溶媒・化学製品

GC Columns Application | SOLVENTS & CHEMICALS
溶媒・化学製品
カラムの選択
ホルムアルデヒド
Formaldehyde on Rt®-U-BOND
(PLOT)
相当品対応表
Peaks
1. Air
2. Carbon dioxide
3. Formaldehyde
4. Water
5. Methanol
Column
Sample
Injection
:Rt®-U-BOND, 30 m × 0.53 mm I.D., 20 µm(Cat.No. 1015-11160)
:Formaldehyde(manual headspace)
ガードカラムについて
Inj. Vol.:10 µL split(split ratio 10:1)
Liner:2 mm split Precision liner w/wool(Cat.No. 3015-90101)
Inj. Temp.:200 ℃
Split Vent Flow Rate:40 mL/min
Oven
Oven Temp.:100 ℃(hold 1 min)to 150 ℃ at 25 ℃ /min(hold 3 min)
Carrier Gas
:He, constant pressure(7.7 psi, 53.1 kPa)
Linear Velocity:39 cm/sec @ 100 ℃
Detector
:TCD @ 200 ℃
Make-up Gas Type:He
フューズドシリカカラム
メタルカラム
GC_CH1137
水中の低級アミン
PLOT カラム
Short Chain Amines in Water on Rtx®-Volatile Amine
225
2
200
スカイライナー
Peaks
1. Methanol
2. Dimethylamine
3. Trimethylamine
4. Methylethylamine
5. Dimethylethylamine
6. Diethylamine
7. Methyldiethylamine
8. Triethylamine
IS = Isopropylamine
pA
175
Column
5
150
Sample
Injection
125
アプリケーション
Inj. Vol.:1.0 µL split(split ratio 15:1)
Inj. Temp.:220 ℃
Split Vent Flow Rate:30 mL/min
Oven
Oven Temp.:40 ℃(hold 10 min)to 250 ℃ at 20 ℃ /min(hold 10 min)
Carrier Gas
:H2 , constant flow
Flow Rate:2.0 mL/min
Linear Velocity:35 cm/sec @ 40 ℃
Detector
:FID @ 250 ℃
100
IS
75
50
6
1
25
0
:Rtx®-Volatile Amine, 60 m × 0.32 mm I.D.
(Cat.No. 1015-11123)
:Short Chain amines
Diluent:Water
Conc.:200-1,000 ppm
0
146 Restek General Catalog
5
3
4
10
Time (min)
7
15
8
20
GC_GN1154
GC Columns Application | SOLVENTS & CHEMICALS
溶媒・化学製品
カラムの選択
第1級アミン
Primary Amine on Rtx®-35 Amine
2,3
5
4
7
8
9
1
Column
Sample
Injection
Diluent:Water
Conc.:50 ppm on-column
Inj. Vol.:1 µL split(split ratio 10:1)
Liner:splitless taper(4 mm), base deactivated(Cat.No. 3015-90091)
Inj. Temp.:250 ℃
Oven Temp.:35 ℃(hold 5 min)
Carrier Gas
:He, constant pressure
Linear Velocity:35.7 cm/sec
Detector
:FID @ 300 ℃
1.0
1.5
2.0
2.5
Time (min)
3.0
3.5
4.0
4.5
メタルカラム
0.5
フューズドシリカカラム
Oven
:Rtx®-35 Amine, 30 m × 0.53 mm I.D.,1.00 µm(Cat.No. 1015-10606)
ガードカラムについて
6
相当品対応表
Peaks
1. Methylamine
2. Dimethylamine
3. Trimethylamine
4. Ethylamine
5. Isopropylamine
6. tert-Butylamine
7. n-Propylamine
8. Diethylamine
9. sec-Butylamine
5.0
GC_CH00578
有機溶剤
Injection
Benzene
1,2-Dimethoxyethane
Trichloroethylene
1,4-Dioxane
Pyridine
Dimethylformamide
Methylcyclohexane
Toluene
2-Hexanone
Chlorobenzene
Ethylbenzene
m-Xylene
p-Xylene
o-Xylene
:Rt®-Q-BOND, 30 m × 0.53 mm I.D., 20 µm
(Cat.No. 1015-11152)
Inj. Vol.:1.0 µL split
Liner:4 mm splitless taper
(Cat.No. 3015-90090)
Inj. Temp.:200 ℃
Split Vent Flow Rate:100 mL/min
Oven
Oven Temp.:120 ℃ to 240 ℃ at 5 ℃ /min(hold 5.0 min)
Carrier Gas
:H2 , constant pressure(4.2 psi, 29.0 kPa)
Linear Velocity:40 cm/sec @ 120 ℃
Detector
:FID @ 240 ℃
GC_PH01082
Restek General Catalog 147
アプリケーション
Column
15.
