure with amplitudes of 2–10 nT/m. This configuration of dozens of point-shaped anomalies becomes very regular with a spacing of 2–3 m, especially outside the enclosure in the north and the south-west (Fig. 5). We think that these magnetic anomalies have no anthropogenic origin, but were caused by a geological frost boil pattern in the subsoil. Four clusters of point-shaped magnetic anomalies with high amplitudes of up to 50 nT/m were detected inside the enclosure. One of them is located exactly in the enclosure’s centre, and a second about 43 m south of the centre. The two other clusters of anomalies are located immediately on the inner side of the bank, close to the southern corner (Fig. 5). Fired bricks, roof or floor tiles can be assumed to have caused the magnetic signals because of the intensity and shape of the anomalies. A comparison with the accurately recorded topographic map of the area (Fig. 3) shows the exposed position of the magnetically detected building remains. However, several other exposed positions inside the enclosure do not show magnetic evidence of fired materials (see combined illustration of Fig. 6). Thus, we conclude that the four magnetic clusters of anomalies indicate buildings of higher rank inside the enclosure. The area of the embankment itself has only a weak magnetic representation. A long-periodic signature of small amplitude is detectable in the north-western and south-eastern sector (compare Fig. 5 with Fig. 6). We can conclude from this that an inner bank structure without sharp vertical margins, and with only a weak magnetic contrast with the materials used, existed. We found similar bank properties at further walled enclosures in the Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM 346 Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun Fig. 11: Map of MOR-13 with location of the two trenches, the soil samples, and the core drilling (graphics: Susanne Reichert) surrounding of MOR-13, for example at MOR-2, some 12 km to the north (see Grützner et al. 2012). However, walled enclosures with pronounced magnetic contrasts in the upper part of the bank slopes can also be found, for example at MOR-9, 25 km southeast of MOR-13 (Lungijn dörvölzhijn [MOR-9]; see Bemmann et al. 2011). The latter anomalies classify the bank as possessing an (intact) rammed earth core. (S. L.) The wall trenches Trench 1 was dug into the bank of the oval structure. The trench was located on the northern side of the structure, some 0.4 km west-northwest of the rectangular walled en- closure (see Fig. 11). The 1 m wide trench started on the crest of the bank and extended 5.5 m towards the northwest. Unlike the faint traces of the structure visible above ground, the section of the trench provided clear information about its man-made features (Fig. 12). Under a very thin layer of topsoil the remains of the bank were found in the south-eastern half of the trench and consisted of grey-brown, very compact sandy loam with some gravel. To the north-west of it, a shallow, U-shaped ditch with a maximum depth of 0.5 m below the modern surface was visible. The bottom fill consisted of a band of yellow loose sandy gravel; located above it were layers of grey-black, mostly loose sand and sandy loam. At the north-western end of the trench, a shallow pit filled with grey-brown to black-grey compact silty sand had been dug into the Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun 347 Fig. 12: MOR-13, profile of Trench 1 through the oval enclosure (drawing: Henny Piezonka) Fig. 13: MOR-13, profile of Trench 2 cut through the square enclosure (drawing: Henny Piezonka) subsoil. Its stratigraphic relationship with the bank and ditch cannot be determined. The only artefact discovered during the excavation is an unglazed ceramic handle (Fig. 19,7). An OSL dating sample was extracted from the bank layer in metre 1 of the north-east profile of the trench (see Fig. 12). The second MOR-13 trench was located on the northeastern bank of the rectangular enclosure (see Fig. 11). The 1 m wide trench started on the crest of the bank and extended 12 m north-east towards the exterior of the enclosure, where a slight depression indicated the presence of a surrounding ditch. In the profile (Fig. 13), the earthen bank is visible in the south-western part. It was covered by a thin layer of topsoil. Its base lay c. 1.0 m under the surface and on top of a very homogenous layer of dark brown, not very compact silty sand, which might represent either a buried natural topsoil, or an anthropogenic horizon predating the construction of the bank. The bank was erected by subsequent heaping of various materials. Most of these layers consisted of grey to ochre-grey, rather compact loamy sand with a high proportion of gravel; some of them also contained charcoal and pieces of burnt clay. The north-eastern half of the profile was dominated by a shallow, ditch-like depression. It was cut into the subsoil to a depth of no more than 0.75 m, measured from the old ground surface (top of the dark-brown layer underneath the bank described previously). The north-eastern edge of the cut lay beyond the limits of the trench and hence its width cannot be determined. As to function, it is not clear whether the depression was actually intended to be a ditch, or whether it is merely the area where material for the bank was excavated. The depression was filled with various layers of dark grey to brown loamy sand. In the area closest to the bank, these layers were very rich in archaeological material, including butchered and partly charred animal bones, charcoal, burnt loam and deco- Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM 348 Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun rated pottery (Figs. 16,44; 17,34; 18,35. 45–46). An interesting artefact among these finds is a broken toggle made of antler (Fig. 20,59)⁶. The abundance of finds in these layers indicates that the depression was used as a rubbish pit for debris thrown from the bank. It is from one of these archaeologically dated layers that the OSL sample was taken. (H. P.; L. M.) Dating the artefacts A general comment from a methodological perspective about the existing dating schemes for the material culture of Mongolia is necessary: the division into periods in archaeology, before information from historical records is available, was based on characteristic types of archaeological monuments, especially the parts of burial structures that are visible above ground. Beginning with the Xiongnu period (209 BCE–2nd century CE), the temporal division is based on dates conveyed in the written documents about the existence of the respective empire or dynasties, and the nomenclature follows the ethnonyms. This has led to apparent gaps in the cultural sequence (see Rogers 2007, 257), because there were long intervals in which there was no unifying central power. Schematically defined pottery types are attributed to these historically defined periods of time. The sherds derive as a rule from surveys or recovery of unstratified finds. A relative pottery sequence, and recognition of coeval forms and their duration, can only be established through the study of cultural layers from settlement excavations, which however are largely lacking or are confined to Kitan or Mongol times⁷. For the period of interest here, the 6th to 9th centuries CE, a distinction is made between the Turkic empire (552–742 CE), subdivided into a first empire (552–630/659 CE) and a second empire (682–742/766 CE)⁸ and the Uyghur empire (744–840 CE). So far no settlements with permanent buildings or complexes are known for the Türks in Mongolia (Stark 2008, 56). With Karabalgasun the largest urban complex in Mongolia – the largest known to this day – emerged under the Uyghurs, encompassing a surface area 6 In the Sayan-Altai region, such items are commonly found in burials of the Turkish period dating between the 6th and the 10th century CE. They were used as part of fetters for tying the feet of a horse (Kubarev 2005, 136–137). In Siberia, similar toggles have remained in use until ethnographically-documented times (Kirpichnikov 1973, 78, fig. 45). 7 The first suggestions for the temporal division of pottery from settlements in the Xiongnu period are now available (Wright 2011; Ramseyer 2013). 