DM-PLOT Alumina / Na2SO4 DM-PLOT Alumina / Na2SO4 • Butanes (impurities in acetylene / propadiene) elute before acetylene / propadiene • Best separation for butene isomers (impurities in butene streams) • Propylene elutes after cyclopropane (impurity in propylene) • Similar to GS-Alumina, HP-PLOT S, Alumina Sulfate PLOT, AT-Alumina, and CP-Al2O3 / Na2SO4 PLOT GC Columns Application Chromatogram Sample / Compound Refinery Gas Page 170 Refinery Gas Column: DM-PLOT Alumina / Na2SO4 1. Methane 2. Ethane 3. Ethylene 4. Propane 5. Propylene 6. Isobutane 7. n -Butane 8. Propadiene 9. Acetylene 10. trans -2-Butene 30 m x 0.53 mm x 10.00 µm Sample: Refinery gas Cat. No.: 8806 Index: CSR01139 Oven Temp.: 60 ºC (hold 2 min) to 200 ºC (hold 1 min) at 10 ºC/min Carrier Gas: He, constant pressure ( 5.0 psi, 34.5 kPa ) 37.3 cm/sec 60 ºC Injection: Split, 10 µL, 200 ºC Split Vent Flow Rate: 40 mL/min Detector: FID, 200 ºC Makeup Gas: N2 DM-PLOT Alumina / Na2SO4 Ordering Information ID (mm) 0.25 0.32 0.53 82 df (µm) 4.00 5.00 10.00 www.dikmatech.com MAOT (ºC) to 200 to 200 to 200 30 m Cat. No. 8860 8804 8806 50 m Cat. No. 8805 8807 11. 1-Butene 12. Isobutylene 13. cis -2-Butene 14. Isopentane 15. n -Pentane 16. 1,3-Butadiene 17. trans -2-Pentene 18. 2-Methyl-2-butene 19. 1-Pentene 20. cis -2-Pentene 21. Hexanes DM-PLOT Alumina / KCI DM-PLOT Alumina / KCl • C4 hydrocarbons (impurities in butane / isobutane) elute after acetylene • 1,3-Butadiene elutes after methyl acetylene (impurity in 1,3-butadiene) • Similar to GS-Alumine / KCI and CP-Al2O3 / KCI PLOT Application Chromatogram Page 170 GC Columns Sample / Compound Butane Lighter Fluid Butane Lighter Fluid Column: DM-PLOT Alumina / KCl 50 m x 0.53 mm x 10.00 µm Cat. No.: 8813 Index: CSR01086 Oven Temp.: 45 ºC (hold 1 min) to 200 ºC (hold 3.5 min) at 10 ºC/min 1. 2. 3. 4. 5. 6. 7. 8. Carrier Gas: H2, constant pressure (8.0 psi, 55.2 kPa) 74 cm/sec at 45 ºC Sample: Butane lighter fluid Injection: Valve, 100 µL, 200 ºC Detector: FID, 200 ºC Methane Ethane Propane Isobutane n -Butane trans -2-Butene 1-Butene Isobutylene DM-PLOT Alumina / KCI Ordering Information ID (mm) 0.25 0.32 0.53 df (µm) 4.00 5.00 10.00 MAOT (ºC) to 200 to 200 to 200 30 m Cat. No. 8861 8808 8811 50 m Cat. No. 8809 8813 www.dikmatech.com 83
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