GC Columns Application | SOLVENTS & CHEMICALS 溶媒・化学製品 カラムの選択 ホルムアルデヒド Formaldehyde on Rt®-U-BOND (PLOT) 相当品対応表 Peaks 1. Air 2. Carbon dioxide 3. Formaldehyde 4. Water 5. Methanol Column Sample Injection :Rt®-U-BOND, 30 m × 0.53 mm I.D., 20 µm(Cat.No. 1015-11160) :Formaldehyde(manual headspace) ガードカラムについて Inj. Vol.:10 µL split(split ratio 10:1) Liner:2 mm split Precision liner w/wool(Cat.No. 3015-90101) Inj. Temp.:200 ℃ Split Vent Flow Rate:40 mL/min Oven Oven Temp.:100 ℃(hold 1 min)to 150 ℃ at 25 ℃ /min(hold 3 min) Carrier Gas :He, constant pressure(7.7 psi, 53.1 kPa) Linear Velocity:39 cm/sec @ 100 ℃ Detector :TCD @ 200 ℃ Make-up Gas Type:He フューズドシリカカラム メタルカラム GC_CH1137 水中の低級アミン PLOT カラム Short Chain Amines in Water on Rtx®-Volatile Amine 225 2 200 スカイライナー Peaks 1. Methanol 2. Dimethylamine 3. Trimethylamine 4. Methylethylamine 5. Dimethylethylamine 6. Diethylamine 7. Methyldiethylamine 8. Triethylamine IS = Isopropylamine pA 175 Column 5 150 Sample Injection 125 アプリケーション Inj. Vol.:1.0 µL split(split ratio 15:1) Inj. Temp.:220 ℃ Split Vent Flow Rate:30 mL/min Oven Oven Temp.:40 ℃(hold 10 min)to 250 ℃ at 20 ℃ /min(hold 10 min) Carrier Gas :H2 , constant flow Flow Rate:2.0 mL/min Linear Velocity:35 cm/sec @ 40 ℃ Detector :FID @ 250 ℃ 100 IS 75 50 6 1 25 0 :Rtx®-Volatile Amine, 60 m × 0.32 mm I.D. (Cat.No. 1015-11123) :Short Chain amines Diluent:Water Conc.:200-1,000 ppm 0 146 Restek General Catalog 5 3 4 10 Time (min) 7 15 8 20 GC_GN1154 GC Columns Application | SOLVENTS & CHEMICALS 溶媒・化学製品 カラムの選択 第1級アミン Primary Amine on Rtx®-35 Amine 2,3 5 4 7 8 9 1 Column Sample Injection Diluent:Water Conc.:50 ppm on-column Inj. Vol.:1 µL split(split ratio 10:1) Liner:splitless taper(4 mm), base deactivated(Cat.No. 3015-90091) Inj. Temp.:250 ℃ Oven Temp.:35 ℃(hold 5 min) Carrier Gas :He, constant pressure Linear Velocity:35.7 cm/sec Detector :FID @ 300 ℃ 1.0 1.5 2.0 2.5 Time (min) 3.0 3.5 4.0 4.5 メタルカラム 0.5 フューズドシリカカラム Oven :Rtx®-35 Amine, 30 m × 0.53 mm I.D.,1.00 µm(Cat.No. 1015-10606) ガードカラムについて 6 相当品対応表 Peaks 1. Methylamine 2. Dimethylamine 3. Trimethylamine 4. Ethylamine 5. Isopropylamine 6. tert-Butylamine 7. n-Propylamine 8. Diethylamine 9. sec-Butylamine 5.0 GC_CH00578 有機溶剤 Injection Benzene 1,2-Dimethoxyethane Trichloroethylene 1,4-Dioxane Pyridine Dimethylformamide Methylcyclohexane Toluene 2-Hexanone Chlorobenzene Ethylbenzene m-Xylene p-Xylene o-Xylene :Rt®-Q-BOND, 30 m × 0.53 mm I.D., 20 µm (Cat.No. 1015-11152) Inj. Vol.:1.0 µL split Liner:4 mm splitless taper (Cat.No. 3015-90090) Inj. Temp.:200 ℃ Split Vent Flow Rate:100 mL/min Oven Oven Temp.:120 ℃ to 240 ℃ at 5 ℃ /min(hold 5.0 min) Carrier Gas :H2 , constant pressure(4.2 psi, 29.0 kPa) Linear Velocity:40 cm/sec @ 120 ℃ Detector :FID @ 240 ℃ GC_PH01082 Restek General Catalog 147 アプリケーション Column 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. スカイライナー Peaks 1. Methanol 2. Ethanol 3. Acetonitrile 4. Acetone 5. Dichloromethane 6. 