8 The second date refers to the independent and longer lasting western Old Turkic qaghanate. of more than 32 km2. Ever since Khudiakov and Tsėvėėndorzh’s study (1975) the stamp-decorated ceramic sherds gathered there have been considered as diagnostic for the identification of settlements and graves of Uyghur times. The danger of circular reasoning, i.e. when stray finds from a complex dated with the aid of written sources are used to describe the material culture of this period, is obvious. The insufficiently researched Old Turkic period in Mongolia (summary of grave finds in Törbat/Odbaatar 2012; a good general overview in Stark 2008) is supposedly characterised by hand-made pottery, which displays fingernail impressions underneath the rim or a coarse incised zigzag decoration or St Andrew’s cross pattern on the body or neck (Stark 2008, 106 pl. 19). Complete vessels have hitherto been found solely in burial contexts. Until a substantiated scheme with absolute dates is established, the duration of the individual ceramic forms and decorations will remain uncertain. At the moment, this results, for example, in a stampdecorated sherd from Khöshöö Tsaidam (the memorial complex of Kül Tegin) being proffered as evidence that the Uyghurs sought out or made use of that site (Šmahelová/Pohl 2009), a proposal submitted without making the context of the find clear at the outset and thus later considered to be secure⁹. On the basis of the radiocarbon dates from the drilled core (Fig. 9), the MOR-13 complex may be dated in terms of absolute chronology to the 8th century CE; it could have been built during the late phase of the second Türk qaghanate or the first phase of the Uyghur empire. In the latter case the traditional dating of stamp-decorated ceramic finds would be in agreement. Both the Old Turkic peoples and the Uyghurs belonged to the same language group; the latter – like their predecessors – used the Old Turkic runic script. The custom of burying a man and a bridled horse in the same grave is similarly common to both groups. During the second Türk qaghanate as well as during the Uyghur empire the Orkhon Valley was the centre of power. In view of so many commonalities the question arises as to why the form, 9 Further stamp-decorated sherds are known from the complex of Kül Tegin (Šmahelová 2009, 336 f. figs. 13–14). During investigations at the Bilgä Qağan memorial complexes within a Turkish-Mongolian project, fragments of a large ceramic vessel with stamped decoration were found in the enclosing ditch near the entrance to the enclosed part of the memorial complexes, excavation area NG 268B. The excavators similarly assigned the ceramic vessel to Uyghur times (Gömeç 2005, 43; 106–107 photographs 68–70; 211). A sherd bearing a stamped decoration – lozenge-shaped designs – was also found in the centre of the Bilgä Qağan complex, excavation area NG 264A; according to current opinion, it was dated to Uyghur times too (TICA 2003, 56; 96 fig. 15,2). Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun decoration and quality of pottery should have altered abruptly with a change in the ruling tribes? In my opinion, the not negligible quantities of ceramics in both memorial complexes at Khöshöö Tsaidam indicate that these so-called Uyghur ceramics were already being produced during the second Türkic qaghanate. In order to give stimulate research on pottery and to impart an impression of a typical spectrum – in our opinion – of ceramic sherds from a settlement site, all the items found at MOR-13 are listed here, most are illustrated, and they are statistically evaluated. Nevertheless, the available database is still far too small to meet all the methodological requirements of pottery analysis. (J. B.) 349 Fig. 14: Percentage distribution of the pottery groups (Excel diagram) (graphics: Susanne Reichert) Ceramics from MOR-13 The evaluation of the ceramics allows some initial observations, which, however, cannot be used as chronological indicators. In total 118 ceramic sherds were found, of which 72.9 % were collected as stray finds during pedestrian surveys (n 86). The remainder comes from the excavation trenches 1 and 2 (27.1 %; n 32). Trench 1 yielded only one fragment of a handle (cat. no. 7, Fig. 19,7); trench 2 was richer in finds: 31 ceramic fragments were found there, mostly in the dump layers of the ditch (Fig. 13, layers 6–9). Formally the fragments can be attributed to the following vessel parts: five rim sherds (cat. nos. 1–5, Fig. 19,1–5), two handle fragments, one being a body sherd with part of the handle (cat. nos. 6, 7, Fig. 19,6–7), 108 body sherds of unglazed earthenware (cat. nos. 8–53, Figs. 16–18) and three glazed or engobed body sherds (cat. nos. 54, 55). The latter are stray finds and of later date, presumably of the period of the Mongol empire. Because of the highly fragmented nature of the sherds it was not possible to refit any sherds to reconstruct vessels. The interpretation of the ceramics is further restricted by the fact that 48.7 % of all sherds were inaccessible and could not be comprehensively documented¹⁰. Thus in these cases we are unable to undertake detailed analyses concerning, for example, the fabric of the pottery. Closer examination of the fabric shows that there are no significant differences between decorated and undecorated body fragments; all earthenware sherds are fairly uniform in their composition. They can be broadly 10 The sherds were photographed and described anew according to uniform criteria in 2012 in the store of the Institute of Archaeology, MAS. Part of the material was no longer accessible. In this case reference was made to notes and photographs made during the expedition. Ceramics still available for analysis was documented along the criteria as proposed by Kunow et al. 1986. Fig. 15: Quantification of single basic motifs (Excel diagram) (graphics: Susanne Reichert). divided into three groups according to their surface colour: grey wares constitute the bulk of the sherds, followed by red wares, whereas the percentage of the third group, yellowish/brown coloured ware, is negligible (Fig. 14). At this stage the meagre database does not allow a more detailed classification, which should take other criteria into account such as the type and amount of temper. About one-third of the body sherds bears characteristic decoration (36.1 %; n 39), through which these fragments could be conventionally dated to Old Turkic and Uyghur times. Decorative motifs range from simple horizontal lines, to grooves, to various stamped patterns like small lozenges in a dense pattern, concentric lozenges, arcs and clusters of rectangular lines (Fig. 15). Some of these individual motifs are combined, for example, horizontal lines and lozenge stamps (cat. no. 34, Fig. 17,34) or horizontal lines and slanted short grooves (cat. no. 45, Fig. 18,45). Aside from horizontal lines, concentric rhombic stamps are the most frequent motif (Fig. 15)¹¹. Apart from 11 Decorations were split into single components for the analysis; therefore, the total number of motifs does not equal the amount of decorated sherds. Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM 350 Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun Fig. 16: Decorated sherds. The numbers refer to the catalogue in the appendix. Scale: 1:1 (photographs: Susanne Reichert; graphics: Gisela Höhn) Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun Fig. 17: Decorated sherds. The numbers refer to the catalogue in the appendix. Scale: 1:1 (photographs: Susanne Reichert; graphics: Gisela Höhn) Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM 351 352 Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun Fig. 18: Decorated sherds. The numbers refer to the catalogue in the appendix. Scale: 1:1 (photographs: Susanne Reichert; graphics: Gisela Höhn) Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun Fig. 19: Ceramics: 1–5 rim sherds; 6–7 handles. The numbers refer to the catalogue in the appendix. Scale: 1:1 (photographs: Susanne Reichert; graphics: Gisela Höhn) Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM 353 354 Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun Fig. 20: Miscellaneous finds: 56–58 iron artefacts; 59–60 bone artefacts; 81 roof tile fragment. The numbers refer to the catalogue in the appendix. Scale: 1:2 for 56–58 and 60; scale 1:1 for 59 and 81 (photographs: Susanne Reichert; graphics: Gisela Höhn) the ‘small lozenge or angular stamp pattern’ motif, every basic motif was found at least once in trench 2. The extent to which this has any bearing on the chronological setting of this type of decoration is questionable, as the main part of these finds derives from the ditch of trench 2, which was probably filled over a considerable span of time. Furthermore, there is probably no direct connection between the occurrence of the different motifs and the three preliminary types of ware. At least red and grey wares are combined with every kind of decoration, whereas angular stamped patterns and concentric rhombic stamps do not occur together with yellowish-brown ceramics. This might be due to the scarcity of this ware. In order to obtain a more comprehensive picture of the Old Turkic and Uyghur ceramics systematic settlement excavations with stratified ceramic assemblages are sorely needed. (S. R.) Organic-geochemical interpretations of soils from MOR-13 Soils are an archive that provides ecosystem information, for example about the history of the vegetation and land use. A huge proportion of this information is stored in the organic residues of organisms living on and in the soil. Soil organic matter (SOM) consists in part of macromolecular vegetation and biomass debris. However, a high proportion of this is degraded in time-scales of days to weeks (fast carbon cycling). Nonetheless, some hydrophobic organic compounds (lipids) remain in the soil for longer periods; they are part of the slow-cycling organic carbon pool. Physical processes protect organic matter in microand nano-pores of soils (Kaiser/Guggenberger 2003), and inorganic components such as iron oxides, for example, act as a keeper of soil organic matter via chemical bonding (for a review see Six et al. 2004). Hence, in soil a stabilisation of SOM was observed within the millennium scale (see for example Mikutta et al. 2009). Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun 355 Fig. 21: Main factors influencing steroid patterns in soil: i) diet, i.e. zoo- or phytosterols feed omnivore and herbivore animals, ii) the digestion process respectively produces C27- or C29-5ß-stanols. Hydrogenation of the carbon = carbon Δ5 double bond in sterols (as highlighted in cholesterol) produces 5ß-orientated carbon-hydrogen bindings in respective stanols. The side chains (positioned at the 12th carbon atom) of phyto- and zoosterols keep their specific structure (i.e. number of carbon atoms) and allow their application as mammal biomarkers (graphics: Eva Lehndorff, INRES Bonn University) Tab. 1: Names and synonyms for common steroids and their potential origin (Eva Lehndorff, INRES Bonn University) Trivial name Name Prevalent source Cholesterol Campesterol Stigmasterol ß-sitosterol Coprostanol Epicoprostanol Cholestanol Ethylcoprostanol (5ß-Stigmastanol) Stigmastanol cholest-5-en-3ß-ol 24ß-methylcholest-5-en-3ß-ol 24ß-ethylcholest-5,22-dien-3ß-ol 24ß-ethylcholest-5-en-3ß-ol 5ß-cholestan-3ß-ol 5ß-cholestan-3a-ol 5a-cholestan-3ß-ol 24ß-ethyl-5ß-cholestan-3ß-ol Zoosterol, cell walls of higher organised organisms (“meat”) Phytosterol, cell walls of plants Phytosterol Phytosterol Omnivore digestion Omnivore digestion Digestion product of soil microbes Herbivore digestion 24ß-ethyl-5a-cholestan-3ß-ol Digestion product of soil microbes Some of these slow-cycling compounds, the lipids, are indicators for their precursor material and can thus be used as biomarkers for a certain type of vegetation, microorganism or mammal. For example, plant waxes (consisting of a homologue series of n-alkanes) have shown specific n-alkane patterns according to the prevailing type of vegetation cover, e. g. grass and herbs (predominance of n-C31-alkane) or deciduous forest (n-C29-alkanes; Schwark et al. 2002). Accordingly, there are studies that employ n-alkanes as vegetation markers in loess and lake sediments (Schwark et al. 2002; Liu/Huang 2005). More recently the ratio of long- to short-chained n-alkanes was used as a marker for anthropogenic activity in archaeological soil samples (Eckmeier/Wiesenberg 2009). Steroids, built of a cyclic ‘sterane carbon body’ and a source-specific carbon side chain, may serve as mammal biomarkers, so-called faecal markers (Grimalt et al. 1990; Fig. 21). Sterols are produced by animals (27 carbon atoms = zoosterols, for example cholesterol), fungi (28 carbon atoms, for example ergosterol) or by plants (29 carbon atoms = phytosterols, for example stigmasterol; Tab. 1). During digestion the carbon-carbon double bond at the second sterane ring is transferred via hydrogenation to energy and a carbon-hydrogen bond at the 5th carbon atom (Gaskell/Eglinton 1975; Fig. 21). According to the digestive process this ends up in either 5α-stanols in bacterial residues (C-H bond opposing orientation of the functional group (-OH)) or 5ß-stanols in mammal faeces (C-H bond parallel to orientation of the -OH group; preferentially produced by animals; Fig. 21). Further discrimination between herbivore and omnivore faeces in the environment can be achieved by comparing the abundance of C27- to C29-5ß-stanols (for example, coprostanol versus ethylcoprostanol; Fig. 21; Tab. 1), as shown for slurries, agricultural soils and water samples (Grimalt et al. 1990; Bull et al. 2000; Derrien et al. 2011). Accordingly, Bull and colleagues (Bull et al. 1999; 2001) managed to distinguish soil- (microbe-) derived steroids from gut-derived steroids and could show that coprostanol is a feasible marker for the input of human faeces in archaeological soil samples. Also other studies successfully employed steroid pattern analysis in archae- Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM 356 Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun Fig. 22: Chromatogram of a lipid extract showing the steroid elution series in sample MOR-13, site 1 (outside the archaeological structure). Abundance of coprostanol and ethylcoprostanol indicates contributions of omnivore and herbivore faeces to the soil lipids, respectively (green = n-alkanes, purple = n-alkanols; orange = steroids) (graphics: Eva Lehndorff, INRES Bonn University) ological soil samples (Birk et al. 2011; Shillito et al. 2011; Lombardo et al. 2013). In the Orkhon Valley slight morphological rises in the landscape occur, which are most likely to represent the remains of Uyghur settlement. A low vegetation cover, low population density and long severe winters make a uniform preservation and accumulation of soil lipids in this area quite possible. Hence, we hypothesise that soil lipids have archived the integrated land use history at least since the time of Uyghur settlement. Here we employ elemental C and N analysis as well as n-alkane and steroid analyses of topsoil material to elucidate land use in a potential Uyghur settlement-pasture complex at MOR-13. Materials and methods Samples The sampling design was adjusted to the morphological structures found at the MOR-13 site (Fig. 11). At five locations four replicate samples of the top 0–10 cm of the soil were taken (20 samples in total Fig. 10). Sites 1 and 3 were located outside an oval structure that had a diameter of c. 700 m. Sites 2 and 4 were located within the oval structure (potentially pasture land), and site 5 comprised four replicates of soil within a square structure (potential settlement, c. 200 m²). Samples were air-dried, sieved to >2 mm, freed from roots, ground and stored deep-frozen before analysis. Soil carbon and lipid analysis The total carbon concentration was analysed by an elemental analyser (Fisons Instruments). The soil organic carbon content (SOC) was calculated by subtraction of volumetrically-determined inorganic carbon contents (treatment with 15 % hydrochloric acid). Lipid extraction was done by accelerated solvent extraction (ASE310, DIONEX, Idstein, Germany) with dichloromethane:methanol (9:1, v/v). Steroids were derivatized with N,O-Bis (trimethylsilyl) trifluoroacetamide (BSTFA), employing pyridine as a catalyst (at 70° C for 3 hours). The n-alkane and steroid patterns were then analysed by gas chromatography-mass spectrometry (Agilent 5971 GC-MSD; HP5-MS column, 30 m in length, 0.25 mm inner diameter, 0.25 μm film; temperature program from 70° C to 320° C with 7° C per minute). Alkanes and steroids were identified by typical mass spectra (lipidlibrary.aocs.org), elution series (Fig. 22) and comparison to data in the literature (Shillito et al. 2011; Lombardo et al. 2013). Lipid contents were expressed in percent of the sum of the respective lipid class (data sheet in the appendix, Tab. 2). Results and discussion According to the evidence from aerial photography we hypothesised that samples could be grouped according to the concentration and quality of their organic matter into i) offsite samples (sites 1 and 3), ii) potentially former pasture land (sites 2 and 4), and iii) a settlement area (site 5). Soil organic carbon (SOC) The SOC concentrations in topsoil were assumed to be higher if soil received above natural organic matter input by, for example in-situ manuring by cattle in the MOR-13 oval structure or domestic waste application in the settlement area (Haynes/Naidu 1998). However, SOC concentrations did not follow this systematically. The SOC varied between 1.3 and 6.7 % of dry soil weight (Tab. 2). At sites 3 and 4 the SOC concentration in topsoil was highest; however, these sites are likely to have had a different land use (pasture versus natural land). This suggested that either the SOC contents were not specific for land use, or that land use inside the oval structure was not all that different from that outside. Soil lipids Organic manuring and intensive agricultural land use were shown to positively affect lipid contents in soil, even when some centuries of natural land use had elapsed (Simpson et al. 1999). In a Roman villa complex in south- Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM replicate A B C D A B C D A B C D A B C D A B C D subsite 1 1 1 1 2 2 2 2 3 3 3 3 4 4 4 4 5 5 5 5 off-site off-site off-site off-site pasture pasture pasture pasture off-site off-site off-site off-site pasture pasture pasture pasture settlement settlement settlement settlement comment 2,2 2,7 1,3 2,1 1,8 2,4 4,5 2,1 1,2 2,3 5,8 5,9 2,4 4,9 6,7 4,1 3,1 3,1 1,9 TOC % 0,3 0,4 0,2 0,6 0,4 0,4 0,3 0,3 0,2 0,3 0,1 0,1 0,2 0,2 0,2 0,2 0,4 0,5 0,3 0,8 0,9 1,0 0,7 3,4 0,5 0,6 1,3 3,4 0,7 2,1 1,0 2,9 0,6 2,6 2,3 4,6 0,5 0,8 1,7 0,6 short-/long coprochained stanol n-alkanes 2,2 1,7 5,9 0,0 4,1 1,4 0,0 3,7 1,0 2,0 0,0 2,4 1,3 2,0 1,8 3,3 2,3 9,8 4,4 12,0 epicoprostanol 74,1 38,2 62,2 73,7 69,3 80,6 56,0 58,0 35,5 52,9 37,0 39,8 72,7 40,3 26,7 38,4 70,0 64,0 50,4 66,1 cholesterol 0,9 3,3 4,0 2,6 0,8 2,9 6,6 3,6 1,4 3,6 3,5 5,3 1,9 9,4 6,0 4,6 2,8 2,0 5,7 2,1 0,0 14,4 2,8 3,1 1,4 1,3 4,2 2,6 2,5 2,7 4,0 2,4 1,8 4,7 4,2 3,5 0,8 0,9 0,0 0,5 0,0 0,8 1,5 0,9 0,0 0,0 4,3 1,3 5,7 3,6 5,8 6,6 1,5 4,4 8,5 2,4 2,1 1,2 0,0 1,0 6,1 6,5 7,5 4,1 5,5 3,7 9,1 7,4 4,5 4,1 6,9 10,3 7,9 12,2 15,2 14,2 5,5 8,7 11,0 11,4 0,0 25,2 7,9 7,2 4,9 3,0 8,0 11,6 43,8 22,5 31,5 21,0 4,0 11,7 24,6 21,5 9,2 7,9 12,0 3,3 12,4 7,5 6,4 4,2 6,0 5,5 8,5 6,8 4,0 5,6 7,6 7,6 7,1 10,8 8,8 6,3 5,5 3,5 12,3 2,3 cholestanol ethylcopro- campesterol stigmasterol ß-sitosterol stigmastanol stanol Tab. 2: Soil organic carbon and lipid