221 Chapter 6 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing Sergio J. Sanabria Laboratory for Wood Physics, Institute for Building Materials, ETH Zurich, Switzerland Jürg Neuenschwander Swiss Federal Laboratories for Materials Science and Technology, Switzerland Roman Furrer Swiss Federal Laboratories for Materials Science and Technology, Switzerland Peter Niemz Laboratory for Wood Physics, Institute for Building Materials, ETH Zurich, Switzerland Urs Sennhauser Swiss Federal Laboratories for Materials Science and Technology, Switzerland ABSTRACT The objective of this chapter is to provide an overview of novel non-destructive testing methodologies for bonding quality assessment in glued laminated timber developed within a recently completed Swiss National Science Foundation research project (Sanabria, 2012). The focus is set on air-coupled ultrasound testing, which has previously been applied to wood-based panels typically up to 50 mm thick. A novel prototype capable of transmitting ultrasound signals through up to 500 mm thick glulam was developed. A computerized-scanning system allowed imaging of DOI: 10.4018/978-1-4666-4554-7.ch006 Copyright ©2014, IGI Global. Copying or distributing in print or electronic forms without written permission of IGI Global is prohibited. Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing the position and geometry of defects within the bonding planes. A normal transmission setup allows a global assessment of defective bonding planes stacks. Latest results are as well shown for a recently patented slanted lateral transmission setup, which allows separate assessment of individual bonding planes with unlimited beam height and length. The investigations allowed an improved understanding of the wave propagation phenomena in thick laminated timber components through both analytical calculations and finite-difference numerical simulations. An overview of the main findings is as well provided. Future research is planned to combine the developed theoretical and experimental tools in a tomographic inspection method. INTRODUCTION The use of wood as a construction material currently experiences a renaissance not only due to its undisputable renewable, environmental-friendly and aesthetic nature, but as well owing to its high strength to weight ratio, durability and resistance against chemical attack, easy machining and predictable fire performance, which are competitive with respect to established construction materials like steel or reinforced concrete (Forest Products Laboratory, 2010). During the last century, developments in fabrication technology and a declining volume of large, old-growth timber have led to the progressive replacement of traditional solid wood structural members by highly engineered adhesively-bonded composites. Glued laminated timber (glulam) is a layered composite manufactured by gluing and stacking timber lamellas (for softwoods typically 35 to 40 mm thick and 100 to 300 mm wide), which are sawn and finger-jointed parallel to the wood grain direction. This arrangement homogenizes mechanical properties, and allows the fabrication of large structural beam or column products of straight or curved form, from 2 laminations up to typically 2.5 m high and 50 m long stacks (Bodig & Jayne, 1982; Dunky & Niemz, 2002; EN 386, 2001). With the proliferation of glued timber constructions, there is an increasing concern about safety problems related to the delamination of timber glue lines. Delaminations are caused by manufacturing errors and in-service unfavorable load combinations (Hansson & Larsen, 2005). A moisture-resistant adhesive and a homogeneous stress distribution in the glue lines are required for a durable bond. Polyurethane adhesives require a minimal ambient humidity for curing whereas urea resins can be hydrolytically removed due to temperature and humidity gradients (Kägi et al., 2006; Schrödter & Niemz, 2006). Residual stresses are induced by improper adhesive curing, long-sustained loads and swelling and shrinkage due to moisture gradients in large glued cross-sections (Gustafsson et al., 1998). Bond delamination is influenced by both the adhesive and wood phases (Frihart, 2009), the mechanisms 222 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing leading to debonding initiation are still not well understood (Bucur, 2011). Several recent building collapses were related to bonding failure, which should be prevented in the future with a timely defect detection (Blass & Frese, 2010). It is therefore a demanding necessity to develop measurement technologies which assess bonding defects in glued timber structural members during their full life cycle, detecting both defective glue lines during manufacturing, tooling or processing and in-service developed delaminations. Non-destructive testing technologies, which probe the full structure without damage or modification and in a cost-efficient way, are desirable. Apart from avoiding predictable hazards for lives and property, the life span of existing glued timber constructions can be optimized if accurate information is available about when, where and which restoration of glue lines is required. BACKGROUND Current standardized delamination testing methods for timber laminates rely on destructive tests for random specimens extracted from a specific production process or from an in-service structural member (increment core) (ANSI/AITC 19011-2007, 2007; EN 386, 2001). Mechanical tests and accelerated aging tests with changing climatic conditions provide direct measurements of the ultimate strength and fracture behavior, microscopic methods probe adhesive-wood interaction and fracture at microstructural and chemical level. These methods provide information on significant drifts from established production parameters and can identify onsite deterioration processes which affect the full structural member. However, they can neither provide quality assurance for each single manufactured specimen nor identify localized damage for in-service structures. The established non-destructive testing methodologies for adhesive bond testing in glued timber structures are still at a primary stage. Condition assessment practice generally relies on techniques that have proven to be adequate for decay inspection, such