大内 幸弘

TEST REPORT
REPORT NO. JP/2014/050134
DATE:May 26,2014
PAGE: 1 OF 4
PANASONIC CORPORATION AUTOMOTIVE & INDUSTRIAL SYSTEMS COMPANY
111 ISHIZUKA KORIYAMA-SHI FUKUSHIMA JAPAN
THE FOLLOWING SAMPLE(S) WAS/WERE SUBMITTED AND IDENTIFIED BY/ON BEHALF OF THE CLIENT AS:
以下のサンプルは顧客により提供され、顧客に代わって確認を行いました:
SAMPLE DESCRIPTION
:
Copper foil F-001
CLIENT REF.NO
:
SAMPLE RECEIVED
:
2014/05/08
TESTING DATE
:
2014/05/08 TO 2014/05/26
TEST REQUESTED
分析項目
:
SELECTED TEST(S) AS REQUESTED BY CLIENT.
分析項目は顧客の要求によります。
TEST METHOD(S)
分析方法
:
WITH REFERENCE TO LATEST EDITION OF IEC62321 FOR RoHS 6 SUBSTANCES.
OTHER CHEMICALS WERE TESTED BY EACH APPROPRIATE METHOD.
RoHS6物質の分析は最新版のIEC62321を参照しました。
それ以外の化学物質についてはそれぞれに最適な方法で分析を行いました。
TEST RESULT(S)
分析結果
:
PLEASE REFER TO THE NEXT PAGE(S).
以下のページをご参照願います。
大内 幸弘
Yukihiro Ouchi / Quality Manager
SGS Japan Inc., Chemical Laboratory
TEST REPORT
REPORT NO. JP/2014/050134
DATE:May 26,2014
PAGE: 2 OF 4
PANASONIC CORPORATION AUTOMOTIVE & INDUSTRIAL SYSTEMS COMPANY
111 ISHIZUKA KORIYAMA-SHI FUKUSHIMA JAPAN
TEST RESULT(S)
UNIT
RESULT
METHOD
INST./PLACE
MDL
CADMIUM(Cd)
㎎/㎏
N.D.
IEC62321-5: 2013
ICP-OES
2
LEAD(Pb)
㎎/㎏
N.D.
IEC62321-5: 2013
ICP-OES
2
MERCURY(Hg)
㎎/㎏
N.D.
IEC62321-4: 2013
ICP-OES
2
IEC62321: 2008 ANNEX B
UV/VIS
0.01
GC/MS
5
5
5
5
5
5
5
5
5
5
GC/MS
5
5
5
5
5
5
5
5
5
5
ITEM(S)
CHROMIUM VI(Cr(VI))
μg/㎠
N.D.
Polybrominated biphenyls(PBBs)
Monobromobiphenyl
㎎/㎏
N.D.
Dibromobiphenyl
㎎/㎏
N.D.
Tribromobiphenyl
㎎/㎏
N.D.
Tetrabromobiphenyl
㎎/㎏
N.D.
Pentabromobiphenyl
㎎/㎏
N.D.
Hexabromobiphenyl
㎎/㎏
N.D.
Heptabromobiphenyl
㎎/㎏
N.D.
Octabromobiphenyl
㎎/㎏
N.D.
Nonabromobiphenyl
㎎/㎏
N.D.
Decabromobiphenyl
㎎/㎏
N.D.
Polybrominated diphenyl ethers(PBDEs)
Monobromodiphenyl ether
㎎/㎏
N.D.
Dibromodiphenyl ether
㎎/㎏
N.D.
Tribromodiphenyl ether
㎎/㎏
N.D.
Tetrabromodiphenyl ether
㎎/㎏
N.D.
Pentabromodiphenyl ether
㎎/㎏
N.D.
Hexabromodiphenyl ether
㎎/㎏
N.D.
Heptabromodiphenyl ether
㎎/㎏
N.D.
Octabromodiphenyl ether
㎎/㎏
N.D.
Nonabromodiphenyl ether
㎎/㎏
N.D.
Decabromodiphenyl ether
㎎/㎏
N.D.
NOTES: mg/kg = ppm, N.D. = Not Detected, INST. = INSTRUMENT, MDL =
IEC62321: 2008 ANNEX A
IEC62321: 2008 ANNEX A
Method Detection Limit
REMARK: Cr(VI) has been tested with regard to the surface area of 12㎠.
Reference: The MDL of Cr(VI) can be converted into 2 (ppm) with regard to the sample weight.
TEST REPORT
REPORT NO. JP/2014/050134
DATE:May 26,2014
PAGE: 3 OF 4
PANASONIC CORPORATION AUTOMOTIVE & INDUSTRIAL SYSTEMS COMPANY
111 ISHIZUKA KORIYAMA-SHI FUKUSHIMA JAPAN
分析フローチャート MEASUREMENT FLOW CHART
1)酸分解前処理において試料を完全分解しています。
The sample was dissolved/ decomposed totally by acid pre-conditioning method according to below flow chart.
2)Cd, Pb, Hg, Cr, Cr(VI)
分析担当者 Name of the person in charge of measurement: 野田 晴美 Harumi Noda
3)PBB/PBDE
分析担当者 Name of the person in charge of measurement: 野田 晴美 Harumi Noda
4)分析責任者 Name of the person responsible for measurement: 大谷 真由美 Mayumi Otani
カッティング・下準備 Cutting・Preparation
Cr(VI)
PBB/PBDE
秤量 Sample measurement
Cd, Pb, Cr
Hg
密閉系/ 開放系による酸分解
(HNO3, HCl, HF等)
Decomposition under closed/
open system (HNO3, HCl, HF,
etc.)
密閉系による酸/ 加熱分解
(HNO3, HCl, HF等)
Decomposition under closed
system (HNO3, HCl, HF, etc.)
ろ過 Filtration
溶液 Solution
秤量
Sample measurement
アルカリ/ 沸騰水による
抽出
Extraction by alkaline
solution/ boiling water
冷却・ろ過
Cooling・Filtration
秤量
Sample measurement
ソックスレー/ 有機
溶媒抽出
Soxhlet/ solvent
extraction
濃縮・希釈
Concentration・Dilution
残渣 Residue
アルカリ溶融 Alkali fusion
ICP-OES, ICP-MS, AAS
ジフェニルカルバジド
添加・pH調整
Add diphenylcarbazide・
pH adjustment
UV/Vis
GC/MS
TEST REPORT
REPORT NO. JP/2014/050134
PANASONIC CORPORATION AUTOMOTIVE & INDUSTRIAL SYSTEMS COMPANY
111 ISHIZUKA KORIYAMA-SHI FUKUSHIMA JAPAN
SAMPLE IMAGE
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DATE:May 26,2014
PAGE: 4 OF 4