proportions in samples from the MOR-13 site. Total, organic, and inorganic carbon (TC, TOC, TIC) are given in % of sample dry weight. The ratio of short- to long-chained alkanes is calculated by: (Σn-C15–n-C22)/(Σn-C23–n-C33). Sterol contents are given in percent of the sum of all sterols (Eva Lehndorff, INRES Bonn University) Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM 357 358 Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun Fig. 23: Box-plots: a) the highest concentration and variation in soil organic carbon was observed at the adjacent sites 3 and 4 (approximate distance: 100 m); b) the proportion of the short-chained n-alkane is highest at site 5; c) ethylcoprostanol as a herbivore marker is almost entirely absent from the settlement area; d) epicoprostanol as an omnivore marker dominates the sum of total steroids in the settlement area (graphics: Eva Lehndorff, INRES Bonn University) ern England pronounced decrease in n-alkane and steroid contents from the villa to the surroundings were found (Simpson et al. 1999). For the n-alkanes the proportion of long-chained, odd-numbered homologues (n-C29, n-C31, n-C33) was elevated in the surroundings of the villa, that is, on managed soil. However, at MOR-13 the opposite was observed: in the settlement area even-numbered, shortchain n-alkanes had the highest percentage in the sum of n-alkanes (Fig. 23b). This indicates that land use did not include intensive soil management in the oval area; in other words, no intensive crop production and manuring were practised at MOR-13. Anthropogenic modification of organic matter, probably by fire, was shown to increase the proportions of the even- and short-chain n-alkanes (n-C16 and n-C18; Eckmeier/Wiesenberg 2009). Hence, here the elevated con- tribution of these n-alkanes at site 5 gave a first indication of anthropogenic land use in the square settlement structure. The steroidal component of soil organic matter is also dependent on arable land use. In the study of Simpson et al. (1999) plant- and digestion-derived steroid contents decreased significantly with distance to the farm site. At MOR-13, the steroid patterns of sites 1–4 (off-site and potential pasture land) were dominated by phytosterols (for example, campesterol, Tab. 2) and a 5ß-stanol of herbivore origin (ethylcoprostanol, Fig. 23c). Site 5 (settlement structure) showed a notable enrichment of epicoprostanol (omnivore faeces), while being depleted in ethylcoprostanol (Fig. 23c and d). Traces of coprostanol (the main marker for human faeces input into the soil) are likely to be abundant in all samples (Tab. 2); however, Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun 359 Oval and round enclosures in the Orkhon Valley – perspectives overview (Fig. 24)¹². As a rule, the large oval enclosures joined to an adjacent and distinctly smaller quadrangular complex. The latter shows evidence of several platforms and yields surface finds. On the ground we discovered that the MOR-15 and MOR-16 complexes similarly connected with an oval enclosure, whose spectrum of ceramic forms resembles that of MOR-13. A date in the same period for these complexes seems likely¹³. Until now no closemeshed survey of the surroundings of Karabalgasun had been undertaken, and hence we cannot make any statements based on surface finds concerning the use of the areas between the walled enclosures. If we apply our findings – i.e. that the oval enclosure MOR-13 was used as a large fenced garden area and that the small square walled sites represent human settlement sites – to other complexes, then we can identify possible areas that served to produce plant foods and supply foodstuffs to the urban population of Karabalgasun. And so the image of a core city emerges with agricultural farms scattered around, a context that matches well the description of Tamīn Ibn Bahr: “… this is a great town, rich in agriculture and surrounded by rustāqs full of cultivation and villages lying close together” (Minorsky 1948, 283)¹⁴. The statement of Jagchid and Hyer (1979, 311) is also worth noting: “The vegetarian doctrine of the religion [Manichaeism] caused the Uighur to try to develop gardening in the vicinity of their capital in Mongolia; but from the records available it is unclear as to what happened with the experiment”. This theory of garden use should be verified at other sites in the future. A second hypothesis concerns the extent of the Uyghur capital. Since the surface material collected suggests that the enclosed sites north-west of Karabalgasun are contemporary with the town, and given that the best and sometimes only parallels for the shape and size of these enclosures are found in the area of the town of Karabalgasun itself, we propose that the Uyghur capital encompassed a far larger area than that proposed in older studies (Radloff 1892, pl. 27) and in recent works (Hüttel/Erdenebat 2009, 18; 35 fig. 32). Thanks to large-scale aerial surveys and the generation of ortho-images over an area of 714 km2, it was possible to compare the complex known as MOR-13 with other complexes identified in aerial photographs. While evaluating Russian aerial photographs taken in 1972 we noticed that comparable structures can be identified only in Karabalgasun and in the area north-west of the city. This finding was confirmed, and the close interconnection with the surroundings of the city is visible in the cartographic 12 Prior to this only a small part of the mapped complex had been inspected on the ground. The mapping is based on images taken during aerial surveys in 2011. 13 When other walled enclosures in the area between the Spring Palace of Ögödei qaghan and Karabalgasun yielded pottery sherds (MOR-14, 17, 79, 80), a spectrum similar to that of MOR-13 was recovered. 14 Some authors, for example Waugh 2010, 103 doubt that this description refers to Karabalgasun. they did not exceed the limits of reliable detection and analytically coincided with the n-C27-alcohol (Fig. 21). From the preferential abundance of epicoprostanol we assume that domesticated, omnivore animals, for example, dogs, pigs or humans used the square structure in Uyghur times. The uniformly elevated abundance of herbivore faeces (indicated by ethylcoprostanol) in off-site locations (sites 1 and 3) and within the oval area (sites 2 and 4) indicates that this is rather a natural signal and that the oval area was not used to fence in a herd of domesticated animals. Conclusions The lipid patterns in the topsoil of a potential settlement area from the Turko-Mongol era differed notably from those in the surrounding soil. A predominance of even- and short-chained n-alkanes and epicoprostanol indicated an input of anthropogenically-modified organic matter, likely to have been altered by fire, and omnivore faeces; this then confirms human settlement in a location that has not been under land use since Uyghur times. The uniform abundance of herbivore markers (especially ethylcoprostanol) in a potential grazing and non-grazing area negates the ‘grazing hypothesis’ and suggests instead that the settlement was surrounded by an oval, fenced garden area. The results from this study reveal the high potential of the sampling design when examining topsoil as an archive for land use history. Thus, in a next step the analytical approach should be extended, for example to bile acid and fire residue (black carbon) analysis, to achieve a more detailed differentiation of the sources of the faecal remains and land use (Lauer et al. 2014). (E. L.) Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM 360 Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun Fig. 24: Karabalgasun and its surroundings. All the sites with walled enclosures which were identified in the field or on aerial images are mapped (graphics: Susanne Reichert) Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun The entire usable space to the north-west of the city, whose extent was contingent upon and constrained by the natural environment, should be ascribed to the city and its peripheral districts¹⁵. This would greatly add to the discussion of the topography and division of the Uyghur capital into quarters. (J. B.) References Allsen 1996: T. T. Allsen, Spiritual Geography and Political Legitimacy in the Eastern Steppe. In: H. J. M. Claessen/ J. G. Oosten (eds), Ideology and the Formation of Early States. Stud. Human Soc. 11 (Leiden 1996) 116–135. – 2006: –, The Royal Hunt in Eurasian History (Philadelphia 2006). Barkmann 2000: U. B. 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Appendix Compilation of sherds and artefacts from MOR-13 Finds nos. 1, 8–22, 47, 56, 57, 61, 76, 80, 82, 83, 86 are inaccessible. Location of finds: nos. 1, 2, 6, 8–33, 47–49, 54–57, 61, 62, 80, 81, 83, 84, 86 = stray finds. Stray find no. 82 was found c. 300 m north of the walled enclosure. Nos. 3–5, 7, 34–46, 50–53, 58–60, 63–79, 85 were from different sections/excavations of test trenches in autumn 2010. 1. Rim sherd, unglazed ceramic; fabric: tempered with fine sand, ochre-grey, slightly porous; surface: well smoothed with slip, horizontal traces of smoothing; firing: medium; rim diameter 17 cm. Inv.no. MOR-13/F2008/1–1 (Fig. 19,1). 