as visual inspection, tapping, resistance drilling, or stress wave timing in suspected damage regions, but which are not necessarily able to detect inner lamination faults in structural laminated beams. Feeler gauges can be used to manually estimate crack depth, the process is however slow and only detects edge open cracks with straight paths. Proof loading provides information about the remaining structure strength provided that live load can be applied to the structure in a cost-efficient and safe way, which is often only possible for timber bridges (Aicher, 2008; Kasal, 2010; Ross et al., 2004). An alternative to these methods is to non-destructively probe the structures with propagating radiation or vibration fields, from which delamination signatures can be extracted. The investigation of such methods for wood has significantly advanced 223 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing in the last two decades, yet some important limitations still exist. Thermography allows accurate subsurface delamination imaging, but is limited to millimeterthick laminates, such as veneer overlays, due to the inherent thermal damping of the porous wood microstructure (Meinlschmidt, 2005; Tsuchikawa et al., 2000). The same restrictions apply for optic methods, which are based on the detection of surface deformations (Castellini et al., 2008). X-rays are able to penetrate thick structural members. Radiation safety needs to be strictly considered for a secure equipment operation. Off-the-shelf portable systems are available which have been applied in glulam constructions (Hasenstab et al., 2004). However, radiographic images obtained with these systems provide a reduced sensitivity to debonding. Applications for finger joint production control have been reported (Hu & Gagnon, 2007). A significantly higher contrast is obtained with three-dimensional computed tomography reconstruction (Hu & Gagnon, 2007; Sirr & Waddle, 1999). However, in this case a large number of radiographic projections is required in a full range of orientations between sample and radiation path, which in structural applications is often not feasible due to geometric and measurement time constraints. Mechanical vibration methods have a long standing tradition in wood science; however, they have only been applied to a minor extent to lamination assessment in glued timber. Low-frequency (<1 kHz) modal analysis performs well for dynamic measurements of global strength properties of timber laminates and is an interesting alternative for quality assurance during manufacture (Gsell et al., 2007), difficulties in defect localization and a high sensitivity to boundary conditions however constrain on-site application. Acoustic emission is based on passive sensor technologies which are potentially capable to detect and localize fracture initiation in glulam (Dill-Langer et al., 1999), yet a practical application requires a large number of sensors to be permanently embedded in each structural member. Ultrasound testing is a well-established tool for non-destructive testing of adhesively bonded composite materials due to its high sensitivity to cracking and delamination, which behave like mechanical discontinuities to ultrasonic wave propagation (Maeva et al., 2004). Moreover, the technology is safe, low-cost and easily portable on-site. Typical testing frequencies for wooden structures range between 20 and 200 kHz. Sufficient ultrasound energy coupling into structural timbers has traditionally required the pressing of the transducers onto the sample surfaces (contact techniques). These methods have shown potential for the detection and characterization of cracks and delaminated areas in timber structural members. Stress wave timing allow edge open crack depth estimates (Garab et al., 2010), the measurement of diffuse ultrasonic energy (acousto-ultrasonics) is applicable to bond curing monitoring and finger-joint production control (Anthony & Philipps, 1993; Beall, 1989). Large planar cracks and lamination defects in structural glulam have been detected with longitudinal wave through-transmission and shear wave pulse-echo measurements with perpendicular 224 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing insonification with respect to the bonding planes (Aicher et al., 2002; Dill-Langer et al., 2005a, 2005b; Dimanche et al., 1994). A shear wave spring-loaded pulse-echo array transducer for reinforced-concrete industry has been applied to single-sided in situ inspection of glulam; cracks could be detected with both perpendicular and parallel insonification with respect to the lamination planes (Hasenstab, 2007; Hasenstab & Osterloh, 2009). Overall, a minimum acceptable measurement reproducibility (15% amplitude error) requires a delicate and generally manually supported adjustment of the coupling pressure at each measurement point (Dill-Langer et al., 2005b; Hasenstab, 2006), which in practice restricts the inspection to a reduced number of measurement points. Therefore, only rough defect position and geometry estimates are practical. Moreover, ultrasonic waves strongly interact with the heterogeneous structure of wood, leading to complex wave propagation phenomena and a strong variability in the ultrasound signal detected in defect-free regions, which complicate the discrimination between defects and material heterogeneity, especially if only few measurement points are available. A discussion of the main ultrasound wave propagation phenomena in glued timber structures is provided in the next sections. Air-Coupled Ultrasound (ACU) is a relatively new transducer technology which overcomes the contact limitation between ultrasound transducers and solid samples. The transducers are held separated by an air gap from the sample surface, which allows a simple acquisition of a large grid of measurement points, for example, by means of a mechanical scanner, and a flexible positioning and orientation of the transducers with respect to the inspected samples. This shows a high potential for the discrimination of defects from background variability. Moreover, the measurement reproducibility significantly outperforms the one of contact techniques, with <1% reproducibility error after one year measurement (Sanabria et al., 2010). These highlights