Industrial applications of the neutrograph - ILL - EPN

The Renaissance
of
Neutrograph
T. Pirling
Institut Laue Langevin
INSTITUT MAX VON LAUE - PAUL LANGEVIN
Camera Obscura
INSTITUT MAX VON LAUE - PAUL LANGEVIN
INSTITUT MAX VON LAUE - PAUL LANGEVIN
Strain imager
(Railway-head,
Webster, Hughes, ILL)
INSTITUT MAX VON LAUE - PAUL LANGEVIN
G
B
D
g
b
Magnification : b/g
Light efficiency : D/b
Blurr :
D*(b+g)/g
INSTITUT MAX VON LAUE - PAUL LANGEVIN
Sketch from 17th century
Neutron Imaging
SIZE (CM)
L/D
Flux 1 x 106 s-1 cm-2
CONRAD2@HZB (cold)
10
500
5.8
ANTARES@FRM2 (cold)
40x40
400
100
ICON@PSI (cold)
40
600
3.4
Neutrograph@ILL
20
150
3000*
INSTITUT MAX VON LAUE - PAUL LANGEVIN
Neutrograph
Flux : 3 109 n cm-2 s-1
field of
divergence view
(deg)
(mm) D (mm) L/D
1.5
130
Blurr at detector distance
(mm):
50
100
200
1
5000
0.01
0.02
0.04
5
1000
0.05
0.1
0.2
20
250
0.2
0.4
0.8
INSTITUT MAX VON LAUE - PAUL LANGEVIN
Neutron radiography at ILL pre 2010
Electrically driven four-piston BMW engine Universität Heidelberg, Paul-Scherrer-Institut and
TU München
NEUTROGRAPH at ILL Grenoble flux of 3*109
n/cm2s and a collimation of L/D=140.
INSTITUT MAX VON LAUE - PAUL LANGEVIN
First experiment
Pb, protected
by 5mm
borated rubber
Boronated polyethylene
B4C-window
50x50mm2
Pb
Scintillator screen
Fast
shutter
70 mm
Sample positions
Pb
CCD camera
Aperture, B4C
Fritte plus Pb
(alternative
Positions between
here and camera)
Pb
(between 2 and 50 mm
in diameter)
INSTITUT MAX VON LAUE - PAUL LANGEVIN
First experiment
INSTITUT MAX VON LAUE - PAUL LANGEVIN
First experiment
INSTITUT MAX VON LAUE - PAUL LANGEVIN
Neutrograph 10m
INSTITUT MAX VON LAUE - PAUL LANGEVIN
Neutrograph 14m50
INSTITUT MAX VON LAUE - PAUL LANGEVIN
Immediate solution
-Improvements of biological shielding and
operation / safety
-Installation of xyz- and rotation stage
-Optical bench for flexible set-up
-Szintillator screens
-Variable collimator
-> High flux = fast, medium resolution
Radiography/Tomography station
INSTITUT MAX VON LAUE - PAUL LANGEVIN
SALSA –today!
High resolution, multiphase materials
(case hardened steel wind turbine bearing)
radial strain
8000
7000
radial Fe(110)
collimator
strain / 1-^-6
6000
5000
4000
3000
2000
1000
0
-10
-8
-6
-4
position / mm
-2
0
INSTITUT MAX VON LAUE - PAUL LANGEVIN
Stress mapping in extremely large
components
Dissimilar weld
austenitic
INCONEL
ferritic
INSTITUT MAX VON LAUE - PAUL LANGEVIN
Texture imaging
Ferritic
Buttering
Weld
INSTITUT MAX VON LAUE - PAUL LANGEVIN
austenitic
Super SALSA
INSTITUT MAX VON LAUE - PAUL LANGEVIN
Next generation strain scanner
Time of flight
Monochromatic (SALSA)
Continuous white beam
Whole diffractogram
1 diffraction peak at a time
At least large part of
diffractogram
Duty cycle 6% (POLDI)
Reflectivity of crystal
monochromator 60%
Reflectivity of crystal analyser
60%
Large detector coverage
possible
Detector coverage limited to
typ. 5° x 15° in 2q
Large analyser/detector
coverage possible
2 strain components available
1 strain component available
2 strain components available
Good focalisation of prim.
White beam needed
Monochromatic beam is
focalised on sample (~20mm)
Good focalisation of prim.
white beam needed
High activation of sample
Low activation of sample
Even higher activation of
sample
Efficiency depends mainly on
focalisation of prim. beam
INSTITUT MAX VON LAUE - PAUL LANGEVIN
TOMO and SUPER-SALSA
 Strain/stress imaging
 water intake in rocks, medical implants
Manipulation of large samples
Follow dynamic processes (i.e. water,
paint etc intake)
Bragg edge technique: texture imaging
in engineering components, fast strain
mapping
Cultural heritage objects
Wavelength selective imaging
Texture imaging in engineering
components, fast strain mapping
PGNAA with lateral resolution
Stresses, built up during solidification
Fast tomography to follow in-situ
dynamic processes in 3D
Heat treatment
Tensile testing
Variable beam size in both parallel
beam and focusing beam geometries
Multiphase materials, i.e. dissimilar
welds
INSTITUT MAX VON LAUE - PAUL LANGEVIN
Next generation strain scanner
INSTITUT MAX VON LAUE - PAUL LANGEVIN