1,1-Dichloroethene 7. Nitromethane 8. trans-1,2-Dichloroethylene 9. cis-1,2-Dichloroethylene 10. Tetrahydrofuran 11. Chloroform 12. Ethyl acetate 13. 1,2-Dichloroethane 14. 1,1,1-Trichloroethane PLOT カラム Solvent Mixture on Rt®-Q-BOND (PLOT) GC Columns Application | SOLVENTS & CHEMICALS 溶媒・化学製品 カラムの選択 有機溶剤 Solvent Mixture on Rt®-QS-BOND (PLOT) 相当品対応表 Peaks 1. Methanol 2. Ethanol 3. Acetonitrile 4. Acetone 5. Dichloromethane 6. 1,1-Dichloroethene 7. Nitromethane 8. trans-1,2-Dichloroethylene 9. cis-1,2-Dichloroethylene 10. Tetrahydrofuran 11. Chloroform 12. Ethyl acetate 13. 1,2-Dichloroethane 14. 1,1,1-Trichloroethane ガードカラムについて Column Injection 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. Benzene 1,2-Dimethoxyethane Trichloroethylene 1,4-Dioxane Pyridine Dimethylformamide Methylcyclohexane Toluene 2-Hexanone Chlorobenzene Ethylbenzene m-Xylene p-Xylene o-Xylene :Rt®-QS-BOND, 30 m × 0.53 mm I.D., 20 µm (Cat.No. 1015-11148) フューズドシリカカラム Inj. Vol.:1.0 µL split Liner:4 mm splitless taper (Cat.No. 3015-90090) Inj. Temp.:200 ℃ Split Vent Flow Rate:100 mL/min Oven Oven Temp.:120 ℃ to 240 ℃ at 5 ℃ /min(hold 5.0 min) Carrier Gas :H2 , constant pressure(4.2 psi, 29.0 kPa) Linear Velocity:40 cm/sec @ 120 ℃ Detector :FID @ 240 ℃ メタルカラム GC_PC01081 有機溶剤 PLOT カラム Solvent Mixture on Rt®-S-BOND (PLOT) スカイライナー Peaks 1. Methanol 2. Ethanol 3. Acetonitrile 4. Acetone 5. Dichloromethane 6. 1,1-Dichloroethene 7. Nitromethane 8. trans-1,2-Dichloroethylene 9. cis-1,2-Dichloroethylene 10. Tetrahydrofuran 11. Chloroform 12. Ethyl acetate 13. 1,2-Dichloroethane 14. 1,1,1-Trichloroethane アプリケーション Column Injection 15. 16. 17. 18. 19. 20. 21. 22. 23. 24. 25. 26. 27. 28. Benzene 1,2-Dimethoxyethane Trichloroethylene 1,4-Dioxane Pyridine Dimethylformamide Methylcyclohexane Toluene 2-Hexanone Chlorobenzene Ethylbenzene m-Xylene p-Xylene o-Xylene :Rt®-S-BOND, 30 m × 0.53 mm I.D., 20 µm (Cat.No. 1015-11156) Inj. Vol.:1.0 µL split Liner:4 mm splitless taper (Cat.No. 3015-90090) Inj. Temp.:200 ℃ Split Vent Flow Rate:100 mL/min Oven Oven Temp.:120 ℃ to 220 ℃ at 5 ℃ /min(hold 5.0 min) Carrier Gas :H2 , constant pressure(4.2 psi, 29.0 kPa) Linear Velocity:40 cm/sec @ 120 ℃ Detector :FID @ 220 ℃ GC_PC01080 148 Restek General Catalog
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