provide an unexplored potential for structural health monitoring based on difference imaging with respect to a defined reference state. The classical constraint of ACU is a low coupling efficiency of ultrasound signals into solid materials (<0.5% of input pressure into wood, Figure 1), which has traditionally limited the inspection to thin plate materials. In the case of wood industry, <50 mm thick woodbased composites (particleboards, fiberboards, plywoods and laminated veneered lumbers) are typically tested with this methodology (Benedetti, 2003; Blum, 1997; Fagus GreCon Greten GmbH & Co. KG, 1994). A careful adjustment of the air gap between transducers and sample by means of metering rollers in contact with the sample allows a higher coupling of ultrasound energy (power sonic resonance) and has achieved inspection of up to 200 mm thick laminated veneered lumbers (Fuchs, 2011). Recent developments in off-the-shelf transducer technologies have recently allowed tomographic inspection of 300 mm thick concrete without any contact between sample and measurement system (Hall, 2011). 225 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing Figure 1. ACU delamination assessment principle. A quasi-specular reflection of ultrasound waves is observed at wood-air interfaces, these lead on one hand to substantial coupling loss (Lcoupling) and on the other hand to an increased signal attenuation (Ljoint) across a bonding defect. In this context, the investigation of the application of air-coupled ultrasound to the bonding quality assessment of glued laminated timber structures is timely. A four-year Swiss National Science Foundation research project has addressed this research gap in the frame of a recently completed doctoral thesis (Sanabria, 2012). The investigations covered three fundamental topics: • • • The development of a theoretical model of ultrasound wave propagation in glulam based on state-of-the-art mechanical models for solid wood. The design and implementation of an ACU prototype system capable of transmitting and detecting ultrasound signals through structural multilayer glulam in flexible configurations. The theoretical and experimental investigation of the applicability of specific ACU inspection configurations for the detection and characterization of bonding defects in glulam. Next, a comprehensive overview of the results of these investigations is provided including latest non-published results. 226 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing ACU Wave Propagation in Timber Laminates The bonding assessment is based on the measurement of the attenuation of an ultrasound beam transmitted between a transmitter/receiver transducer pair (Tx/ Rx) through a delaminated timber glue line (Figure 1). Ultrasonic waves are quasispecularly reflected at air/solid interfaces, which leads to a significantly increased attenuation if a small air gap (crack or debond) is present at the glue line. The voltage level recorded at the receiver transducer is directly proportional to the pressure level integrated on its surface. The ratio between the voltage level recorded through a reference (defect-free) and a delaminated glue line gives the attenuation or contrast Ljoint at the joint, which is conveniently expressed in logarithmic units with Ljoint = 6, 12, 20, 40, 60 dB corresponding to an attenuation factor of x2, x4, x10, x100, x1000 in a linear scale. For insonification perpendicular to the bonding planes, the maximum available contrast is given by Ljoint = 20 log10 (4ZaZw/(Za+Zw) 2), where Za, Zw are the acoustic impedances of air and wood, defined as Z = (ρ C)0.5, where ρ and C are the density and stiffness for each material. In the case of Norway spruce (Picea abies Karst.), a softwood, one of the most representative wood species used in glulam production, the maximum contrast is Ljoint = 50 dB. The variations are not large between wood species, with for example Ljoint = 56 dB for European beech (Fagus sylvatica L.), a representative hardwood. The ultrasound beam is transparent to well-glued joints; the adhesive product therefore does not play a significant role. The contrast is reduced with decreasing air gap separation between timber lamellas and decreasing testing frequency, due to the constructive interference of ultrasound pulse echoes at the glue joint. The maximum contrast of Ljoint = 50 dB is reduced down to 20 dB for 10 µm thin air gaps between delaminated interfaces and typical 100 kHz pulses. This value is of the order of the size of the cellular micro voids in wood, which defines a minimum air separation between timber lamellas, thus, in practice, an efficient blocking of the transmitted ultrasound beam is expected by asymptotically thin discontinuities between timber lamellas and with a lateral surface larger than the extension of the pressure field incident into the glue line (Sanabria et al., 2010, 2010d). The assessment of bonding planes requires the transmission of an ultrasound beam through at least its adjacent timber lamellas. The wave propagation in timbers is consequently strongly influenced by the heterogeneous and anisotropic wood material structure. The density distribution, the annual ring structure and the grain angle are the main material parameters influencing the ultrasound wave propagation. In a first approximation, a homogenized density distribution is assumed and the long dimension of the lamellas is considered to be well-oriented to the wood grain direction (L), the annual ring structure being the main influence in the wave propagation. In particular, as a consequence of wood’s anisotropy, a normally inci227 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing dent ultrasound beam experiences significant trajectory shifts by an angle χ within a timber lamella (Figure 2). The angle χ is a function of the ring angle ϕ between the insonification axis and the direction tangential to the annual rings (T). In general, the ring angle ϕ locally changes within each timber lamella, so that the angle χ is position-dependent. A two-dimensional Finite-Difference Time-Domain (FDTD) numerical simulation model was developed to simulate ACU wave propagation through arbitrary heterogeneous and anisotropic material distributions. The model allows the direct definition of material