DM-PLOT Alumina / Na2SO4

DM-PLOT Alumina / Na2SO4
DM-PLOT Alumina / Na2SO4
• Butanes (impurities in acetylene / propadiene) elute before acetylene /
propadiene
• Best separation for butene isomers (impurities in butene streams)
• Propylene elutes after cyclopropane (impurity in propylene)
• Similar to GS-Alumina, HP-PLOT S, Alumina Sulfate PLOT, AT-Alumina,
and CP-Al2O3 / Na2SO4 PLOT
GC Columns
Application Chromatogram
Sample / Compound
Refinery Gas
Page
170
Refinery Gas
Column:
DM-PLOT Alumina / Na2SO4
1. Methane
2. Ethane
3. Ethylene
4. Propane
5. Propylene
6. Isobutane
7. n -Butane
8. Propadiene
9. Acetylene
10. trans -2-Butene
30 m x 0.53 mm x 10.00 µm
Sample:
Refinery gas
Cat. No.:
8806
Index:
CSR01139
Oven Temp.:
60 ºC (hold 2 min) to 200 ºC (hold 1 min) at 10 ºC/min
Carrier Gas:
He, constant pressure ( 5.0 psi, 34.5 kPa )
37.3 cm/sec 60 ºC
Injection:
Split, 10 µL, 200 ºC
Split Vent Flow Rate: 40 mL/min
Detector:
FID, 200 ºC
Makeup Gas:
N2
DM-PLOT Alumina / Na2SO4 Ordering Information
ID (mm)
0.25
0.32
0.53
82
df (µm)
4.00
5.00
10.00
www.dikmatech.com
MAOT (ºC)
to 200
to 200
to 200
30 m
Cat. No.
8860
8804
8806
50 m
Cat. No.
8805
8807
11. 1-Butene
12. Isobutylene
13. cis -2-Butene
14. Isopentane
15. n -Pentane
16. 1,3-Butadiene
17. trans -2-Pentene
18. 2-Methyl-2-butene
19. 1-Pentene
20. cis -2-Pentene
21. Hexanes
DM-PLOT Alumina / KCI
DM-PLOT Alumina / KCl
• C4 hydrocarbons (impurities in butane / isobutane) elute after acetylene
• 1,3-Butadiene elutes after methyl acetylene (impurity in 1,3-butadiene)
• Similar to GS-Alumine / KCI and CP-Al2O3 / KCI PLOT
Application Chromatogram
Page
170
GC Columns
Sample / Compound
Butane Lighter Fluid
Butane Lighter Fluid
Column:
DM-PLOT Alumina / KCl
50 m x 0.53 mm x 10.00 µm
Cat. No.:
8813
Index:
CSR01086
Oven Temp.: 45 ºC (hold 1 min) to 200 ºC (hold 3.5 min) at 10 ºC/min
1.
2.
3.
4.
5.
6.
7.
8.
Carrier Gas: H2, constant pressure (8.0 psi, 55.2 kPa) 74 cm/sec at 45 ºC
Sample:
Butane lighter fluid
Injection:
Valve, 100 µL, 200 ºC
Detector:
FID, 200 ºC
Methane
Ethane
Propane
Isobutane
n -Butane
trans -2-Butene
1-Butene
Isobutylene
DM-PLOT Alumina / KCI Ordering Information
ID (mm)
0.25
0.32
0.53
df (µm)
4.00
5.00
10.00
MAOT (ºC)
to 200
to 200
to 200
30 m
Cat. No.
8861
8808
8811
50 m
Cat. No.
8809
8813
www.dikmatech.com
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