2. Rim sherd, unglazed ceramic, earthenware; rectangular rim, flanged outwards; traces of working: inside and outside fine horizontal lines from smoothing; surface: inside and outside smoothed with slip, finely grained, colour outside and inside reddish brown (2.5YR 5/3), black at the rim – perhaps due to secondary burning; fabric: red (2.5YR 5/6), structure splintery, tempered with stone grit, grain – coarse 2, evenly distributed, medium amounts; hardness 5; fired under oxidizing conditions; extant height 2.4 cm, rim diameter 14 cm, opening diameter 13 cm. Inv. no. MOR-13/F2009Spring/2 (Fig. 19,2). 3. Rim sherd, unglazed ceramic, earthenware; rim slanting outwards, edge of rim and inner surface flaked off; traces of production: outside fine horizontal lines from smoothing; surface: outside coarsely grained, temper visible on the surface, smoothed with slip but mostly weathered, colour grey (10YR 6/1); fabric: structure splintery, colour grey (10YR 5/1), tempered with stone grit and sand, medium grained, evenly distributed, large amounts; hardness 4; fired under reducing conditions; extant height 2.3 cm, rim diameter c. 24 cm, extant thickness 1.1 cm. Trench 2, section 8–10 m, removal 2, collected finds. Inv. no. MOR-13/F2010Fall/30 (Fig. 19,3). 4. Rim sherd, unglazed ceramic, earthenware; rounded rim, horizontally flanged outwards; decoration: on upper side of rim single rilling; traces of production: inside and outside fine horizontal lines from smoothing; surface: outside and inside smoothed with slip, partly weathered, structure: smooth to chalky, colour outside and inside very dark grey (10YR 3/1); fabric: structure splintery, colour grey to very dark grey (10YR 6–3/1), tempered with quartz, medium grained, evenly distributed, medium amounts; hardness 2; fired under reducing conditions; extant height 1.9 cm, rim diameter 18 cm, opening diameter 12 cm, thickness 1 cm. Inv. no. MOR-13/F2010Fall/24. Trench 2, section 8–10 m, layers 7–9, removal 2, collected finds (Fig. 19,4). 5. Rim sherd, unglazed ceramic, earthenware; rounded rim, slightly slanting outwards; decoration: inside 1 cm below the rim two narrow rillings; surface: outside flaked off, inside coarsely grained, temper visible on the surface, colour light grey (2.5Y 7/2); fabric: structure splintery, colour grey (2.5Y 6/1), tempered with stone grit, grain – coarse 1, evenly distributed, large amounts; hardness 3; fired under reducing conditions; extant height 2.8 cm, rim diameter 22 cm, opening diameter 21 cm, width 4.4 cm, extant thickness 1 cm. Inv. no. MOR-13/F2010Fall/8. Trench 2, section 10–12 m, removal 2 (Fig. 19,5). 6. Body sherd with remains of attached handle, unglazed ceramic, earthenware, hand-made, freely formed; Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM 364 Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun surface: structure finely grained to chalky, outside colour dark grey (10YR 4/1), coated with white substance inside and partly over broken edges; fabric: colour brown (10YR 5/3), tempered with stone grit and sand, partly visible on the surface, grain – coarse 1, evenly distributed, large amounts; hardness 2; fired under reducing conditions; extant height 5.4 cm, diameter of knob attachment 3.1 cm. Inv. no. MOR-13/F2009Spring/2 (Fig. 19,6). 7. Handle fragment, unglazed ceramic, earthenware; arched, semi-circular in section; traces of production: on the inner side coarsely dispersed slip; surface: finely grained on the outer side, inner side rather smooth, colour outside light yellowish brown (10YR 6/4), inside grey (2.5Y 6/1); fabric: colour light grey (2.5Y 7/2), structure splintery and coarsely porous, tempered with stone grit, grain – coarse 2, unevenly distributed particles in small amounts; hardness 5; fired under reducing conditions; extant height 5.3 cm, width 2.5–2.7 cm, thickness 1.5–1.6 cm. Trench 1, collected finds. Inv. no. MOR-13/F2010Fall/1 (Fig. 19,7). 8. Decorated body sherd, unglazed ceramic; fabric: no temper discernible, medium grey; surface: inside smoothed with slip, horizontal traces of smoothing, outside very well smoothed with slip; decoration: concentric lozenge stamps; firing: medium. Inv. no. MOR-13/ F2008/1–2 (Fig. 16,8). 9. Decorated body sherd; unglazed ceramic; fabric: tempered with small amounts of fine stone grit, greybrown; surface: inside very poorly smoothed with slip (uneven), outside very well smoothed with slip; decoration: concentric lozenge stamps. Inv. no. MOR-13/ F2008/1–3 (Fig. 16,9). 10. Decorated body sherd, unglazed ceramic; fabric: tempered with small amounts of medium-coarse stone grit, inside grey-brown, outside medium grey; surface: inside moderately well smoothed without slip, outside well smoothed with slip; decoration: concentric lozenge stamps; firing: poor to medium. Inv. no. MOR-13/F2008/1–4 (Fig. 17,10). 11. Decorated body sherd, unglazed ceramic; fabric: temper not discernible, red-brown; surface: outside well smoothed with slip, outside flaked off; decoration: concentric lozenge stamps; firing: medium. Inv. no. MOR-13/ F2008/1–5 (Fig. 16,11). 12. Decorated body sherd, unglazed ceramic, fabric: tempered with small amounts of fine stone grit, greybrown (dark), slightly porous; surface: inside well smoothed with slip, vertical traces of smoothing, outside moderately well smoothed with slip; decoration: concentric lozenge stamps; firing: medium. Inv. no. MOR-13/ F2008/1–6 (Fig. 16,12). 13. Decorated body sherd, unglazed ceramic; fabric: tempered with very small amounts of fine stone grit, medium grey; surface: inside and outside well smoothed with slip; decoration: arched stamps; firing: medium. Inv. no. MOR-13/F2008/1–7 (Fig. 17,13). 14. Decorated body sherd, unglazed ceramic; fabric: tempered with small amounts of fine stone grit, medium grey, slightly porous; surface: inside and outside well smoothed with slip; decoration: small lozenge pattern, horizontal scratched lines; firing: medium. Inv. no. MOR-13/F2008/1–8 (Fig. 16,14). 15. Decorated body sherd, unglazed ceramic; fabric: tempered with small amounts of fine stone grit, red-brown, slightly porous; surface: inside well smoothed, outside well smoothed with slip; decoration: concentric lozenge stamps; firing: medium. Inv. no. MOR-13/F2008/1–9 (Fig. 16,15). 16. Decorated body sherd, unglazed ceramic; fabric: tempered with small amounts of fine stone grit, inside redbrown, outside grey-brown; surface: inside and outside well smoothed with slip; decoration: angular stamped pattern; firing: medium. Inv. no. MOR-13/F2008/1–10 (Fig. 16,16). 17. Decorated body sherd, unglazed ceramic; fabric: tempered with small amounts of medium stone grit, ochre-red; surface: well smoothed with slip; decoration: small lozenge stamps; firing: medium. Inv. no. MOR-13/ F2008/1–11 (Fig. 17,17). 18. Decorated body sherd, unglazed ceramic; fabric: no temper, medium grey; surface: inside flaked off, outside well smoothed; decoration: stamped slanting lines; firing: medium. Inv. no. MOR-13/F2008/1–12 (Fig. 17,18). 19. Decorated body sherd, unglazed ceramic; fabric: tempered with small amounts of fine stone grit, medium grey; surface: inside moderately well smoothed, outside well smoothed with slip, decoration: small lozenge stamps; firing: medium to moderately good. Inv. no. MOR-13/F2008/1–13 (Fig. 17,19). 20. Decorated body sherd, unglazed ceramic; fabric: tempered with small amounts of fine stone grit, core greyred, inside and outside ochre-grey; surface: well smoothed with slip; decoration: small lozenge stamps or angular indentations. Inv. no. MOR-13/F2008/1–14 (Fig. 17,20). 21. Decorated body sherd, unglazed ceramic; fabric: tempered with small amounts of fine stone grit, brick-red; surface: inside flaked off, outside very well smoothed with slip; decoration: horizontal scratched line; firing: medium. Inv. no. MOR-13/F2008/1–15 (Fig. 18,21). 22. Decorated body sherd, unglazed ceramic; fabric: tempered with medium amounts of fine and medium coarse stone grit, light ochre-grey; surface: inside and Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun outside very well smoothed (almost burnished); decoration: arched stamps; firing: medium. Inv. no. MOR-13/ F2008/1–16 (Fig. 17,22). 23. Decorated body sherd, unglazed ceramic, earthenware, hand-made; decoration: outside slanting scratched line (width 0.2 cm); traces of working: outside fine horizontal lines from smoothing; surface: outside smoothed with slip, structure inside and outside finely grained to chalky, temper visible on the outside, colour outside light yellowish brown (10YR 6/4), inside dark grey (10YR 4/1); fabric: structure splintery and porous, colour brown (10YR 5/3), tempered with quartz, medium grained with some very coarse particles, evenly distributed, medium amounts; hardness 4; fired under reducing conditions; extant height 4.5 cm, width 3.6 cm, thickness 1 cm. Inv. no. MOR-13/F2009Spring/2 (Fig. 18,23). 24. Decorated body sherd, unglazed ceramic, earthenware, hand-made; decoration: outside horizontal scratched line (width 0.15 cm); traces of production: inside and outside fine horizontal lines of smoothing, inside horizontally applied cordon; surface: structure smooth to finely grained, colour outside varying from light grey to reddish yellow (5YR 7/1–6/8), inside reddish yellow (5YR 6/6); fabric: structure splintery, coarsely porous, colour edges up to 0.3 cm like outer colours, middle part grey (5YR 5/1), tempered with stone grit, grain – coarse 1, evenly distributed, large amounts; hardness 3; fired partly under oxidizing conditions; extant height 3.2 cm, width 3.7 cm, thickness 0.6–1.1 cm. Inv. no. MOR-13/F2009Spring/2 (Fig. 18,24). 