properties at each pixel with high accuracy and numerical stability. By combining established orthotropic stiffness models of wood, which are defined with respect to the material axes (L, R, T), and by performing local transformation of the stiffness tensor as a function of ϕ, the curvature of the annual rings in individual timber lamellas is fully characterized. Air-coupling, bonding planes and delaminations are directly implemented by defining the mechanical properties of air and adhesive at the corresponding pixels. The two-dimensional model implements wave propagation through arbitrary sections of a glued laminated timber beam. The FDTD model was validated by comparing the simulated χ for lamellas with constant ϕ against analytical calculations based on plane wave solutions of the wave propagation equations. Figure 2a shows simulation time snapshots of the calculated Figure 2. Finite-difference time-domain (FDTD) simulation of ACU wave propagation through Norway spruce timber lamella as a function of annual ring orientation ϕ. Due to the material anisotropy, the ultrasound beam deviates from the insonification direction by a ϕ-dependent angle χ. a) Simulation snapshots of the stress fields σyy through air and wood. b) Comparison of χ calculated from analytical plane wave solutions with geometrically calculated values from FDTD snapshots, a total of 90 simulations were run for each of the represented ϕ - χ pairs. 228 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing stress fields σyy illustrating the ACU transmission of an ultrasound pulse through a 40 mm thick timber lamella. At the interfaces (air-wood, or wood-wood) three modes are coupled (quasi-longitudinal QP, quasi-shear in-plane QSV and shear outof-plane SH), out of which the QP mode is dominant. The shifts of the QP mode range between -30° and 10° and tend to align the ultrasound beam with the principal material axes (R and T), if the insonification direction coincides with these axes no shifts (χ = 0°) are theoretically expected. The shift χ obtained from the FDTD simulations is in excellent agreement with the analytical calculation (Figure 2-right), the uncertainties (<3°) being rather due to small physical differences between the limited-width pulsed ultrasound beam and the analytical plane wave front than due to inaccuracies of the model. In fact, by doubling the width of the ultrasound beam the uncertainties are reduced to <0.3°. A similar agreement is observed between FDTD and analytical prediction for other relevant wave propagation parameters, for example, the ultrasound transmission through a delaminated glue line as a function of the air gap separation. In addition to the described wave propagation phenomena, the strong gradients of mechanical properties across the periodical earlywood/latewood transitions in the annual rings and the grain angle distortion around knots introduce strong scattering in the transmitted pressure fields and contribute to the overall variability of the ultrasonic signal in defect-free regions. The porous microstructure of wood introduces at 100 kHz a material attenuation coefficient of 2.4 dB cm-1 in the RT plane. Furthermore, as a consequence of the strong anisotropy between grain (L) and cross-grain (RT) directions, an incident circular-section ultrasound beam deforms into an elliptical shape elongated along L when transmitted through wood, leading to a lower lateral resolution along L. Since the described phenomena are accumulative, the wave propagation becomes increasingly complex with longer propagation paths in wood. Development of ACU Prototype for Structural Timber Inspection An air-coupled ultrasound system prototype was developed to inspect structural timbers up to a thickness of 500mm (Figure 3). State-of-the-art high-efficiency aircoupled ultrasound transducers (50 mm diameter 100 kHz Gas Matrix Piezoelectric Composites, The Ultran Group Inc., State College, PA, USA) were combined with high-power pulsed electronics (>1000 Vpp), low-noise receiver electronics (input referred noise of 0.9 nVrms Hz-0.5) and dedicated signal processing. This system allowed bridging the total 115 dB signal loss through a defect-free 280 mm thick glulam beam (including coupling loss and material attenuation) with a signal-to-noise ratio (SNR) of 40 dB, which provided enough dynamic range to resolve bonding defects from the variability in ultrasound signals introduced by the timber material. 229 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing Transmitter and receiver are positioned on two opposing surfaces of the inspected glued laminated timber beam. An arbitrary waveform generator generates an ultrasonic pulse which is amplified by the pulser and excited into the transmitter transducer. The propagated signals are captured by the receiver transducer and amplified by the low-noise receiver chain, the resulting time waveforms are digitized by an analog to digital converter for further signal processing. The transmitter-receiver pair is moved with respect to the sample surfaces with a computerized mechanical scanning system; at each scanned pixel ultrasound signals are recorded. From the recorded datasets, ultrasound images of the defect positions and geometries are calculated. The excitation and recording of ultrasound signals are synchronized with the scanner movement by means of a control trigger. Due to the pulsed operation principle, there is usually no need of physically blocking spurious signals transmitted in air around the sample, which is particularly attractive for on-site inspection. Moreover, the adjustment of the air gaps between transducers and sample is not critical, allowing for fully non-contact operation. Air-Coupled Ultrasound Normal Transmission Testing A global bonding quality assessment was investigated with a normal transmission setup (NT). Figure 3 illustrates the geometrical configuration and data acquisition sequence. The transmission is performed perpendicular to the bonding plane stack; the transmitter and receiver transducers are scanned as a fix unit in a raster fashion along the beam width (Y) and length (X). For each scanned position a pulsed ultrasound time waveform is recorded. The recorded datasets are processed to generate images of the internal bonding defects