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
27.
28.
スカイライナー
Peaks
1. Methanol
2. Ethanol
3. Acetonitrile
4. Acetone
5. Dichloromethane
6. 1,1-Dichloroethene
7. Nitromethane
8. trans-1,2-Dichloroethylene
9. cis-1,2-Dichloroethylene
10. Tetrahydrofuran
11. Chloroform
12. Ethyl acetate
13. 1,2-Dichloroethane
14. 1,1,1-Trichloroethane
PLOT カラム
Solvent Mixture on Rt®-Q-BOND
(PLOT)
GC Columns Application | SOLVENTS & CHEMICALS
溶媒・化学製品
カラムの選択
有機溶剤
Solvent Mixture on Rt®-QS-BOND
(PLOT)
相当品対応表
Peaks
1. Methanol
2. Ethanol
3. Acetonitrile
4. Acetone
5. Dichloromethane
6. 1,1-Dichloroethene
7. Nitromethane
8. trans-1,2-Dichloroethylene
9. cis-1,2-Dichloroethylene
10. Tetrahydrofuran
11. Chloroform
12. Ethyl acetate
13. 1,2-Dichloroethane
14. 1,1,1-Trichloroethane
ガードカラムについて
Column
Injection
15.
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
27.
28.
Benzene
1,2-Dimethoxyethane
Trichloroethylene
1,4-Dioxane
Pyridine
Dimethylformamide
Methylcyclohexane
Toluene
2-Hexanone
Chlorobenzene
Ethylbenzene
m-Xylene
p-Xylene
o-Xylene
:Rt®-QS-BOND, 30 m × 0.53 mm I.D., 20 µm
(Cat.No. 1015-11148)
フューズドシリカカラム
Inj. Vol.:1.0 µL split
Liner:4 mm splitless taper
(Cat.No. 3015-90090)
Inj. Temp.:200 ℃
Split Vent Flow Rate:100 mL/min
Oven
Oven Temp.:120 ℃ to 240 ℃ at 5 ℃ /min(hold 5.0 min)
Carrier Gas
:H2 , constant pressure(4.2 psi, 29.0 kPa)
Linear Velocity:40 cm/sec @ 120 ℃
Detector
:FID @ 240 ℃
メタルカラム
GC_PC01081
有機溶剤
PLOT カラム
Solvent Mixture on Rt®-S-BOND
(PLOT)
スカイライナー
Peaks
1. Methanol
2. Ethanol
3. Acetonitrile
4. Acetone
5. Dichloromethane
6. 1,1-Dichloroethene
7. Nitromethane
8. trans-1,2-Dichloroethylene
9. cis-1,2-Dichloroethylene
10. Tetrahydrofuran
11. Chloroform
12. Ethyl acetate
13. 1,2-Dichloroethane
14. 1,1,1-Trichloroethane
アプリケーション
Column
Injection
15.
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
27.
28.
Benzene
1,2-Dimethoxyethane
Trichloroethylene
1,4-Dioxane
Pyridine
Dimethylformamide
Methylcyclohexane
Toluene
2-Hexanone
Chlorobenzene
Ethylbenzene
m-Xylene
p-Xylene
o-Xylene
:Rt®-S-BOND, 30 m × 0.53 mm I.D., 20 µm
(Cat.No. 1015-11156)
Inj. Vol.:1.0 µL split
Liner:4 mm splitless taper
(Cat.No. 3015-90090)
Inj. Temp.:200 ℃
Split Vent Flow Rate:100 mL/min
Oven
Oven Temp.:120 ℃ to 220 ℃ at 5 ℃ /min(hold 5.0 min)
Carrier Gas
:H2 , constant pressure(4.2 psi, 29.0 kPa)
Linear Velocity:40 cm/sec @ 120 ℃
Detector
:FID @ 220 ℃
GC_PC01080
148 Restek General Catalog