25. Decorated body sherd, unglazed ceramic, earthenware, hand-made; decoration: horizontal scratched line (width 0.1 cm); traces of production: inside and outside fine horizontal lines of smoothing; surface: outside and inside smoothed with slip, structure smooth, partly coated with white substance, colour outside reddish grey (5YR 5/2), inside reddish brown (5YR 5/3); fabric: structure splintery, colour reddish grey 0.2 cm from the outside, rest dark grey (5YR 4/1), tempered with quartz, grain – coarse 1, evenly distributed, large amounts; hardness 4; fired under reducing conditions; extant height 4 cm, width 2.6 cm, thickness 0.8–1.2 cm. Inv. no. MOR-13/F2009Spring/2 (Fig. 18,25). 26. Decorated body sherd, unglazed ceramic, earthenware, hand-made; decoration: outside curved impressed line (width 0.4 cm); surface: temper visible on the surface, structure smooth to finely grained, colour outside reddish yellow (5YR 6/6), inside light brown (7.5YR 6/4); fabric: structure splintery, colour changing from light brown (7.5YR 6/4) via brown (7.5YR 5/2) to very dark grey (7.5YR 3/1), tempered with quartz, grain – coarse 1, evenly 365 distributed, very large amounts; hardness 2; fired partly under oxidizing conditions; extant height 3.1 cm, width 3.8 cm, thickness 1.2 cm. Inv. no. MOR-13/F2009Spring/2 (Fig. 18,26). 27. Decorated body sherd, unglazed ceramic, earthenware; decoration: outside concentric lozenge stamps; surface: temper visible on the surface, outside partly flaked off, colour outside dark grey (5YR 4/1), inside light reddish brown (5YR 6/4); fabric: structure slightly splintery, colour light reddish brown (5YR 6/4), tempered with stone grit and grog, grain – coarse 2, evenly distributed, large amounts; hardness 4; fired under oxidizing conditions?; extant height 4.2 cm, width 3.9 cm, thickness 1 cm. Inv. no. MOR-13/F2009Spring/2 (Fig. 16,27). 28. Decorated body sherd, unglazed ceramic, earthenware; decoration: outside arched stamps (individual arches 0.25 cm apart); surface: structure smooth, partly coated with a white substance, colour outside light grey (10YR 7/2), inside grey (10YR 6/1); fabric: structure splintery, colour like surface, tempered with stone grit, medium grained, evenly distributed, medium amounts; hardness 5; fired under reducing conditions; extant height 2.5 cm, width 3.5 cm, thickness 0.7–0.8 cm. Inv. no. MOR-13/ F2009Spring/2 (Fig. 16,28). 29. Decorated body sherd, unglazed ceramic, earthenware; decoration: outside lozenge and angular indentations in no apparent pattern; surface: strongly weathered, outside smoothed with slip, inside structure finely grained, temper visible on the inner surface, colour outside very pale brown (10YR 7/4), inside grey to reddish yellow (5YR 6/1–6); fabric: structure splintery, colour red (2.5YR 5/8) with dark grey lumps (GLEY1 4/N), tempered with stone grit, medium grained, evenly distributed, large amounts; hardness 3; fired partly under oxidizing conditions; extant height 2.7 cm, width 4.7 cm, thickness 0.7–0.9 cm. Inv. no. MOR-13/F2009Spring/2 (Fig. 17,29). 30. Decorated body sherd, unglazed ceramic, earthenware; decoration: outside concentric lozenge stamps; surface: outside smoothed with slip, inside flaked off, colour outside brown (10YR 5/3); fabric: structure slightly splintery, colour reddish brown (5YR 5/4), tempered with stone grit, grain – coarse 1, evenly distributed, large amounts; hardness 3; fired under oxidizing conditions?; extant height 2.6 cm, width 3.2 cm, extant thickness 0.7 cm. Inv. no. MOR-13/F2009Spring/2 (Fig. 16,30). 31. Decorated body sherd, unglazed ceramic, earthenware; decoration: pattern of concentric lozenge stamps above break (individual height c. 1.7 cm, max. width c. 1 cm); surface: structure smooth to chalky, outside colour grey (10YR 6/1), inside coated with a white substance, original colour invisible; fabric: structure splintery, colour Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM 366 Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun light grey to grey (10YR 7–6/1), tempered with stone grit, grain – coarse 1, evenly distributed, medium amounts; hardness 3; fired under reducing conditions; extant height 4.8 cm, width 3.5 cm, thickness 1–1.2 cm. Inv. no. MOR-13/ F2009Fall/1 (Fig. 16,31). 32. Decorated body sherd, unglazed ceramic, earthenware; decoration: outside vertical grooves (width up to 0.5 cm); surface: structure smooth, outside colour light grey (2.5Y 7/2), inside nearly completely covered with white substance, colour reddish brown (5YR 5/3); fabric: structure splintery, colour pinkish grey (5YR 6/2), tempered with stone grit and grog, grain – coarse 1, evenly distributed, medium amounts; hardness 3; fired under reducing conditions; extant height 2.7 cm, width 4.1 cm, thickness 1 cm. Inv. no. MOR-13/F2009Fall/1 (Fig. 18,32). 33. Decorated body sherd, unglazed ceramic, earthenware; decoration: outside two crossing slightly curved grooves (width 0.2–0.3 cm); traces of production: fine lines from smoothing; surface: outside and inside smoothed with slip, temper visible on the surface, colour outside grey (5YR 5/1), inside grey (5YR 6/1); fabric: structure splintery, colour edges like outer sides, core light reddish brown (5YR 6/4), tempered with quartz and stone grit, grain – coarse 2, evenly distributed, medium amounts; hardness 4; fired under oxidizing conditions?; orientation unclear, 2.1 × 1.8 cm, thickness 0.9 cm. Inv. no. MOR-13/ F2010Spring/3 (Fig. 18,33). 34. Decorated body sherd, unglazed ceramic, earthenware; decoration: outside three horizontal scratched lines, two only 0.5 cm apart, third 1.8 cm apart, on the two lines concentric lozenge stamps; traces of production: outside fine lines from smoothing with slip; surface: outside smoothed with slip, colour outside dark grey (7.5YR 4/1), outside temper visible on the surface, colour grey (7.5YR 5/1); fabric: structure splintery, colour grey (7.5YR 4/1), tempered with stone grit (white – 10YR 9.5/1), grain – coarse 1, evenly distributed, very large amounts; hardness 2; fired under oxidizing conditions?; extant height 4.8 cm, width 3.7 cm, thickness 1 cm. Trench 2, section 0–2 m, collected finds. Inv. no. MOR-13/F2010Fall/12 (Fig. 17,34). 35. Decorated body sherd, unglazed ceramic, earthenware; decoration: outside one horizontal scratched line (width 0.2 cm); surface: temper visible on the surface, outside moderately well smoothed without slip, colour grey (7.5YR 5/1), inside smoothed with slip, colour grey (7.5YR 6/1); fabric: structure splintery, colour grey (7.5YR 5/1), tempered with stone grit (white – 10YR 9.5/1); grain – coarse 1, evenly distributed, very large amounts; hardness 2; fired under oxidizing conditions?; extant height 3.6 cm, width 4.8 cm, thickness 0.8-1 cm. Trench 2, section 0–2 m, collected finds. Inv. no. MOR-13/F2010Fall/12 (Fig. 18:35). 36. Decorated body sherd, unglazed ceramic, earthenware; decoration: horizontal grooves (width 0.2 cm); surface: structure smooth, outside colour dark grey (5YR 4/1), inside and all edges coated with white substance, colour and fabric, therefore not determined; hardness 3; extant height 4.1 cm, width 2.4 cm, thickness 0.8 cm. Trench 2, section 4–6 m, removal 1. Inv. no. MOR-13/ F2010Fall/6 (Fig. 18,36). 37. Decorated body sherd, unglazed ceramic, earthenware; decoration: concentric lozenge stamps and arched stamps, bordered by horizontal incised line (width 0.15 cm), no stamp completely extant; surface: structure smooth, colour outside and inside reddish brown (5YR 5/4); fabric: structure splintery, colour yellowish red (5YR 5/8), tempered with sand, fine grained, evenly distributed, medium amounts; hardness 3; fired under oxidizing conditions?; extant height 3 cm, width 2.7 cm, thickness 0.8 cm. Trench 2, section 6–8 m, layers 7–9, collected finds. Inv. no. MOR-13/F2010Fall/22 (Fig. 17,37). 38. Decorated body sherd, unglazed ceramic, earthenware; decoration: outside concentric lozenge stamps, strongly weathered; surface: structure chalky, outside strongly weathered, colour outside and inside light red (2.5YR 6/8); fabric: structure splintery, colour red (2.5YR 5/8), tempered with quartz and sand, medium grained, evenly distributed, large amounts; hardness 3; fired under oxidizing conditions; extant height 2.4 cm, width 3.2 cm, thickness 0.8–0.9 cm. Trench 2, section 6–8 m, layers 7–9, collected finds. Inv. no. MOR-13/F2010Fall/22 (Fig. 16,38). 39. Decorated body sherd, unglazed ceramic, earthenware; decoration: crossing horizontal and slightly slanting grooves (width up to 0.5 cm, depth 0.2 cm), edges of displaced fabric; traces of production: outside fine horizontal lines from smoothing; surface: outside smoothed with slip, structure chalky, colour outside grey (2.5Y 5/1), inside dark grey (2.5Y 4/1); fabric: structure splintery, colour grey (2.5Y 6/1), tempered with stone grit, grain – coarse 2, evenly distributed, medium amounts; hardness 3; fired under reducing conditions; extant height 6.7 cm, width 7.3 cm, thickness 0.8–1.3 cm. Trench 2, section 6–8 m, layers 7–9, removal 2, collected finds. Inv. no. MOR-13/F2010Fall/28 (Fig. 18,39). 