of the sample; the peak value of a selected Figure 3. Air-coupled ultrasound system referred to normal transmission setup 230 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing time portion of the recorded ultrasound waveforms is represented as a function of the scanned position. The calculated amplitude values are represented normalized in logarithmic scale with respect to its mean value in reference well-glued regions (Amplitude(dB) = -Attenuation(dB)). Low signal levels are consequently associated with defect positions. Figure 4 demonstrates ACU NT imaging of delaminations induced by strong climate variations. The test sample consists of two 20 mm thick lamellas, one made from Norway spruce and the other one from European beech, which were glued together with a one-component polyurethane adhesive. The samples were then exposed to exterior climatic conditions for several months until delaminations occurred as a consequence of internal stresses developed in the bond line due to climate variations. The delamination process was accelerated by the gradient of mechanical properties between both wood adherends. The delamination depth was measured at the sample edges with a 100 µm thick feeler gauge and is marked in the ACU image. Drops of ACU signal amplitude were consistently identified at delamination positions. The ACU image shows additional delamination indications (DI) at positions that were not accessible by the feeler gauge. Overall, a broad range of bonding defects (non-glued areas, saw cuts, cracks, non-adherent glue, debonding of vibration-welded joints) can be detected as long as there exists an asymptotically thin material discontinuity between timber lamellas. For laminates of comparable thickness, the lateral resolution in the images is limited by the beam width of the ultrasound beam excited by the ACU transmitter (around 35 mm) With additional deconvolution image processing, >12 mm diameter adhesive droplets were detected in 10 mm thick test samples (Sanabria et al., 2009, 2010, 2010b). Figure 4. ACU NT imaging of delaminations induced by strong climate variations. The ACU assessment successfully detects the delamination areas identified with the feeler gauge, moreover providing additional defect indications (DI). 231 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing As the thickness of the timber laminate increases, so does the variability of the ultrasound signals recorded in defect-free regions and the spread of the ultrasound beam within the sample, leading to an overall reduction in the lateral resolution of the defect images. Figure 5 shows an amplitude profile along the length of a glulam beam in which non-glued regions of specific lengths were defined. The same glulam beam was assessed after gluing together, two, four and six timber lamellas, the gluing defects always located at the middle bonding plane. As expected, the lateral resolution is anisotropic and lowest along the grain direction, with a 20 dB amplitude drop at 22, 55 and 110 mm from the defect in the wood grain direction, and at 9, 16 and 24 mm in cross-grain direction for 78, 150 and 230 mm thick glulam, respectively. The described method is thus well-suited for the detection of lengthwise elongated cracking and delamination, which frequently occur in glulam constructions (Sanabria et al., 2010c, 2010d, 2011a, 2011b). Air-Coupled Ultrasound Slanted Lateral Transmission Testing The setup outlined in Figures 3 to 5 performs a global assessment of the full laminated stack, allowing the identification of defective areas along their length and width. For structural glulam with a large number of lamellas (beam height >300 mm), and especially for on-site inspection of glulam constructions, it is important to determine which specific bonding planes are defective. This information allows to quantify the structural relevance of the defect and to decide whether either no action, reinforcement or a full replacement of the faulty member is required. A novel ACU slanted lateral transmission setup (SLT) has been developed to address these requirements (Sanabria, et al., 2011c, 2013) (Figure 6). An ultrasound beam Figure 5. Detection of gluing defects along the length X of glulam beam as a function of the number of laminations. The method provides a global assessment of bonding quality along the full lamination stack. The lateral resolution decreases with increasing number of laminations. 232 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing Figure 6. Air-coupled ultrasound slanted lateral insonification of glulam: Left) setup; Right) ultrasound waveforms in well-glued and defective bonding planes. Individual bonding planes can be tested separately; the assessment is not limited by the height and length of the glulam beam. is transmitted and received through opposite lateral faces of the beam. The inclination of the ultrasound beam (typically <10°) is adjusted with respect to the wave propagation models to achieve a controlled refraction path across single bonding planes. A user-defined wave propagation path is obtained by adjusting the relative orientation and inclination of the ACU transducers. The transducers are then scanned as a single unit in beam height (Z) and length (X) directions. The assessment is not limited by the height and length of the beam. Defects in individual bonding planes are successfully separated. For example, in Figure 6 the third glue line contains a full width non-glued area whereas the fourth glue line is defect-free. At the glued position, the ultrasound beam is transmitted through the pre-calculated defect-free wave propagation path (T1-R1) and a signal is received through wood at the Rx (Glued). In the case of the defective glue line, the ultrasound beam refracted into the sample is scattered by the gluing defect off the pre-calculated path (T2-R2), and a reduced signal level for waves propagating through wood is therefore observed at the receiver position R2 (Defect). Spurious paths diffracted in air around the sample (Air) arrive delayed in time and can be filtered out in time with the pulsed electronics. Defect maps indicating the position and extension of the delaminated areas are obtained with this method, following a similar data evaluation principle of the recorded datasets as in the case of the ACU NT setup. Amplitude drops in the images are associated to bonding defect positions. Figure 7 illustrates ACU SLT imaging of delaminations in a commercial multilayered glued laminated timber sample (200 x 395 x 750 mm3). The sample was repeatedly tested, first as provided by the manufacturer, then after introducing one saw cut D2 in the bonding plane B5, and finally after introducing additional saw cuts D1, D3 and D4 in the bonding planes B3, B7 and B8, respectively. The mean 233 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing Figure 7. ACU SLT imaging of glulam sample with multiple bonding defect regions D1, D2, D3, and D4 (saw cuts at bonding plane positions): a) setup; b) and c) ACU SLT images. Experiments were performed for two specific measurement configurations leading to different refraction paths, so that the ultrasound beam interacted with two timber lamellas (∆h = 2d, Figure 7b) and with three timber lamellas (∆h = 3d, Figure 7c). For each case, ACU SLT images were obtained before introducing the defects (left), after introducing the defect D2 (middle), and after introducing the remaining defects D1, D3, and D4 (right). The assessment allows identification of the defective bonding planes (B3, B5, B7, and B8), providing information about the length and width extension of the defect areas. 234 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing timber lamella thickness is d = 40 mm. Experiments were performed for two specific measurement configurations: in the first one the ultrasound beam refracted within the sample interfaces a reduced portion of the beam height ∆h corresponding to two timber lamellas (∆h = 2d, Figure 7b), in the second one the refracted beam interfaces three timber lamellas (∆h = 3d, Figure 7c). The bonding planes B1, B2 … B9 are marked in the ACU SLT images with horizontal lines with respect to the Z positions insonified by the transmitter transducer Tx. Full-width defects lead to an amplitude reduction in the ACU SLT images in a region below the tested bonding plane with a Z extension equal to ∆h. This region corresponds to positions for which the propagation of the transmitted ultrasound beam is blocked by the bonding defect (Figure 7a). Similarly, defect areas of a fraction f = 0…1 of the beam width are identified in the ACU SLT images as a reduced amplitude region with a Z extension of f·∆h. For example, for ∆h = 2d = 80 mm (Figure 7b), full-width defects (D1, D2, and D3) lead to a reduced ACU signal in a 80 mm Z-region below the respective defective planes B3, B5 and B7. Similarly, the half-width bonding defect D3 can be identified as a reduced amplitude region with a Z extension of 0.5∆h = 40 mm below the defective plane B8. In the case of the SLT assessment with ∆h = 3d (Figure 7c), the full-width defects introduce attenuation regions of ∆h = 3d = 120 mm, whereas the half-width defect introduces an attenuation region of 0.5∆h = 60 mm. The defective bonding planes are consistently identified in both measurement configurations. The length of the defective areas is directly determined from the X extension of the reduced amplitude regions in the ACU SLT images. The choice of the insonified beam height portion ∆h is a trade-off between ultrasound signal variability in defect-free regions, contrast at defect areas and signal-to-noise ratio at the receiver transducer. The higher ∆h the longer the wave propagation paths in wood and consequently the higher the signal variability and the higher the attenuation – consequently the lower the signal-to-noise ratio. Conversely, the higher ∆h the smaller the sample width fraction of the tested bonding planes interacting with the ultrasound beam and thus the better lateral resolution along the sample width. The higher ∆h as well the lower the spurious ultrasound energy diffracting around the defect being captured by the receiver and thus the higher contrast at defective areas. Overall, values of ∆h = K·d with K = 1…3 were shown to provide a good performance. The values of K were generally chosen as integer values 1, 2 and 3 for simplicity in the interpretation of the ACU images, although other values are as well possible. For K > 1, an overlap of the information extracted from adjacent bonding planes is present in the ACU images. This is for example clearly visible in Figure 7c, where the bonding defects D1 and D2 are present in the same length region X and in two bonding planes B3 and B5 separated by two timber lamellas. Since in this case ∆h = 3d, there is an overlap between the defect regions 235 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing D2 and D1 in the ACU image, which reduces the discrimination capacity along Z. However, since delaminations are assumed to be scarcely located in both X and Z, this overlaps are in general not problematic, and otherwise can be further resolved by repeating the assessment with lower K in the conflictive regions. The described SLT setup assumes a constant wave propagation path between transmitter and receiver transducers. However, as discussed in the theoretical section, the wave propagation paths in timber laminates are highly influenced by the annual ring structure in the timber lamellas. In order to gain further understanding about these mechanisms, finite-difference time-domain simulations were run for specific defect inspection scenarios as a function of the annual ring curvature, which was characterized by the position of the stem pith for each sawn timber lamella. In order to keep the number of case studies tractable, a series of practical simplifications were introduced. The annual rings were assumed to grow cylindrically with respect to the tree stem. All lamellas were of a same representative size (40 x 200 mm2) and showed the same year ring curvature. The horizontal pith position was equal to center width of the timber lamella. The vertical position of the pith y was chosen as a multiple of the lamella width d, with y/d = -3, -2, -1, 0, 1, 2, 3. Negative and positive y/d values correspond to convex and concave year ring curvatures, respectively. y/d = 0 corresponds to a scenario in with the pith P is located at middle lamella width. The highest absolute y/d values are given by the usual diameter of the tree stems from which the lamellas are cut