40. Decorated body sherd, unglazed ceramic, earthenware; decoration: outside lozenge stamps, barely visible because of weathering; surface: outside and inside smoothed with slip, structure smooth to chalky, colour outside dark grey (2.5Y 4/1), inside light brownish grey (2.5Y 6/2); fabric: structure splintery, colour reddish yellow, tempered with stone grit, medium grained, evenly distributed, medium amounts; hardness 2; fired under oxidizing conditions?; extant height 2.2 cm, width 3.6 cm, Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun thickness 1.2 cm. Trench 2, section 6–8 m, layers 7–9, removal 2, collected finds. Inv. no. MOR-13/F2010Fall/28 (Fig. 16,40). 41. Decorated body sherd, unglazed ceramic, earthenware; decoration: outside incised concentric arches, at least two rows but no single motif completely extant; surface: smooth to chalky, outside smoothed with slip but weathered, colour outside light brownish grey (2.5Y 6/2), inside light grey (2.5Y 7/2); fabric: structure slightly splintery, colour light grey (2.5Y 7/2), tempered with stone grit, grain – coarse 1, evenly distributed, medium amounts; hardness 2; fired under reducing conditions; extant height 3.5 cm, width 3.1 cm, thickness 0.9–1 cm. Trench 2, section 6–8 m, layers 7–9, removal 2, collected finds. Inv. no. MOR-13/F2010Fall/33 (Fig. 17,41). 42. Decorated body sherd, unglazed ceramic, earthenware. Decoration: horizontal scratched line (width 1.5 mm, depth 0.5 mm); traces of production: fine horizontal lines caused by smoothing of surface; surface: structure smooth to finely grained, smoothed with slip inside and outside, colour outside very dark grey (GLEY1 3/N), inside very dark grey (7.5YR 3/1); fabric: colour dark grey (7.5YR 4/1) to brown (7.5YR 5/2), structure splintery, tempered with quartz, evenly distributed, grain – coarse 1, large amounts; hardness 2; fired under reducing conditions; 2.3 cm × 2.5 cm, thickness 0.8–1 cm. Trench 2, section 8–10 m, layers 7–9, removal 2, collected finds. Inv. no. MOR-13/F2010Fall/25 (Fig. 18,42). 43. Decorated body sherd, unglazed ceramic, earthenware; decoration: outside angular stamped pattern; surface: outside colour dark grey (7.5YR 4/1), inside surface completely flaked off; fabric: structure slightly porous and splintery, colour light red (10R 6/6), tempered with stone grit and grog, grain – coarse 1, evenly distributed, large amounts; hardness 2; fired under oxidizing conditions; 2.8 × 2.6 cm, extant thickness 0.7 cm. Trench 2, section 10–12 m, collected finds. Inv. no. MOR-13/F2010Fall/19 (Fig. 17,43). 44. Decorated body sherd, unglazed ceramic, earthenware; decoration: concentric lozenge stamps (strongly eroded); surface: temper visible on the surface, inside and outside well smoothed, colour outside dark grey (7.5YR 4/1), inside weak red (10R 5/2); fabric: structure splintery, colour pale red (10R 6/4), tempered with stone grit, grain – coarse 1, evenly distributed, very large amounts; hardness 2; fired under oxidizing conditions; 3.6 × 4.4 cm, thickness 0.8 cm. Trench 2, section 10–12 m, collected finds. Inv. no. MOR-13/F2010Fall/19 (Fig. 16,44). 45. Decorated body sherd, unglazed ceramic, earthenware; decoration: outside two horizontal incised lines (width 0.15 cm) 2.5 cm apart, space in between and lower 367 line intersected by slightly slanting short grooves (length about 1.5 cm, width up to 0.2 cm; surface: structure finely grained, outside lower part secondarily blackened, colour pale brown (10YR 6/3), inside dark grey/dark greyish brown (10YR 4/1–2); fabric: structure splintery, colour grey (10YR 5/1), tempered with stone grit, grain – coarse 2, evenly distributed, large amounts; hardness 3; fired under reducing conditions; extant height 5.2 cm, width 6.9 cm, thickness 0.9 cm. Trench 2, section 10–12 m, removal 2. Inv. no. MOR-13/F2010Fall/9 (Fig. 18,45). 46. Decorated body sherd, unglazed ceramic, earthenware; decoration: outside indented bow (width 0.2 cm); surface: structure finely grained, temper visible on the surface, colour outside dark grey (5YR 4/1), inside yellowish red (5YR 5/6); fabric: structure smooth, colour yellowish red (5YR 5/6), tempered with stone grit and quartz, grain – coarse 1, evenly distributed, large amounts; hardness 2; fired under oxidizing conditions; orientation unclear, 3.5 × 2.3 cm, thickness 1 cm. Trench 2, section 10–12 m, removal 2. Inv. no. MOR-13/F2010Fall/9 (Fig. 18,46). 47. 41 body sherds, undecorated, unglazed ceramic. Inv. no. MOR-13/F2008/1. 48. Nine body sherds, undecorated, unglazed ceramic, earthenware, none with traces of wheel-throwing. – 1) surface: structure smooth, temper visible on the surface, outside slightly shiny, outside colour very dark grey (2.5Y 3/1), inside dark grey (2.5Y 4/1); fabric: colour dark grey to very dark grey (2.5Y 3–4/1), structure splintery, tempered with quartz, grain – coarse 1, evenly distributed, very large amounts; hardness 4; fired under reducing conditions; 3.2 cm × 2.2 cm, thickness 0.7 cm. – 2) surface: structure smooth, outside smoothed with slip, slightly shiny, outside and inside colour very dark grey (GLEY1 3/N); fabric: structure splintery and coarsely porous, colour very dark grey (GLEY1 3/N), tempered with stone grit, quartz and grog, medium grained, evenly distributed, large amounts; hardness 4; fired under reducing conditions; 1.9 × 2.3 cm, thickness 0.5 cm. – 3) surface: structure smooth, temper visible on the surface, outside smoothed with slip, slightly shiny, colour reddish brown (5YR 5/4), inside yellowish red (5YR 5/6); fabric: colour inner half yellowish red (5YR 5/6), outer half reddish grey (5YR 5/2), structure splintery, tempered with stone grit and sand, medium grained, evenly distributed, large amounts; hardness 2; firing partly oxidizing; 2.4 × 3 cm, thickness 1.3 cm. – 4) traces of working: outside horizontal traces of smoothing, hand-made by coiling; surface: outside smoothed with slip, structure smooth, temper visible on the surface, colour outside light brownish grey (10YR 6/2), inside light red (2.5YR 6/8); fabric: structure splintery, colour 2 mm from the outside light brownish grey (10YR Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM 368 Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun 6/2), rest light red (2.5YR 6/8), tempered with quartz and stone grit, medium grained with some very coarse particles, evenly distributed, large amounts; hardness 2; fired partly under oxidizing conditions; 2.3 × 3.1 cm, thickness 0.6–0.9 cm. – 5) Surface: structure smooth, colour outside and inside pinkish grey (7.5YR 6/2); fabric: structure splintery, colour grey (7.5YR 6/1), tempered with quartz, grain – coarse 1, evenly distributed, medium amounts; hardness 3; fired under reducing conditions; 4.1 × 4.1 cm, thickness 0.8 cm. – 6) surface: structure finely grained, temper visible on the surface, colour outside and inside grey (7.5YR 6/1); fabric: structure splintery, colour brown (7.5YR 4/2), tempered with stone grit, medium grained, evenly distributed, large amounts; hardness 4; fired under reducing conditions; 3.8 cm × 2.3 cm, thickness 0.7–0.8 cm. – 7) Surface: structure chalky to smooth, colour outside and inside grey (10YR 6/1); fabric: structure slightly splintery, colour yellowish brown (10YR 5/4), tempered with stone grit, evenly distributed, medium grained, medium amounts; hardness 3; fired under reducing conditions; 2.5 × 2.2 cm, thickness 0.8 cm. – 8) Surface: outside smoothed with slip, structure smooth, colour light grey (10YR 7/2), inside flaked off; fabric: structure splintery, colour very dark grey (10YR 3/1), tempered with stone grit, grain – coarse 1, evenly distributed, medium amounts; hardness 6; fired under reducing conditions; 2.1 × 2.9 cm, extant thickness 0.9 cm. – 9) Surface: inside and outside smoothed with slip, structure smooth, colour outside light brownish grey (10YR 6/2), inside grey (10YR 6/1); fabric: structure splintery, colour grey (10YR 5/1), tempered with quartz and stone grit, grain – coarse 1, evenly distributed, large amounts; hardness 4; fired under reducing conditions; 1.8 × 2.2 cm, thickness 1 cm. Inv. no. MOR-13/F2009Spring/2. 49. Four body sherds, undecorated, unglazed ceramic, earthenware, none shows traces of wheel-throwing. – 1) Traces of production: outside and inside fine horizontal lines from smoothing; surface: partly coated with white substance, outside and inside smoothed with slip, structure chalky, colour outside and inside grey (10YR 6/1); fabric: structure splintery, colour grey (10YR 7/1), tempered with stone grit, grain – coarse 1, evenly distributed, small amounts; hardness 3; fired under reducing conditions; extant height 4 cm, width 5.8 cm, thickness 0.9 cm. – 2) Surface: outside strongly weathered, inside structure chalky, colour outside grey (2.5Y 6/1), inside light brownish grey (2.5Y 6/2); fabric: structure slightly splintery, colour at the edges as outer sides, core dark grey (2.5Y 4/1), tempered with quartz, fine grained, evenly distributed, medium amounts; hardness 3; fired under reducing conditions; 3.8 × 3.2 cm, extant thickness 0.7 cm. – 3) Surface: outside smoothed with slip, weathered, struc- ture smooth to finely grained, inside flaked off, colour outside dark grey (10YR 4/1); fabric: structure splintery, colour reddish brown (2.5YR 5/4), tempered with quartz and stone grit, grain-coarse 1, evenly distributed, large amounts; hardness 4; fired under oxidizing conditions?; 3.4 × 3 cm, extant thickness 0.9 cm. – 4) Surface: structure outside chalky to finely grained, inside flaked off, colour outside pale yellow (2.5Y 7/3); fabric: structure splintery, colour reddish yellow (5YR 6/6), tempered with stone grit, grain – coarse 2, evenly distributed, large amounts; hardness 4; fired under oxidizing conditions?; 3.7 × 3.6 cm, extant thickness 1.2 cm. Inv. no. MOR-13/F2010Spring/3. 50. Body sherd, unglazed ceramic, earthenware; surface: inside and outside smoothed with slip, temper visible on the surface, colour inside and outside grey (7.5YR 5/1); fabric: structure splintery, colour grey (7.5YR 6/1), tempered with stone grit, grain – coarse 1, evenly distributed, very large amounts; hardness 4; fired under oxidizing conditions?; extant height 4.6 cm, width 7.4 cm, thickness 0.8–1.1 cm. Trench 2, section 0–2 m, collected finds. Inv. no. MOR-13/F2010Fall/13. 51. Body sherd, unglazed ceramic, earthenware; surface: nearly completely coated with white substance, structure outside finely grained, colour inside grey (10YR 5/1), inside flaked off; fabric: structure splintery, colour and fabric not determinable due to white coating; hardness 4; 6 × 5.5 cm; extant thickness 1.1 cm. Trench 2, section 6–8 m, layers 7–9, removal 2, collected finds. Inv. no. MOR-13/F2010Fall/34. 52. Ten body sherds, unglazed ceramic, earthenware, none shows traces of wheel-throwing. – 1) Surface: outside smoothed with slip, structure chalky, colour outside and inside dark grey (5YR 4/1); fabric: structure splintery, colour reddish brown (5YR 5/4), tempered with sand, fine grained, evenly distributed, large amounts; hardness 2; fired under oxidizing conditions?; 3.8 × 2.9 cm, thickness 0.8–1 cm. – 2) Traces of production: fine lines of smoothing: surface: outside flaked off, inside smoothed with slip, colour very dark grey (GLEY1 3/N); fabric: structure splintery, colour very dark grey (GLEY1 3/N), tempered with stone grit, grain – coarse 2, evenly distributed, small amounts; hardness 3; fired under reducing conditions; 3 × 2 cm, extant thickness 0.7 cm. – 3) Eight fragments of the same ware, surfaces mostly flaked off, surface: structure outside and inside smooth, colour outside and inside grey (GLEY1 6/N); fabric: structure splintery, colour light grey (GLEY1 7/N), tempered with stone grit, grain – coarse 1, evenly distributed, small amounts; hardness 2; fired under reducing conditions; 1.6 × 0.9 × 0.5 cm to 2.7 × 2 × 1.2 cm. Trench 2, section 8–10 m, layers 7–9, removal 2, collected finds. Inv. no. MOR-13/F2010Fall/26. Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun 53. Three body sherds of the same ware, unglazed ceramic, earthenware; surface: one surface of each sherd is completely flaked off, fragments too small to determine whether outside or inside, extant surface smooth, temper visible on the surface, colour black (5YR 2.5/1); fabric: structure splintery, colour dark reddish grey (5YR 4/2), tempered with stone grit and quartz, medium grained with some very coarse particles, evenly distributed, large amounts; hardness 3; fired under reducing conditions; 2.4 × 2 × 0.9 cm/1.8 × 1.7 × 0.8 cm/1.8 × 1 × 0.6 cm. Trench 2, section 10–12 m, removal 2. Inv. no. MOR-13/ F2010Fall/10. 54. Two body sherds, glazed ceramic. – 1) stoneware, wheel-thrown; traces of production: inside and outside turning marks; surface: structure smooth, outside glazed, colour white (2.5Y 8/1), slightly shiny, flaked off in spots; inside colour light grey (2.5Y 7/2); fabric: colour light grey (2.5Y 7/2), structure smooth, tempered with black sand or stone grit, medium grained, evenly distributed, very large amounts; hardness 8; fired under reducing conditions; 3.5 cm × 2.6 cm; thickness 0.5–0.6 cm. – 2) earthenware, wheel-thrown; traces of production: outside turning marks, inside vertical traces of smoothing; surface: outside engobed, dim, weathered, smooth, colour black (5YR 2.5/1), inside smoothed with slip, colour red (2.5YR 5/6); fabric: colour red (2.5YR 5/6), structure splintery, tempered with quartz, grain – coarse 1, evenly distributed, very large amounts; hardness 2; fired under oxidizing conditions; 3.6 cm × 5.6 cm, thickness 0.7–0.8 cm. Inv. no. MOR-13/F2009Spring/1. 55. Body sherd, glazed ceramic, stoneware or porcelain; surface: outside glazed, metallic shine, colour reddish brown (5YR 4/4), inside structure uneven, thinly coated with semi-lucent glaze, colour yellowish brown (10YR 5/6); fabric: structure layered to smooth, colour very pale brown (10YR 8/2), tempered with particles of undetermined material, fine grained, evenly distributed, large amounts; hardness 9; fired under oxidizing conditions?; 1.6 × 1.5 cm, thickness 0.4 cm. Inv. no. MOR-13/ F2010Spring/1. 56. Iron plate, drilled through, broken at the edges. Inv. no. MOR-13/F2008/3 (Fig. 20,56). 57. Iron nail, broken at the extremities. Inv. no. MOR-13/F2008/3 (Fig. 20,57). 58. Iron ball, slightly compressed, perforated in the centre (round hole, diameter 1.2 cm); height 4.8 cm, diameter 5.8 cm. Trench 2 (x: 2.7 m from A, y: 0.2 m from AB, z: –0.2 m). Inv. no. MOR-13/F2010Fall/17 (Fig. 20,58). 59. Toggle, bone, broken at one end, surface weathered so that inner bone structure is partly visible; now H-shaped, long sides convex, respectively concave, inner 369 part for strap rounded (extant length c. 2 cm, width 0.5 cm); surface smoothed; extant length 5.2 cm, width 0.5–1.6 cm, thickness 0.5 cm. Trench 2, section 6–8 m, layers 7–9, collected finds. Inv. no. MOR-13/F2010Fall/21 (Fig. 20,59). 60. Worked bone or horn, dense structure; three sides broken, slightly curved, one end cut at a slant and smoothed, on the surface inside and outside traces of teeth marks or other scratches; length 9.1 cm, width 2.3 cm, thickness 0.5–0.8 cm. Trench 2, section 8–10 m, removal 2, collected finds. Inv. no. MOR-13/F2010Fall/31 (Fig. 20,60). 61. Animal bone, angular. Inv. no. MOR-13/F2008/2. 62. Two fragments of bone, probably animal. Inv. no. MOR-13/F2009Spring/4. 63. 15 bone fragments, probably animal. Trench 2, removal 1, collected finds. Inv. no. MOR-13/F2010Fall/2. 64. 42 bone fragments, probably animal. Trench 2, section 0–2 m, collected finds. Inv. no. MOR-13/ F2010Fall/14. 65. Eight bone fragments. Trench 2, section 2–4 m, collected finds. Inv. no. MOR-13/F2010Fall/15. 66. 16 bone fragments, probably animal. Trench 2, section 2–4 m, removal 1, collected finds. Inv. no. MOR-13/ F2010Fall/3. 67. Eight bone fragments, probably animal. Trench 2, section 4–6 m, collected finds. Inv. no. MOR-13/ F2010Fall/16. 68. 17 bone fragments, probably animal. Trench 2, section 4–6 m, removal 1, collected finds. Inv. no. MOR-13/ F2010Fall/5. 69. 38 bone fragments, probably animal. Trench 2, section 6–8 m, removal 2, collected finds. Inv. no. MOR-13/ F2010Fall/36. 70. 67 bone fragments, probably animal. Trench 2, section 6–8 m, layers 7–9, collected finds. Inv. no. MOR-13/ F2010Fall/23. 71. 97 bone fragments, probably animal. Trench 2, section 6–8 m, layers 7–9, removal 2, collected finds. Inv. no. MOR-13/F2010Fall/35. 72. 102 bone fragments, probably animal. Trench 2, section 6–8 m, layers 7–9, removal 2, collected finds. Inv. no. MOR-13/F2010Fall/29. 73. Eleven bone fragments, probably animal. Trench 2, section 8–10 m, removal 1, collected finds. Inv. no. MOR-13/F2010Fall/7. 74. 26 bone fragments, probably animal. Trench 2, section 8–10 m, removal 2, collected finds. Inv. no. MOR-13/F2010Fall/32. 75. 67 bone fragments, probably animal. Trench 2, section 8–10 m, layers 7–9, removal 2, collected finds. Inv. no. MOR-13/F2010Fall/27. Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM 370 Jan Bemmann et al., Biomarkers in archaeology – Land use around the Uyghur capital Karabalgasun 76. 19 bone fragments, probably animal. Trench 2, section 10–12 m, collected finds. Inv. no. MOR-13/ F2010Fall/20. 77. Two bone fragments, probably animal. Trench 2, section 10–12 m, collected finds. Inv. no. MOR-13/ F2010Fall/18. 78. 19 bone fragments, mostly rib fragments, two vertebrae, one tooth, probably animal. Trench 2, section 10-12 m, removal 1. Inv. no. MOR-13/F2010Fall/37. 79. Two bone fragments, probably animal. Trench 2, section 10–12 m, removal 2. Inv. no. MOR-13/F2010Fall/11. 80. 33 fragments of roof tiles. Inv. no. MOR-13/ F2008/6. 81. Piece of roof tile, burnt brick, fragment of round end tile with round, flatly raised knobs (diameter 1 cm, height 0.3 cm); surface: unglazed, structure coarsely grained, colour outside very pale brown (10YR 8/2), inside flaked off; fabric: grey (10YR 6/1), structure coarsely porous, tempered with stone grit, medium grained, evenly distributed, large amounts; hardness 2; fired under reducing conditions; original diameter about 6 cm, 2.8 cm × 1.8 cm, extant thickness 0.9 cm. Inv. no. MOR-13/F2009 Spring/3 (Fig. 20,81). 82. Piece of roof tile. Inv. no. MOR-13/F2008/7. 83. Three pieces of slag. Inv. no. MOR-13/F2008/4. 84. Piece of slag; colour dark reddish brown (2.5YR 3/4) and reddish black (2.5YR 2.5/1); 3.4 × 3.2 × 2.2 cm, weight 30.6 g. Inv. no. MOR-13/F2010Spring/2. 85. Two pieces of charcoal, 1.2 cm × 1 cm × 0.4 cm/1.6 cm × 1.1 cm × 0.8 cm, weight 0.3 g. Trench 2, section 2–4 m, removal 1. Inv. no. MOR-13/F2010Fall/4. 86. Modern coin, Mongolian, minted 1927, 5 müngü. Inv. no. MOR-13/F2008/5. (S. R./H. P.) Authenticated | [email protected] author's copy Download Date | 7/27/15 8:11 PM
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