from (Norway spruce). Gluing defects of 25%, 50%, 75% and 100% width section were assessed with ∆h = 2d, the defects were centered at middle width except for the 50% width defects, which were as well simulated at both edge positions. The insonification position was adjusted to achieve the maximum possible interaction with the defect. The theoretical wave propagation paths were calculated by assuming an isotropic material with sound speed equals to the longitudinal wave velocity parallel to the timber lamellas. The orientation and position of the ACU transmitter Tx was adjusted accordingly. Figure 8 represent the waveform peak stress distribution (σyy) simulated within the glued laminated timber samples as a function of y/d and the defect size, which gives an idea of the main wave propagation paths. Overall, the annual ring structure has a strong influence on the ultrasound wave propagation, leading to an energy distribution which is not concentrated within the calculated propagation paths, but that to a large extent “follows” the annual ring curvature. This leads to significant position drifts in the wave propagation paths, and to spurious signal coupling in the timber lamellas adjacent to the inspected ones. Some general trends can be identified. Differentiated stress distributions are obtained for concave and convex year ring orientations. The simulated stress distribution fits closer to the theoretical wave propagation paths the higher the absolute value of y/d, namely the lower the annual ring curvature. Above y/d = 2 and below 236 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing Figure 8. Finite-difference time-domain simulation of ACU SLT inspection of glued laminated timber beams for specific defect scenarios and year ring curvatures. The peak waveform stress σyy at each pixel of the computation domain is represented, normalized with respect to the mean value along Z. The same logarithmic scale is applied to all snapshots. The pixel size is 200 µm and the time step 100 ns. The ring curvature is the same for all lamellas of each sample and defined with respect to the vertical position y of the pith with respect to the lamella thickness d (40 mm). The size of the simulated glued laminated timber cross-sections is 200 x 320 mm2. 237 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing y/d = -2 the observed variations were negligible. The highest beam distortion was observed when the pith was present within the lamellas (y/d = 0). This effect is as well experimentally observed in Figure 7. A reduced signal amplitude is consistently observed along X around Z positions 250 to 350 mm (Figures 7b, 7c), corresponding to the interactions of the ultrasound beam with the timber lamella between B6 and B7, which contains the pith. In practice, such timber lamellas are generally avoided during glulam manufacture due to their lower mechanical properties. An analysis of the attenuation of ultrasound signals simulated at the receiver transducer with specific defect sizes with respect to well-glued material revealed for y/d = 3 attenuation factors of -45 dB, -21 dB, -6 dB and -3 dB, for defect sections of 100%, 75%, 50% and 25%. Considering the signal variability in defect-free regions, the detectability of defects sections <50% is problematic. An in-depth discussion of the SLT method including several techniques to improve the robustness of the assessment and defect detectability can be found in Sanabria et al. (2013). COMPLEMENTARY INVESTIGATIONS In this chapter the discussion has been restricted to air-coupled ultrasound methodologies for bonding quality assessment of timber laminates. Within the framework of the project, additional investigations were carried out in the field of non-destructive bonding quality assessment of glued timber. An automatized ultrasonic point contact method was developed to optimize the data acquisition and reproducibility of the ultrasonic contact technique. With this purpose, the off-the-shelf shear wave spring-loaded pulse-echo array transducer, which was previously discussed in the Background section, was combined with the computerized mechanical system used in the ACU investigations. The method is single-sided and shows an amplitude reproducibility error <10%. Experiments were performed for commercial glued laminated timber samples with artificial defects and for a 90 year old roofing glulam. With appropriate data evaluation, edge delaminations deeper than 20 mm can be successfully detected in the signature of the surface wave and large scale delaminations (>80% of beam width) in the backwall echo. The data interpretation was supported by finite-difference time-domain simulations (Neuenschwander et al., 2013; Sanabria et al., 2011b). An X-ray limited-angle computed tomography (LCT) method has been investigated for the detection of gluing defects in timber laminates. In order to overcome the limitations associated to conventional computer tomography methods (previously discussed in the Background section), only a reduced number of radiographies in a small angular range (0.6 to 1.8°) parallel to the inspected timber glue lines were used in the three-dimensional reconstruction. The method was implemented in a 238 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing laboratory environment with a microfocus system. A dramatic reduction in the measurement and reconstruction times was achieved. Moreover, density gradients in the wood timber lamellas (earlywood/latewood transitions, wood knots) were filtered out while highlighting the information from the glue lines. The assessment is theoretically independent of the height and length of the inspected sample. Air gaps down to 150 µm could be detected in 10 and 65 mm thick samples with a lateral resolution >5 mm (Sanabria et al., 2011d). Finally the ACU NT method described has been applied to the characterization of material properties in particleboard composites. ACU images of ultrasound velocity and amplitude were correlated with X-ray radiographies of the density distribution of the samples. Correlations between acoustic parameters and the density and particle geometry were found, which were as well influenced by the testing frequency. FDTD simulations allowed interpretation of the observed trends in terms of multi-scale porosity and grain scattering (Sanabria et al., 2013b). CONCLUSION Air-Coupled Ultrasound (ACU) is a well-suited non-destructive testing technology for the structural health monitoring of glued laminated timber, both during manufacture and at the construction site. The inspection does not require contact between transducers and samples, which leads to highly reproducible measurements (<1% amplitude error). Moreover, a large grid of measurement points can be efficiently acquired by attaching the transducers to a computerized scanning system, the ultrasound beam excitation can be flexibly controlled by adjusting the transducer position and orientation. This allows higher resolution in the imaging of defect positions and geometries, together with a better differentiation of defects from background material variability. The classical constraint of this technology is the inefficient coupling of ultrasound waves into solid materials, which has classically limited the assessment to <50 mm thick wood-based composites. However, with a careful system design based on state-of-the-art transducers and electronics, the feasibility of ACU transmission through up to 500 mm thick glued laminated timber has been demonstrated. Ultrasonic waves strongly interact with air-solid discontinuities and therefore show a high sensitivity to cracking and debonding. An ultrasound beam transmitted with normal incidence through a delaminated timber glue line is attenuated by up to 50 dB, gaps as thin as 10 µm provide a contrast of 20 dB. Ultrasonic waves do not only interact with the inspected glue lines, but also with the adjacent timber lamellas. Wood is an anisotropic, heterogeneous and porous material, all of which have a strong influence in the wave propagation. An ultrasound beam propagating 239 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing within timber is gradually shifted from the insonification direction along trajectories, which are a complex function of the annual ring and grain structure. Moreover, mechanical gradients at annual ring and knot heterogeneities scatter the transmitted fields. The porous structure additionally introduces strong damping in the signals transmitted through wood. A finite-difference time-domain simulation tool has been developed to efficiently simulate pulsed ultrasound wave propagation in timber laminates, arbitrarily heterogeneous and anisotropic materials can be simulated by locally defining the mechanical properties at each pixel. A normal transmission setup has been first investigated, which transmits an ultrasound beam perpendicular to the bonding stack, providing a global assessment for each length and width position along the glued laminated timber sample. Delaminations and cracks induced by exterior climatic conditions were successfully detected. The ACU assessment is in excellent agreement with delamination indications obtained by sizing edge open cracks with a feeler gauge, providing moreover information about inner defects. For thin laminates (<40 mm) the lateral resolution in the images is limited by the beamwidth coupled by the ACU transducers, defects <20 mm size are typically assessed. As the thickness of the timber laminate increases, so does the variability of the signals recorded at defect-free regions and the spread of the ultrasound beam, leading to an overall lateral resolution loss. The reduction in lateral resolution is more significant in grain than in cross-grain direction, making the method well-suited for the assessment of lengthwise elongated cracking and delamination. For structural glulam with a large number of lamellas (beam height >300 mm) and constrained access to the beam surfaces parallel to the bonding planes, a slanted lateral transmission setup has been proposed. Here an ultrasound beam is coupled with a small inclination with respect to the inspected glue lines. This setup allows determining which specific bonding planes of the glued stack are defective. Moreover, it is not limited by the height and length of the inspected sample. The applicability of this method has been successfully validated in multi-layered glued laminated timber beams; the position and geometry of multiple defects were successfully identified. The defect detectability limits were as well discussed with the help of finite-difference time-domain simulations. The timber lamellas strongly scatter the incident ultrasound fields, leading to an energy distribution which is not concentrated within the pre-calculated propagation paths. The energy distribution is strongly coupled with the annual ring structure, leading to significant position drifts in the wave propagation paths, and spurious signal coupling in the timber lamellas adjacent to the inspected ones. Defects down to 50% width section were successfully assessed in commercial glued laminated timbers with general annual ring orientations in each timber lamella. The described method an installation led to a Swiss patent application (Sanabria et al., 2011c). 240 Bonding Defect Imaging in Glulam with Novel Air-Coupled Ultrasound Testing FUTURE RESEARCH DIRECTIONS An in-depth discussion of the SLT method including several techniques to improve the robustness of the assessment and defect detectability is under preparation. So far, the developed Finite-Difference Time-Domain (FDTD) numerical simulation model has been applied to predict and interpret the ACU wave propagation phenomena occurring in timber laminates for a priori defined transducer excitation, material properties and defect configurations. The model has been verified with analytical results and shows a good quantitative agreement with parametric experimental studies (not shown). The question naturally rises, whether the inverse problem is as well feasible, that is, whether experimentally acquired ultrasound fields can be used as input to the simulation model. The objective is to partially compensate for known material heterogeneity and anisotropy in wood material, in order to improve the detectability and lateral resolution of the bonding assessment. Further research is planned in this direction. The developed NT and SLT setups have been tested with real glued laminated timber samples in a laboratory environment. 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